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Plastics -- Determination of the viscosity of polymers in dilute solution using capillary viscometers -- Part 5: Thermoplastic polyester (TP) homopolymers and copolymers
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GB/T 1632.5-2008
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Basic data Standard ID | GB/T 1632.5-2008 (GB/T1632.5-2008) | Description (Translated English) | Plastics -- Determination of the viscosity of polymers in dilute solution using capillary viscometers -- Part 5: Thermoplastic polyester (TP) homopolymers and copolymers | Sector / Industry | National Standard (Recommended) | Classification of Chinese Standard | G31 | Classification of International Standard | 83.080.10 | Word Count Estimation | 14,165 | Date of Issue | 2008-08-14 | Date of Implementation | 2009-04-01 | Quoted Standard | GB/T 1632.1-2008; GB/T 6379.2-2004; GB/T 8170-1987; GB/T 9345.2-2008; ISO 3105: 1994; ISO 7792-1: 1997 | Adopted Standard | ISO 1628-5-1998, MOD | Regulation (derived from) | National Standard Approval Announcement 2008 No.14 (Total No.127) | Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China | Summary | This standard specifies the determination of solvents in certain thermoplastic polyester (TP) dilute solution viscosity number (using a " reduced viscosity " means) of. This section applies to polyethylene terephthalate (PET), polyethylene terephthalate, polybutylene terephthalate (PBT), polyethylene terephthalate cyclohexene two methylene ester (PCT) and poly tea ethylene naphthalate (PEN), and other polyesters and polyester copolymers specified in ISO 7792-1: 1997, they can be dissolved in a predetermined condition specified in a particular solvent. |
GB/T 1632.5-2008: Plastics -- Determination of the viscosity of polymers in dilute solution using capillary viscometers -- Part 5: Thermoplastic polyester (TP) homopolymers and copolymers ---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
. Plastics Determination of the viscosity of polymers in dilute solution using capillary viscometers Part 5. Thermoplastic polyester (TP) homopolymers and copolymers
ICS 83.080.10
G31
National Standards of People's Republic of China
Plastic polymer using a capillary viscometer.
Dilute solution viscosity
Part 5. homopolymer and copolymer thermoplastic polyester (TP)
(ISO 1628-5.1998, MOD)
Posted 2008-08-24
2009-04-01 implementation
Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China
Standardization Administration of China released
Foreword
GB/T 1632 "plastic using a capillary viscometer polymer dilute solution viscosity" is divided into the following parts.
--- Part 1. General
--- Part 2. PVC resin
--- Part 3. polyethylene and polypropylene
--- Part 4. polycarbonate molding and extrusion materials
--- Part 5. homopolymer and copolymer thermoplastic polyester (TP)
--- Part 6. methyl methacrylate polymer
This section GB/T 1632 Part 5.
The partial modification of the use of ISO 1628-5. Part 5 "plastic --- using a capillary viscometer dilute polymer solution viscosity --- 1998
Score. homopolymer and copolymer thermoplastic polyester (TP) "(in English).
This section according to ISO 1628-5.1998 redrafted. This section lists the reg number and ISO 1628-5 in Appendix A.1998
Reg number control list. In Appendix B gives a list of these technical differences and the reasons for the reference.
Appendix C of this section is normative appendix, Appendix A, Appendix B, Appendix D is an informative annex.
This part is proposed by the China Petroleum and Chemical Corporation.
This part of the National Standardization Technical Committee plastic plastic resins and petrochemical products Club (SAC/TC15/SC1) centralized.
This section drafted by. China Petrochemical Research Institute of Beijing Yanshan Company.
The main drafters of this section. first Chao, Huang Ling, Wang Yan, the Wang Xuhui, Jiang Tao, Cai Chunfei.
This section first release.
Plastic polymer using a capillary viscometer.
Dilute solution viscosity
Part 5. homopolymer and copolymer thermoplastic polyester (TP)
1 Scope
This section specifies the determination method in certain solvents Thermoplastic polyester (TP) dilute solution viscosity number (also with the "inherent viscosity" shown).
This section applies to polyethylene terephthalate (PET), polyethylene terephthalate, polybutylene terephthalate (PBT), polyethylene terephthalate cyclohexene
Dimethylene ester (PCT), and polyethylene terephthalate polyethylene naphthalate (PEN), and ISO 7792-1.1997 and other polyester copolymers specified
He polyesters, which under specified conditions can be dissolved in a solvent of a particular provision.
Determination of the viscosity of the general method according to GB/T 1632.1-2008 prescribed determination, and in accordance with the test conditions specified in this part.
Determination of the number of sticky thermoplastic polyester provides a method for measuring the molecular weight of the polymer.
2 Normative references
The following documents contain provisions which, through reference in this text, constitute provisions of this part. For dated references, subsequent
Amendments (not including errata content) or revisions do not apply to this section, however, encourage the parties to this part of the research agreement
Whether the latest versions of these documents. For undated reference documents, the latest versions apply to this section.
GB/T 1632.1-2008 plastic using a capillary viscometer dilute polymer solution viscosity - Part 1. General
(ISO 1628-1.1998, IDT)
(Trueness and precision) - Part 2 Accuracy GB/T 6379.2-2004 measurement methods and results. the standard measurement to determine the party
Method repeatability and reproducibility of the basic method
GB/T 8170-1987 numerical rounding rules
9345.2-2008 Plastics - Determination of ash GB/T Part 2. polyethylene terephthalate, alkylene esters (ISO 3451-2.1998,
IDT)
ISO 3105.1994 glass capillary viscometer motion specifications and procedures
ISO 7792-1.1997 Plastics - Thermoplastic polyester (TP) molding and extrusion materials - Part 1. Designation system and basis
Principle 3
Measured according to conventional methods 25 ℃ solvent flow time and at a concentration of 0.005g/mL of the sample solution, based on the measured efflux time
And a known concentration of the solution viscosity of the calculation. In this method, the density difference and kinetic energy correction value is very small, will not be considered.
4 Solvent
Unless otherwise indicated in the analysis using only recognized as analytical reagents, reagent should be placed in a stoppered brown glass bottles stored in the dark.
Warning --- solvents used are toxic. Avoid skin contact and inhalation of its vapor.
The kind of solvent 4.1
Unsaturated polyester and the number of sticky solvent used relevant provisions of this part of the six different solvents.
Every day at least once measure the efflux time of the solvent (see 8.3). If the flow time of the solvent exceeds the initial preparation of the initial value
1%, the preparation should be discarded and a new solvent.
4.1.1 phenol/1,2-dichlorobenzene
Weigh 1 part by mass of phenol and dissolved in 1 part by mass of 1,2-dichlorobenzene. Weighing accurate to at least 1%.
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