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GB/T 22982-2008 English PDF

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GB/T 22982-2008: Determination of metronidazole, ronidazole, dimetridazole residues in milk and milk powder -- LC-MS-MS method
Status: Valid
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GB/T 22982-2008English229 Add to Cart 3 days [Need to translate] Determination of metronidazole, ronidazole, dimetridazole residues in milk and milk powder -- LC-MS-MS method Valid GB/T 22982-2008

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Basic data

Standard ID GB/T 22982-2008 (GB/T22982-2008)
Description (Translated English) Determination of metronidazole, ronidazole, dimetridazole residues in milk and milk powder -- LC-MS-MS method
Sector / Industry National Standard (Recommended)
Classification of Chinese Standard X04
Classification of International Standard 67.050
Word Count Estimation 10,117
Date of Issue 2008-12-31
Date of Implementation 2009-05-01
Quoted Standard GB/T 6379.1; GB/T 6379.2; GB/T 6682
Regulation (derived from) National Standard Approval Announcement 2008 No.26 (Total No.139)
Issuing agency(ies) General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China
Summary This standard specifies the milk and milk powder metronidazole, ronidazole, two residues of metronidazole and its metabolites by high performance liquid chromatography-tandem mass spectrometry. This standard applies to milk and milk powder metronidazole, ronidazole, two metronidazole and its metabolites residues determination and confirmation. This standard method detection limit: milk metronidazole, ronidazole, two metronidazole 0. 5��g/kg, hydroxy metronidazole 1��g/kg, 1-methyl-2-(hydroxymethyl) -5-nitroimidazole as 2. 5��g/kg, milk metronidazole, ronidazole, two metronidazole 2. 5��g/kg, hydroxy metronidazole 5��g/kg, 1-methyl-2-(hydroxymethyl)-5-nitroimidazole as 12. 5��g/kg.

GB/T 22982-2008: Determination of metronidazole, ronidazole, dimetridazole residues in milk and milk powder -- LC-MS-MS method


---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Determination of metronidazole, ronidazole, dimetridazole residues in milk and milk powder. LC-MS-MS method ICS 67.050 X04 National Standards of People's Republic of China Milk and milk powder metronidazole, Ronidazole, Determination of two metronidazole and its metabolites residues Liquid chromatography - tandem mass spectrometry Posted 2008-12-31 2009-05-01 implementation Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China Standardization Administration of China released

Foreword

The Standard Appendix A, Appendix B is an informative annex. This standard is proposed and managed by the State Administration of Quality Supervision Inspection and Quarantine of People's Republic of China. This standard was drafted. People's Republic of China Exit Inspection and Quarantine Qinhuangdao, Hebei People's Republic of China Entry-Exit Inspection and Quarantine Bureau. The main drafters of this standard. Wang Fengchi, Yilian Feng, Guo Chunhai, paragraph Wenzhong, Chenrui Chun, Lv Hongying, Doucai Yun, Mayu Song, Pang Guofang. Milk and milk powder metronidazole, Ronidazole, Determination of two metronidazole and its metabolites residues Liquid chromatography - tandem mass spectrometry

1 Scope

This standard specifies the milk and milk powder metronidazole, Ronidazole, two of metronidazole and its metabolites residues by high performance liquid chromatography - tandem Mass spectrometry. This standard applies to milk and milk powder metronidazole, Ronidazole, two of metronidazole and its metabolites residues measured and confirmed. The standard method detection limit. milk metronidazole, Ronidazole, two metronidazole 0.5μg/kg, hydroxy metronidazole 1μg/kg, 1-methyl-2-hydroxymethyl-5-nitroimidazole was 2.5μg/kg; milk metronidazole, Ronidazole, two metronidazole 2.5μg/kg, hydroxy metronidazole Oxazole was 5μg/kg, 1- methyl-2-hydroxymethyl-5-nitroimidazole was 12.5μg/kg.

2 Normative references

The following documents contain provisions which, through reference in this standard and become the standard terms. For dated references, subsequent Amendments (not including errata content) or revisions do not apply to this standard, however, encourage the parties to the agreement are based on research Whether the latest versions of these documents. For undated reference documents, the latest versions apply to this standard. GB/T 6379.1 measurement methods and results of Accuracy (trueness and precision) - Part 1. General principles and definitions (GB/T 6379.1- 2004, ISO 5725-1.1994, IDT) GB/T 6379.2 measurement methods and results of Accuracy (trueness and precision) - Part 2. Determine the standard measurement method to repeat Of the basic methods of reproduction (GB/T 6379.2-2004, ISO 5725-2.1994, IDT) GB/T 6682 analytical laboratory use specifications and test methods (GB/T 6682-2008, ISO 3696. 1987, MOD) Principle 3 With acetonitrile - ethyl acetate extract the analyte in the sample, the cationic solid phase extraction (SPE), high performance liquid chromatography - tandem mass spectrometry, within Standard method.

4 Reagents and materials

Unless otherwise stated, all reagents HPLC grade water to a water GB/T 6682 regulations. 4.1 acetonitrile. 4.2 ethyl acetate. 4.3 methanol. 4.4 acetone. 4.5 acetic acid. 4.6 ammonia. 4.7 anhydrous sodium sulfate, AR. After burning 650 ℃ 4h, placed in the dryer set aside. 4.8 ammonia - acetonitrile (1 + 19). amount of 5mL ammonia with acetonitrile and dilute to 100mL. 4.9 Standard. metronidazole (metronidazole, CAS. 13182-89-3), Ronidazole (ronidazole, CAS. 7681-76-7), dimethyl Metronidazole (dimetridazole, CAS. 551-92-8), hydroxy metronidazole (metronidazole-OH, CAS. 7681-76-7), 1- methyl-2-hydroxymethyl Imidazole-5-nitro (hydroxydimetridazole, CAS. 936-05-0), deuterated Ronidazole (RNZ-D3), deuterated hydroxy metronidazole (MZNOH-D2) and deuterated-hydroxymethyl-1-methyl-5-nitroimidazole (HMMNI-D3). 98% or greater purity.

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