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GB/T 22946-2008: Determination of lincomycin, erythromycin, tilmicosin, tylosin, spiramycin, clindamycin, kitasamycinand josamycin residues in royal jelly and lyophilized royal jelly powder -- LC-MS-MS method
Status: Valid
| Standard ID | Contents [version] | USD | STEP2 | [PDF] delivered in | Standard Title (Description) | Status | PDF |
| GB/T 22946-2008 | English | 279 |
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Determination of lincomycin, erythromycin, tilmicosin, tylosin, spiramycin, clindamycin, kitasamycinand josamycin residues in royal jelly and lyophilized royal jelly powder -- LC-MS-MS method
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GB/T 22946-2008
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PDF similar to GB/T 22946-2008
Basic data | Standard ID | GB/T 22946-2008 (GB/T22946-2008) | | Description (Translated English) | Determination of lincomycin, erythromycin, tilmicosin, tylosin, spiramycin, clindamycin, kitasamycinand josamycin residues in royal jelly and lyophilized royal jelly powder -- LC-MS-MS method | | Sector / Industry | National Standard (Recommended) | | Classification of Chinese Standard | X04 | | Classification of International Standard | 67.050 | | Word Count Estimation | 12,135 | | Date of Issue | 2008-12-31 | | Date of Implementation | 2009-05-01 | | Quoted Standard | GB/T 6379.1; GB/T 6379.2; GB/T 6682 | | Regulation (derived from) | National Standard Approval Announcement 2008 No.26 (Total No.139) | | Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China | | Summary | This standard specifies the royal jelly and royal jelly lyophilized powder lincomycin, erythromycin, tilmicosin, tylosin, spiramycin, clindamycin, Kitasamycin and josamycin residues liquid chromatography-tandem mass spectrometry. This standard applies to royal jelly and royal jelly lyophilized powder lincomycin, erythromycin, tilmicosin, tylosin, spiramycin, clindamycin, Kitasamycin and josamycin residues Determination. This standard method detection limit: Royal Jelly lincomycin, erythromycin, tilmicosin, tylosin, spiramycin, clindamycin, Kitasamycin, Josamycin are 2. 0 ��g/kg, royal jelly lyophilized powder in lincomycin, erythromycin, tylosin, clindamycin, josamycin are 2. 0��g/kg, tilmicosin, spiramycin, guitar ADM are 5. 0��g/kg. | GB/T 22946-2008: Determination of lincomycin, erythromycin, tilmicosin, tylosin, spiramycin, clindamycin, kitasamycinand josamycin residues in royal jelly and lyophilized royal jelly powder -- LC-MS-MS method
---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Determination of lincomycin, erythromycin, tilmicosin, tylosin, spiramycin, clindamycin, kitasamycinand josamycin residues in royal jelly and lyophilized royal jelly powder. LC-MS-MS method
ICS 67.050
X04
National Standards of People's Republic of China
Royal jelly and royal jelly lyophilized lincomycin,
Erythromycin, tilmicosin, tylosin, spiramycin,
Clindamycin, neomycin guitar, josamycin
Determination of residues of liquid chromatography - tandem mass spectrometry
Posted 2008-12-31
2009-05-01 implementation
Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China
Standardization Administration of China released
Foreword
The Standard Appendix A, Appendix B is an informative annex.
This standard is proposed and managed by the State Administration of Quality Supervision, Inspection and Quarantine.
This standard was drafted. People's Republic of China Qinhuangdao Exit Inspection and Quarantine.
The main drafters of this standard. Wang Fei, Wang Haiyang, Caoyan Zhong Jia light group, Zhang Jinjie, Shiyu Qiu, Pang Guofang.
Royal jelly and royal jelly lyophilized lincomycin,
Erythromycin, tilmicosin, tylosin, spiramycin,
Clindamycin, neomycin guitar, josamycin
Determination of residues of liquid chromatography - tandem mass spectrometry
1 Scope
This standard specifies the royal jelly and royal jelly lyophilized lincomycin, erythromycin, tilmicosin, tylosin, spiramycin, clindamycin
Su, guitar neomycin and josamycin residues liquid chromatography - tandem mass spectrometry.
This standard applies to royal jelly and royal jelly powder lincomycin, erythromycin, tilmicosin, tylosin, spiramycin, clindamycin
Su, guitar neomycin and josamycin residues determination.
The standard method detection limit. Royal Jelly lincomycin, erythromycin, tilmicosin, tylosin, spiramycin, clindamycin, Kyrgyzstan
He adriamycin, josamycin were 2.0μg/kg; royal jelly freeze-dried powder of lincomycin, erythromycin, tylosin, clindamycin, josamycin
Were 2.0μg/kg, tilmicosin, spiramycin, guitar ADM were 5.0μg/kg.
2 Normative references
The following documents contain provisions which, through reference in this standard and become the standard terms. For dated references, subsequent
Amendments (not including errata content) or revisions do not apply to this standard, however, encourage the parties to the agreement are based on research
Whether the latest versions of these documents. For undated reference documents, the latest versions apply to this standard.
GB/T 6379.1 measurement methods and results of Accuracy (trueness and precision) - Part 1. General principles and definitions
(GB/T 6379.1-2004, ISO 5725-1.1994, IDT)
GB/T 6379.2 measurement methods and results of Accuracy (trueness and precision) - Part 2. Determine the standard measurement method to repeat
Of the basic methods of reproduction (GB/T 6379.2-2004, ISO 5725-2.1994, IDT)
GB/T 6682 analytical laboratory use specifications and test methods (GB/T 6682-2008, ISO 3696. 1987, MOD)
Principle 3
Royal jelly and royal jelly lyophilized lincomycin, erythromycin, tilmicosin, tylosin, spiramycin, clindamycin, amphotericin and guitar
Josamycin residue was extracted with Tris extract, the extract was OasisHLB SPE column 1) purification, methanol eluate was concentrated set
After the capacity for liquid chromatography - tandem mass spectrometry. External standard.
1) OasisHLB solid phase extraction columns are Waters company's product trade name, this information is given for the convenience of users of this standard, not the table
Endorsement of the product shown. If other equivalent product has the same effect, you can use these equivalent products.
4 Reagents and materials
Unless otherwise indicated, the reagents used were of analytical grade.
4.1 Water. GB/T 6682, level.
4.2 Methanol. chromatographically pure.
4.3 ammonium acetate.
4.4 acetonitrile. chromatography.
4.5 hydrochloric acid.
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