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GB/T 29170-2012: Petroleum and natural gas industries -- Drilling fluids -- Laboratory testing
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Petroleum and natural gas industries -- Drilling fluids -- Laboratory testing
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GB/T 29170-2012
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Basic data | Standard ID | GB/T 29170-2012 (GB/T29170-2012) | | Description (Translated English) | Petroleum and natural gas industries -- Drilling fluids -- Laboratory testing | | Sector / Industry | National Standard (Recommended) | | Classification of Chinese Standard | E13 | | Classification of International Standard | 75.020 | | Word Count Estimation | 95,965 | | Quoted Standard | GB/T 261; GB/T 262; GB/T 1884; GB/T 3535; GB/T 5005-2010; GB/T 6682-2008; GB/T 16783.1; GB/T 16783.2; ISO 91-1-1992; ISO 3007; ISO 3104; ISO 3405-2011; ISO 3839; ASTM D1141; ASTM D4052; ASTM D5186; ASTM E100; IP 391 | | Adopted Standard | ISO 10416-2008, MOD | | Regulation (derived from) | National Standards Bulletin No. 41 of 2012 | | Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China | | Summary | This standard specifies the water recycling system (hereinafter referred to as " water plant") classification, technology portfolio, general requirements, selection, testing and acceptance requirements. This standard applies to agricultural water, industr | GB/T 29170-2012: Petroleum and natural gas industries -- Drilling fluids -- Laboratory testing---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Petroleum and natural gas industries. Drilling fluids. Laboratory testing
ICS 75.020
E13
National Standards of People's Republic of China
Oil drilling and natural gas industries laboratory tests
(ISO 10416.2008, MOD)
Issued on. 2012-12-31
2013-07-01 implementation
Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China
Standardization Administration of China released
Table of Contents
Preface Ⅶ
Introduction Ⅷ
1 Scope 1
2 Normative references 1
3 Terms and definitions 2
4 Symbols and abbreviations 2
4.1 Symbols 2
4.2 Abbreviations 4
The physical properties of barite powder 4 5
5.1 Overview 4
5.2 Reagents and Instruments 4
Sampling 5 5.3
5.4 Calculation of water 5
5.5 sieve residue analysis 6
5.6 Settlement of 6
6 barite powder rheological properties of the drilling fluid 10
6.1 Overview 10
6.2 Reagents and Instruments 11
6.3 based drilling fluid slurry preparation 11
6.4 Rheological test 12
6.5 Calculation 12
7 aggravate abrasive material 13
7.1 Overview 13
7.2 Reagents and Instruments 13
7.3 abrasive test 13
8 drilling barite powder mercury content 14
8.1 Overview 14
8.2 Reagents and Instruments 15
8.3 Preparation of standard solution of mercury 16
Sample digestion 16 8.4
8.5 recovery test mercury digestion period of 16
8.6 standard solution and sample analysis 16
8.7 Calculation 17
9 drilling barite powder, cadmium and lead content 17
9.1 Overview 17
9.2 Reagents and Instruments 17
Cd and Pb compound preparation 9.3 standard solution of 18
Sample digestion 18 9.4
9.5 standard solution and sample analysis 18
9.6 Calculation 19
10 drilling barite powder with arsenic content of 19
10.1 Overview 19
10.2 Reagents and Instruments 19
20 10.3 Preparation of standard solution
10.4 20 sample digestion
10.5 Analysis of the standard solution and the sample solution 21
21 10.6 Calculation
11 bridge plugging material 21
11.1 Overview 21
21 11.2 Instrument
11.3 Preparation of test drilling 22
11.4 Static test program slit 22
11.5 dynamic test procedure slit 22
11.6 Static test bed program 22 marbles
11.7 marbles dynamic test bed program 23
11.8 Static test program 23 balls bed
11.9 ball dynamic test bed program 23
12 fluid loss additive 23
12.1 Overview 23
12.2 Reagents and Instruments 23
12.3 Base paste formulated to claim 25
12.4 saturated brine drilling fluid 25
12.5 High hardness saturated brine drilling fluid 25
12.6 10% KCl drilling fluid 25
12.7 Pre-hydrated bentonite slurry 26
12.8 artificial seawater drilling fluid 26
12.9 Low concentration brine drilling fluid 26
12.10 27 drilling calcium treatment
12.11 low solids non-dispersed drilling fluid 27
12.12 Freshwater lignosulfonate drilling 27
12.13 Initial performance testing 28
After heat aging performance test 12.14 28
13 cuttings and commodity bentonite methylene blue test (MBT) 28
13.1 cuttings methylene blue capacity 28
13.2 Goods Bentonite methylene blue capacity 31
13.3 Solid content 32
Deflocculation diluent rating 32 14
14.1 Overview 32
14.2 Reagents and Instruments 33
14.3 Moisture measurement program 33
14.4 Calculation of water 34
14.5 Base paste formulated 34
34 14.6 Calculation
14.7 Determination of flow variability 35
14.8 diluent computing efficiency 36
15 test drilling 36 oil base
15.1 Overview 36
15.2 Reagents and Instruments 36
15.3 density, relative density (specific gravity), or API Gravity --- liquid density method (in line with the provisions of GB/T 1884's) 36
15.4 digital density meter measuring liquid density and relative density (in line with the provisions of ASTMD4052) 36
15.5 kinematic viscosity of transparent and opaque liquid petroleum --- calibration capillary method (ISO 3104 compliance) is 37
15.6 distillate (of compliance with ISO 3405) 37
15.7 aniline point and mixed aniline point (in line with GB/T 262-2010 requirements) 37
15.8 pour point (in line with GB/T 3535 provisions) 38
15.9 Pensky - Martens closed cup flash point test method (in line with GB/T 261 requirements) 38
15.10 aromatics content (in compliance with IP391 or ASTMD5186) 38
16 potassium ion content --- Ion Selective Electrode 39
16.1 Overview 39
16.2 Reagents and Instruments 39
16.3 Electrode Preparation 40
16.4 operating system to check the electrode 40
16.5 Concentration direct reading instrument measurement 41
16.6 millivolts digital or analog output measurement instrument 41
17 Calcium content --- Ion Selective Electrode 41
17.1 Overview 41
17.2 Reagents and Instruments 42
17.3 Electrode Preparation 42
17.4 operating system to check the electrode 43
17.5 Concentration direct reading instrument measurement 43
17.6 millivolts digital or analog output measurement instrument 43
18 Sodium content --- Ion Selective Electrode 44
18.1 Overview 44
18.2 Reagents and Instruments 44
Prepare and check the electrode system 45 18.3
18.4 Concentration direct reading instrument measurement 45
18.5 millivolts digital or analog output measurement instrument 46
The true density of solid density --- 19 46 Law
19.1 Overview 46
46 19.2 Instrument
19.3 Test Procedure Act 46 --- true density
19.4 --- calculate the true density of France 47
20 solid density --- air Pyknometer 47
20.1 Overview 47
47 20.2 Instrument
20.3 Test procedure --- air Pyknometer 48
20.4 Calculation --- air Pyknometer 48
Conservation of water-based drilling fluid 21 48
21.1 Overview 48
Conventional drilling operations 21.2 sample preparation, processing and testing 48
Sample preparation and maintenance of drilling fluid at room temperature 21.3 49
21.4 Drilling Fluid temperature [temperature to 65 ℃ (150 ℉)] Conservation 50
High temperature drilling fluid 21.5 [higher than 65 ℃ (150 ℉)] Conservation 51
21.6 high temperature curing tanks inert and chemical compatibility 53
21.7 Conservation drilling needed supplies and services 53
22 oil-based drilling fluids conservation 54
22.1 Overview 54
54 22.2 Instrument
Conventional drilling operations 22.3 sample preparation, processing and testing 55
22.4 drilling fluid at room temperature curing 56
22.5 Drilling Fluid temperature [temperature to 65 ℃ (150 ℉)] Conservation 56
High temperature drilling fluid 22.6 [higher than 65 ℃ (150 ℉)] Conservation 57
22.7 high temperature curing tanks inert and chemical compatibility 58
22.8 Conservation drilling needed supplies and services 59
Scroll shale recovery test 23 59
23.1 Overview 59
23.2 Reagents and Instruments 59
23.3 Determination program 60
61 23.4 Calculation
24 drilling material --- high viscosity polyanionic cellulose (PAC-HV) (General) 61
24.1 Overview 61
24.2 Moisture 61
24.3 PAC-HV test fluid containing the test program 62
25 drilling materials --- low viscosity polyanionic cellulose (PAC-LV) 64
25.1 Overview 64
25.2 Moisture 64
25.3 PAC-LV containing the test fluid measurement program 65
26 invert emulsion drilling fluid formulation and evaluation 67
26.1 Overview 67
26.2 Reagents and Instruments 67
26.3 based slurry mixing procedure 68
26.4 Performance Test drilling fluid base mud 69
Sample preparation 26.5 pollution of the sea 69
Evaluation of soil contaminated samples preparation 26.6 69
26.7 composite brine sample preparation contamination 69
26.8 hot rolling conservation program 69
26.9 stationary conservation program 70
26.10 after curing test program 70
27 Determination of drilling HTHP filtration loss 70 screwed lid type permeability tester closure
27.1 Overview 70
27.2 Safety Precautions 70
27.3 Instrument --- screw lid closure type permeability tester 72
27.4 HTHP Filtration test program 73
76 27.5 end of the test and removal
27.6 Data Report 77
28 threaded lid sealing formula permeability measured drilling HTHP filtration loss 78
28.1 Overview 78
28.2 Safety Precautions 78
28.3 Instrument --- threaded lid closure type permeability tester 79
28.4 HTHP Filtration test program 81
83 28.5 end of the test and removal
28.6 Data Report 84
Appendix A (informative) This standard and ISO 10416.2008 technical differences and their reasons 85
References 86
Foreword
This standard was drafted in accordance with GB/T 1.1-2009 given rules.
This standard uses redrafted Law Amendment uses ISO 10416.2008 "oil and gas industry drilling laboratory tests" (English
Version).
This standard and ISO 10416.2008 technical differences exist compared to the terms of these differences involved have been incorporated into the body and through the outer
Vertical singlet side margin position (|) have been marked, the list given in Appendix A corresponding technical differences and their causes.
This standard also made the following editorial changes.
a) use the "standard" instead of "this International Standard";
'.' B) with a decimal point instead of a comma as the decimal point, '';
c) the text of the original text has been corrected the wrong place.
1) Original Table 2, 3.31 and 3.20 to be exchanged;
2) Original 8.2.16 in 8mm (3/16in) should be changed to 8mm (5/16in);
3) should be replaced by the original 9.5.5 228.8nm 283.3nm;
5) Original 14.2.7 and 26.2.6 in 10000r/min ± 100r/min should be changed to 1000r/min ± 100r/min;
6) should be replaced in its original 14.5.1 in 350g 360g;
7) Original 14.7.1 in 750r/min ± 50r/min should be changed to 7500r/min ± 500r/min;
8) should be replaced by the original 16.2.3 in 5mol 5mol/L;
9) the original formula (26) should be replaced in md m0;
10) Original 24 23.1.1 to 24.1.1;
11) Original 24.3.1.10 and 25.3.1.10 should be replaced in the 150 ℉ 140 ℉;
12) Original 25.2.1.1 in 25 ℃ ± 1 ℃ (77 ℉ ± 3 ℉) should be changed to 105 ℃ ± 3 ℃ (220 ℉ ± 5 ℉);
13) Original 26.4.1 in 50 ℃ (300 ℉) should be changed to 50 ℃ (120 ℉);
14) Original 27.4.1.3 and 28.4.1.3 in 6 ℃ (10 ℉) should be changed to 6 ℃ (43 ℉);
15) The original 28.2.6.1 6200kPa (460psi) should be changed to 6200kPa (900psi);
16) The original 28.3.1.4 9.87 × 10-16m2 ~ 9.87 × 10-11 m2 (100 mD ~ 100D) should be replaced
1.02 × 10-13m2 ~ 1.02 × 10-10m2 (100mD ~ 100D).
This standard by the National Standardization Technical Committee of Oil and Gas (SAC/TC355) and focal points.
This standard was drafted. China Research Institute of Petroleum and Chemical Corporation Zhongyuan Petroleum Exploration Bureau drilling engineering technology.
The main drafters of this standard. Zhenjian Wu, Meng Lei Zu, WANG Xing-wu, Zhang Qilin, Mengli Yan, Song Shijun, ANS.
Introduction
Determination of drilling fluid materials used in this standard is referenced from APIRP13I seventh edition/ISO 10416.2002 [2]. This standard provides
More and more rigorous testing methods to ensure the reproducibility and accuracy of test results. This standard applies to laboratory tests, if the site has
More sophisticated equipment, through strict control of experimental conditions, can also be used for on-site drilling tests.
This standard is used to test drilling site maintenance unconventional performance, and field testing standards GB/T 16783.1 and
GB/T 16783.2 compared to test results or more accurately, or to provide on-site testing standard does not mention the performance test method.
Users of this standard process can be made more or different requirements according to the special requirements of this standard is not intended to prevent vendors push
Or a user acceptance test in favor of improvements in technology and innovative alternative products or engineering technology programs. When there are alternative products or technologies introduced
, The supplier shall submit their differences with the technical specifications of this standard.
If the test requires the use of hazardous chemicals, the user of this standard should have the appropriate knowledge and acceptance of the use and handling of these chemicals
Training. Users should comply with local, regional and national labor laws and the HSE regulations.
The standard example of a footnote apparatus, reagents and materials are examples of suitable commercially available products. This information is given for the convenience of the standard
The user does not imply an endorsement of these products, if other equivalent product has the same effect, you can use these equivalent products.
Oil drilling and natural gas industries laboratory tests
1 Scope
This standard specifies the method for laboratory testing of materials and drilling mud physical, chemical, rheological properties.
This standard applies to water-based drilling fluids, oil-based drilling fluids and other fluid-based solutions or man made.
This standard does not apply to control drilling fluid properties detailed manual. Since the test temperature and stirring conditions on drilling performance significantly
The present standard gives the recommended test temperature and stirring conditions.
2 Normative references
The following documents for the application of this document is essential. For dated references, only the dated version suitable for use herein
Member. For undated references, the latest edition (including any amendments) applies to this document.
GB/T 261 Flash Point by Pensky - Martens closed cup method (GB/T 261-2008, ISO 2719.2002, MOD)
GB/T 262 Petroleum products and hydrocarbon solvents aniline point and mixed aniline point measurement method (GB/T 262-2010, ISO 2977.1997,
MOD)
GB/T 1884 crude oil and liquid petroleum products - Laboratory determination of density (density meter method) (GB/T 1884-2000, eqv ISO
3675.1998)
GB/T 3535 Petroleum products - Determination of pour point (GB/T 3535-2006, ISO 3016.1994, MOD)
GB/T 5005-2010 drilling material specification (ISO 13500.2008, MOD)
GB/T 6682-2008 analytical laboratory use specifications and test methods (ISO 3696. 1987, MOD)
GB/T 16783.1 Petroleum and natural gas industries - Field testing of drilling fluids - Part 1. Water-based drilling fluids
GB/T 16783.2 Petroleum and natural gas industries - Field testing of drilling fluids - Part 2. Oil-based drilling fluids (GB/T 16783.2-
2012, ISO 10414-2.2002, MOD)
ISO 91-1.1992 Petroleum Measurement Tables - Part 1. 60 ℉ to 15 ℃ and the temperature of the standard table (Petroleum
measurementtables-Part 1. Tablesbasedonreferencetemperaturesof15 ℃ and60 ℉)
ISO 3007 Petroleum products and crude oil measurement Reid vapor pressure (Reid) Act (Petroleumproductsandcrudepe-
troleum-Determinationofvapourpressure-Reidmethod)
Determination and calculation of dynamic viscosity ISO 3104 Petroleum products - Transparent and opaque liquids kinematic viscosity (Petroleum
products-Transparentandopaqueliquids-Determinationofkinematicviscosityandcalculationof
dynamicviscosity)
Determination (Petroleumproducts-Determinationofdis- distillation characteristics of petroleum products under pressure 2011. ISO 3405
tilationcharacteristicsatatmosphericpressure)
ISO 3839 Petroleum products distillates and aliphatic olefins - Determination of bromine number potentiometric titration (Petroleumproducts-Deter-
minationofbrominenumberofdistilatesandaliphaticolefins-Electrometricmethod)
ASTMD1141 seawater substitutes (Standardpracticeforpreparationofsubstituteoceanwater)
ASTMD4052 digital density meter test method for determining the density and relative density of the liquid (Standardtestmethodforden-
sityandrelativedensityofliquidsbydigitaldensitymeter)
ASTMD5186 measured diesel and aviation turbine fuel aromatic content and polynuclear aromatics content by supercritical fluid chromatography
Standard Test Method (Standardtestmethodfordeterminationofaromaticcontentandpolynucleararomatic
|