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Measurement of the average viscometric degree of polymerization of new and aged cellulosic electrically insulating materials
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GB/T 29305-2012
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Basic data | Standard ID | GB/T 29305-2012 (GB/T29305-2012) | | Description (Translated English) | Measurement of the average viscometric degree of polymerization of new and aged cellulosic electrically insulating materials | | Sector / Industry | National Standard (Recommended) | | Classification of Chinese Standard | K15 | | Classification of International Standard | 29.035.01 | | Word Count Estimation | 20,266 | | Quoted Standard | IEC 60814; ISO 287; ISO 3105 | | Adopted Standard | IEC 60450-2004/Amd 1-2007, IDT | | Regulation (derived from) | National Standards Bulletin No. 41 of 2012 | | Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China | | Summary | This standard specifies the kind of new and aged cellulosic electrically insulating materials viscosity average degree of polymerization (DP) measurement standard method. This standard applies to all cellulosic insulation materials, such as transformers, |
GB/T 29305-2012: Measurement of the average viscometric degree of polymerization of new and aged cellulosic electrically insulating materials ---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Measurement of the average viscometric degree of polymerization of new and aged cellulosic electrically insulating materials
ICS 29.035.01
K15
National Standards of People's Republic of China
New and aged cellulosic electrically insulating materials
Measuring the viscosity average degree of polymerization
(IEC 60450.2004 Al.2007, IDT)
Issued on. 2012-12-31
2013-06-01 implementation
Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China
Standardization Administration of China released
Table of Contents
Preface Ⅰ
Introduction Ⅱ
1 Scope 1
2 Normative references 1
3 Terms and definitions, symbols 1
4 Principle 3
5 Equipment and Reagent 3
Sample 4 6
7 Test Step 4
8 Test Report 8
Appendix A (normative) copper ethylene diamine solution 10
Preparation (normative) copper ethylene diamine Appendix B 11
Annex C (normative) copper ethylene diamine solution
cEn
cCu
Ratio calibration procedure 13
Annex D (informative) function according to Martin equation [ν] · c multiplied νs Table 14
References 15
Foreword
This standard was drafted in accordance with GB/T 1.1-2009 given rules.
This standard uses the translation method identical with IEC 60450.2004 A1.2007 "New and cellulosic electrically insulating material sticky after aging
Average degree of polymerization of the measure. "
Consistency correspondence with this standard Normative documents of the following documents.
--- GB/T 462-2008 paper, board and pulp - Determination of water samples (ISO 287. 1985, MOD)
The standard proposed by China Electrical Equipment Industrial Association.
This standard by the National Electrical insulation materials and insulation systems assessment Standardization Technical Committee (SAC/TC301) centralized.
Participated in the drafting of this standard. Suzhou Jufeng Electrical Insulation Systems Co., Ltd., Beijing Electrical Machinery Industry Technology Research Institute of Economy,
Shenzhen City, measuring Detection Technology Co., Ltd., Shanghai Electric Equipment detection.
The main drafters of this standard. Wang, Xia Yu, Liu Yali, Liu Shufen, Guo Bing, Sun Huashan, ZHAO Chao, Guo Liping.
Introduction
Experience has shown the need to improve test methods and new cellulosic electrically insulating material sticky after aging average degree of polymerization may be repeated speculation.
This standard applies to oxidative degradation in the processing stage and outflow generated. Another important factor is the need to ensure that the materials used to dissolve
And it is used, which is accelerated outflow.
New and aged cellulosic electrically insulating materials
Measuring the viscosity average degree of polymerization
1 Scope
This standard specifies a new electrical insulating materials and cellulose sticky after aging average degree of polymerization to standard methods (DPν) measurements.
This standard applies to all cellulose insulation, cellulose insulation such as transformers, cables, capacitors and other products used.
Test methods described in this standard also applies to after chemical modification can be completely dissolved in the solvent selection kraft intrinsic viscosity measurement.
The test method described in this standard when glazed kraft paper for caution.
Note. For a sample material, the degree of polymerization of the cellulose molecule is not the same, so the average degree of polymerization as measured by the viscosity may be related by other methods (such as
Osmosis or ultra-centrifugation) different values \u200b\u200bmeasured.
2 Normative references
The following documents for the application of this document is essential. For dated references, only the dated version suitable for use herein
Member. For undated references, the latest edition (including any amendments) applies to this document.
The water content of the oil insulating liquid IEC 60814 Paper and board Determination by Karl Fischer titration with automatic power
(Insulatingliquids-Oil-impregnatedpaperandpressboard-Determinationofwaterbyautomatic
coulometricKarlFischertitration)
ISO 287 paper, board and pulp - Determination of water samples for analysis (Paperandboard-Determinationofmoisture
content-Oven-dryingmethod)
ISO 3105 glass capillary kinematic viscosity specifications and operating instructions (Glasscapilarykinematicviscometers-Spec-
ificationsandoperatinginstructions)
3 Terms and definitions, symbols
The following terms and definitions, symbols apply to this document.
3.1 Terms and Definitions
3.1.1
Degree of polymerization of the cellulose molecule degreeofpolymerizationofacelulosemolecule
Cellulose molecules of anhydrous glucose monomers number -β- (C6H10O5) is.
Note. Figure 1 shows the chemical formula of the cellulose molecule.
1 cellulose molecule chemical structural formula diagram
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