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GB/T 23594.1-2009: Chemical analysis methods of rare earth contents in samarium-europium-gadolinium concentrates -- Part 1: Determination of total rare earth oxide content -- Gravimetry
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| Standard ID | Contents [version] | USD | STEP2 | [PDF] delivered in | Standard Title (Description) | Status | PDF |
| GB/T 23594.1-2009 | English | 189 |
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Chemical analysis methods of rare earth contents in samarium-europium-gadolinium concentrates -- Part 1: Determination of total rare earth oxide content -- Gravimetry
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GB/T 23594.1-2009
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Basic data | Standard ID | GB/T 23594.1-2009 (GB/T23594.1-2009) | | Description (Translated English) | Chemical analysis methods of rare earth contents in samarium-europium-gadolinium concentrates -- Part 1: Determination of total rare earth oxide content -- Gravimetry | | Sector / Industry | National Standard (Recommended) | | Classification of Chinese Standard | H14 | | Classification of International Standard | 77.120.99 | | Word Count Estimation | 8,859 | | Date of Issue | 2009-04-23 | | Date of Implementation | 2010-02-01 | | Regulation (derived from) | National Standard Approval Announcement 2009 No.5 (Total No.145) | | Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China | | Summary | This standard specifies the method for the determination of total rare earth oxides of europium, gadolinium, samarium enriched composition. This section applies to samarium determination of total rare earth oxides of europium, gadolinium enrichment. Measuring range: solid europium, samarium, gadolinium enrichment 90. 00%-99. 00%, liquid europium, samarium, gadolinium enrichment 100g/L ~ 300g/L. | GB/T 23594.1-2009: Chemical analysis methods of rare earth contents in samarium-europium-gadolinium concentrates -- Part 1: Determination of total rare earth oxide content -- Gravimetry
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Chemical analysis methods of rare earth contents in samarium-europium-gadolinium concentrates Part 1. Determination of total rare earth oxide content Gravimetry.
ICS 77.120.99
H14
National Standards of People's Republic of China
Chemical analysis of Sm-Eu-Gd Concentrate
Part 1. Determination of total rare earth oxides
Gravimetric method
Posted 2009-04-23
2010-02-01 implementation
Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China
Standardization Administration of China released
Foreword
GB/T 23594-2009 "Methods for chemical analysis of Sm-Eu-Gd Concentrate" is divided into two parts.
--- Part 1. Determination of total rare earth oxide gravimetric method;
--- Part 2. fifteen rare earth element oxide with components measured by inductively coupled plasma emission spectrometry.
This is Part 1.
This part of the National Standardization Technical Committee rare and centralized.
This part of the Inner Mongolia Baotou Steel Rare Earth Hi-Tech Company, China Nonferrous Metals Industry Institute of Standards Metrology and Quality is responsible for drafting.
This section is Jiangyin Jiahua Advanced Material Resources Co., Ltd., Baotou Rare Earth Research Institute, Baotou Huamei Co. participated in the drafting.
The main drafters of this section. Zhanggui Mei, Wang Xinping, Xu Ning.
The drafters of some of the participants. Yao Jingbi, Yao Wenji, Zhang Shujie, Luan red, red Zhou Kai, Gong Jianhua.
Chemical analysis of Sm-Eu-Gd Concentrate
Part 1. Determination of total rare earth oxides
Gravimetric method
1 Scope
This section provides for the determination of total rare earth oxide Sm-Eu-Gd Concentrate.
This section applies to the determination of samarium rare earth oxides of europium, gadolinium total Concentrate. Measurement range. solid Sm-Eu-Gd Concentrate 90.00% ~
99.00%; liquid Sm-Eu-Gd Concentrate 100g/L ~ 300g/L.
2 principle of the method
Sample was dissolved in hydrochloric acid, in the presence of ammonium chloride under the conditions, pH > 9 with an aqueous ammonia precipitation of rare earth, separated calcium, magnesium. Nitrate and perchlorate
Acid destruction of paper, dissolve the precipitate, removed from the filtrate after the silicon with rare earth oxalate precipitation, the pellet burning into oxides, constant weight.
3 Reagents and materials
3.1 ammonium chloride.
3.2 hydrochloride (ρ1.19g/mL).
3.3 HCl (1 + 1).
3.4 hydrochloric acid (0.0119g/L).
Nitrate 3.5 (ρ1.42g/mL).
3.6 perchloric acid (ρ1.67g/mL).
3.7 Hydrogen peroxide (30%).
Ammonia 3.8 (1 + 1).
3.9 ammonia - ammonium chloride washing liquid. 2g of ammonium chloride dissolved in 95mL water, adjusted to pH9 ~ pH10 with aqueous ammonia when used.
3.10 oxalic acid solution (100g/L).
3.11 oxalic acid wash (10g/L).
3.12 cresyl violet ethanol solution (1g/L).
4 Instrument
4.1 high-temperature furnace. temperature > 1000 ℃.
4.2 platinum crucible.
5 Sample
5.1 solid sample Sm-Eu-Gd oxide concentrate burning at 950 ℃ 1h, placed in a desiccator, cooled to room temperature, and immediately weighed.
Sm-Eu-Gd sample 5.2 solid carbonate concentrate weighed immediately after opening.
5.3 Sm-Eu-Gd Concentrate liquid sample dispensing shake.
Step 6 Analysis
6.1 Sample
6.1.1 Solid samples samarium europium, gadolinium oxide concentrate of. Weigh 0.2000g sample (5.1), accurate to 0.0001g.
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