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Carbonaceous materials used in the production of aluminium -- Calcined coke -- Part 2: Determination of trace elements content -- Flame atomic absorption spectroscopy
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GB/T 26310.2-2010
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Basic data Standard ID | GB/T 26310.2-2010 (GB/T26310.2-2010) | Description (Translated English) | Carbonaceous materials used in the production of aluminium -- Calcined coke -- Part 2: Determination of trace elements content -- Flame atomic absorption spectroscopy | Sector / Industry | National Standard (Recommended) | Classification of Chinese Standard | Q52 | Classification of International Standard | 71.100.10 | Word Count Estimation | 10,120 | Date of Issue | 2011-01-14 | Date of Implementation | 2011-11-01 | Quoted Standard | GB/T 26297.6; ISO 385-1-1984; ISO 835-1-1981; ISO 1042-1983; ISO 3696-1987 | Adopted Standard | ISO 8658-1997, IDT | Regulation (derived from) | National Standard Approval Announcement 2011 No.85 | Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China | Summary | This standard specifies the method for the determination of primary aluminum production and use of trace elements in focus after forging oil. This section applies to the ash content of petroleum coke is not greater than the determination of trace elements in 1% after forging. Measuring range (mass fraction) are shown in Table 1. |
GB/T 26310.2-2010: Carbonaceous materials used in the production of aluminium -- Calcined coke -- Part 2: Determination of trace elements content -- Flame atomic absorption spectroscopy ---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Carbonaceous materials used in the production of aluminium Calcined coke Part 2. Determination of trace elements content Flame atomic absorption spectroscopy.
ICS 71.100.10
Q52
National Standards of People's Republic of China
Primary aluminum production of calcined petroleum coke detection method
Determination of trace element contents. Part 2
Flame Atomic Absorption Spectrometry
Part 2. Determinationoftraceelementscontent-
(ISO 8658.1997, Carbonaceousmaterialsforuseintheproductionof
traceelementsbyflameatomicabsorptionspectroscopy, IDT)
Issued on. 2011-11-01 2011-01-14 implementation
Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China
Standardization Administration of China released
Foreword
GB/T 26310 "primary aluminum production of calcined petroleum coke detection method," a total of five sections.
--- Part 1. Determination of density in xylene Pyknometer;
--- Part 2. Determination of trace elements by flame atomic absorption spectrometry;
--- Part 3. Determination of apparent oil heating;
--- Part 4. Determination of oil content by solvent extraction;
--- Part 5. Determination of the residual hydrogen content.
This is Part 2 GB/T 26310 of.
This part identical with ISO 8658.1997 "Determination of aluminum production side with carbon material after calcined coke and petroleum coke Trace Elements
Flame Atomic Absorption Spectrometry. " This part identical with ISO 8658.1997, the standard for style and consistency of the front
Introduction INTRODUCTION deleted, and the precision of the terms listed separately chapter.
This part is proposed by the China Nonferrous Metals Industry Association.
The non-ferrous metal part by the National Standardization Technical Committee.
This section is responsible for drafting units. Aluminum Corporation of China Zhengzhou Research Institute, China Nonferrous Metals Industry Quality Standards and Metrology Institute
The study.
Participated in the drafting of this section. Shandong Chenyang Carbon Co., Ltd., Shandong Nanshan Aluminum Co., Ltd., a limited cable-Development
the company.
The main drafters of this section. Liyue Ping, Zhang Wei-hua, Shi Lei, Zhang Jie, Mr Chan Jun, Gulu Ning.
Primary aluminum production of calcined petroleum coke detection method
Determination of trace element contents. Part 2
Flame Atomic Absorption Spectrometry
1 Scope
This section GB/T 26310 specifies the method for determination of primary aluminum production Coke Trace Elements Calcined petroleum.
This section applies to an ash content of not greater than the determination of trace elements in petroleum coke after 1% fumed. Measurement range (mass fraction) are shown in Table 1.
Table 1
element
Measuring range /%
no greater than
element
Measuring range /%
no greater than
element
Measuring range /%
no greater than
Calcium Chromium 0.005 0.025 0.025 Copper
Magnesium iron 0.030 0.010 0.010 Lead
Nickel 0.050 0.100 0.001 silicon manganese
Vanadium Zinc 0.100 0.004 - -
2 Normative references
The following documents for the application of this document is essential. For dated references, only the dated version suitable for use herein
Member. For undated references, the latest edition (including any amendments) applies to this document.
GB/T 26297.6 carbonaceous materials used in aluminum sampling methods - Part 6 calcined petroleum coke (GB/T 26297.6-2010,
ISO 6375. 1980, IDT)
ISO 385-1. 1984 Laboratory glassware graduated tube - Part 1. General requirements
ISO 835-1. 1981 Laboratory glassware graduated pipettes - Part 1. General requirements
ISO 1042. 1983 laboratory glassware volumetric flask
ISO 3696. 1987 laboratory use - Specification and test methods
3 PRINCIPLE OF THE METHOD
The sample to be tested is placed in a muffle furnace at 700 ℃ calcined at 10h, the resulting molten ash using a mixture of boric acid and sodium carbonate, with
Dilute hydrochloric acid to dissolve the melt, the resulting solution Determination of trace elements using atomic absorption spectrometry.
4 Reagents
4.1 anhydrous sodium carbonate (excellent pure).
4.2 borate (excellent pure).
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