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US$159.00 · In stock Delivery: <= 2 days. True-PDF full-copy in English will be manually translated and delivered via email. GB 28652-2012: [GB/T 28652-2012] High quality anhydrous potassium fluoride Status: Valid
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[GB/T 28652-2012] High quality anhydrous potassium fluoride
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GB 28652-2012
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Basic data | Standard ID | GB 28652-2012 (GB28652-2012) | | Description (Translated English) | [GB/T 28652-2012] High quality anhydrous potassium fluoride | | Sector / Industry | National Standard | | Classification of Chinese Standard | G12 | | Classification of International Standard | 71.060.50 | | Word Count Estimation | 6,644 | | Quoted Standard | GB 190-2009; GB/T 191-2008; GB/T 6678; GB/T 8170; GB/T 27813-2011 | | Regulation (derived from) | National Standards Bulletin No. 24 of 2012 | | Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China | | Summary | This Chinese standard provides high-quality potassium fluoride water requirements, test methods, inspection rules, marking, labeling, packaging, transportation, storage, and security. This standard applies primarily as a glass sculpture agent, electroplat |
GB 28652-2012: [GB/T 28652-2012] High quality anhydrous potassium fluoride---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
High quality anhydrous potassium fluoride
ICS 71.060.50
G12
National Standards of People's Republic of China
High quality anhydrous potassium fluoride
Published 2012-09-03
2013-06-01 implementation
Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China
Standardization Administration of China issued
Foreword
This standard Chapter 7 and Chapter 8 and Chapter 9 8.1,8.3,8.4 content is mandatory, the rest are recommended.
This standard was drafted in accordance with rules GB/T 1.1-2009 given.
The standard proposed by China Petroleum and Chemical Industry Federation.
This standard by the National Standardization Technical Committee chemical inorganic chemicals branch (SAC/TC63/SC1).
This standard was drafted. CNOOC Tianjin Chemical Research & Design Institute, Xinxiang Yellow River Fine Chemical Co., Ltd., Zhejiang Chemical Research Institute
Ltd., Shandong-fluoro New Materials Co., Ltd., Zhejiang fluorescent Chemical Co., Ltd. of Xinxiang City Shengwei biological, chemical stocks Fluoride
Limited copies.
The main drafters. Zhao Meijing, Liu Zhong Shan, Wang Song, Fang Road, Zhou Pengpeng, Guo Liming, Cheng Ye, Xue Xu Jin.
High quality anhydrous potassium fluoride
1 Scope
The standard provides high-quality requirements of anhydrous potassium fluoride, test methods, inspection rules, marking, labeling, packaging, transportation, storage, and security.
This standard applies primarily as glass engraving agent, electroplating auxiliaries, welding flux, pesticides, organic fluorinating agent, the catalyst,
Anhydrous potassium fluoride high quality absorbent (moisture absorption) and the like.
2 Normative references
The following documents for the application of this document is essential. For dated references, only applies to the version dated paper
Pieces. For undated references, the latest edition (including any amendments) applies to this document.
GB 190-2009 dangerous goods packaging logo
GB/T 191-2008 Packaging Pictorial signs
GB/T 6678 General Principles for Sampling Chemical Products
GB/T 8170 rounding off means about rules and determining limiting values
GB/T 27813-2011 anhydrous potassium fluoride Analysis
Molecular formula and molecular weight 3
Molecular formula. KF
Molecular weight. 58.10 (according to 2007 international relative atomic mass)
4 Requirements
4.1 Appearance. white crystal or spherical particles.
4.2 Test Method for detecting high-quality indicators of anhydrous potassium fluoride required by this standard shall comply with the technical requirements of Table 1.
Table 1 Technical Requirements
project
index
First grade Qualified
Potassium fluoride (KF) w /% ≥ 99.5 99.3
Chloride (based on Cl) w /% ≤ 0.05 0.05
Loss on ignition w /% ≤ 0.2 0.2
The free acid or free base
(In terms of HF) w /% ≤ 0.05 0.05
(As KOH) w /% ≤ 0.05 0.1
Sulfate (in terms of SO4) w /% ≤ 0.1 0.2
Fluoro-silicate (as SiO2) w /% ≤ 0.01 0.01
TABLE 1 (cont.)
project
index
First grade Qualified
Arsenic (As) w /% ≤ 0.0005 0.0005
Iron (Fe) w /% ≤ 0.0005 0.002
Lead (Pb) w /% ≤ 0.0005 0.001
Chromium (Cr) w /% ≤ 0.0005 0.0005
Silicon (Si) w /% ≤ 0.002 0.005
Boron (B) w /% ≤ 0.0005 0.001
Calcium (Ca) w /% ≤ 0.0005 0.001
Nickel (Ni) w /% ≤ 0.0003 0.0005
5 Test methods
5.1 Visual inspection
In natural light, the appearance was visually determined in a white plastic plate.
5.2 Determination of potassium fluoride content
The results were measured and calculated according to a predetermined GB/T 27813-2011 Chapter 5.
5.3 Determination of chloride content
The results were measured and calculated as specified in Chapter 6 GB/T 27813-2011.
5.4 Determination of loss on ignition
The results were measured and calculated as specified in Chapter 7 GB/T 27813-2011.
5.5 Determination of free acid or free base content
The results were measured and calculated according to the provisions of Chapter 8 GB/T 27813-2011.
5.6 Determination of the sulfate content
The results were measured and calculated according to a predetermined GB/T 27813-2011 Chapter 9.
5.7 Determination of the content of fluorosilicate
The results were measured and calculated according to a predetermined GB/T 27813-2011 chapter 10.
5.8 Determination of arsenic content, iron content, lead content, the chromium content, silicon content, boron content, calcium content and nickel content
The results were measured and calculated according to the provisions of Chapter 12 GB/T 27813-2011.
6 Inspection Rules
All items specified index of 6.1 as standard factory inspection items should be tested batches.
6.2 with the same level of the same material, substantially same production conditions, the same team or continuous production of high-quality production of anhydrous potassium fluoride
Batch. Each batch of products is not more than 30t.
Unit 6.3 determines the number of samples required to GB/T 6678's. When sampling, the sampler pouch obliquely from above to the insertion depth of material
3/4 of the sampling. The collected samples were placed in a sealed plastic container and mix by quartering reduced to less than 500g, dispensed into two clear
Clean, dry plastic bottle (or plastic bags), the sealing. Bottle or bag sticker stating. manufacturer name, product name, grade, batch number, sampling
Date and sample's name. As a laboratory sample, and a second copy for future reference, the retention time by the manufacturer according to the actual needs.
6.4 If the test results do not meet the requirements of this standard index, since twice the amount should be re-packaging samples reinspection, the reinspection results i.e.
So that only an indicator does not meet the requirements of this standard, then the entire batch of product is substandard.
Rounding value comparison method using 6.5 GB/T 8170 test results determines whether a predetermined standard.
7 signs and labels
7.1 high-quality solid anhydrous potassium fluoride should be clearly marked packaging, including. the production name and address, product name, grade, having a net
Quantity, batch or production date, and the standard number "toxic substances" in the labeling GB 190-2009, GB/T in a predetermined 191-2008
The "fear of the sun", "afraid of the rain" logo.
7.2 each batch of high quality anhydrous potassium fluoride should be accompanied by a certificate of quality. Include. manufacturer's name and address, product name, grade,
Net content, lot number or production date, the standard number.
8 packaging, transport and storage
Anhydrous potassium fluoride 8.1 high quality packaging in three ways.
8.1.1 woven Packing. a single layer of polyethylene plastic film packaging bags, using heat sealing. Packaging plastic bags with dimensions
Nylon thread or other line of comparable quality sewn securely.
8.1.2 cardboard drum. the packaging with double polyethylene plastic film bag, an inner layer and an outer plastic film bag, respectively dimensional plastic film bag
Nylon thread or other solid mass equivalent Zhakou line. Using cardboard packaging, firmly capped and ferrule.
8.1.3 foil bag. aluminum foil bags, heat sealing.
8.2 high-quality packaging of anhydrous potassium fluoride net content. net weight woven bag bag 20kg. Net weight 20kg cardboard drum barrel
Or 75kg. Aluminum foil bag net weight 20kg. Net content or negotiated package according to user requirements.
8.3 high quality anhydrous potassium fluoride during transport should be covered to prevent rain and moisture.
8.4 high quality anhydrous potassium fluoride should be kept cool and dry place, to prevent rain, moisture.
9 Security
9.1 having a high quality over anhydrous potassium fluoride toxic, workplace and rest areas should be strictly separated; operators and analysts sampling should
Wear labor protection.
After 9.2 high quality anhydrous potassium fluoride in contact with the eye or skin, rinse immediately with plenty of water at least 15min; serious immediate medical attention.
9.3 high quality anhydrous potassium fluoride Accidental. isolation leakage, to prevent contact with the acid, restricted access. Spills should be collected immediately
Into the fixed container, according to environmental requirements focus. Contaminated ground water flush, the flushing water should enter the sewage treatment system, not
Directly into the sewer.
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