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GB 20952-2020 English PDF (GB 20952-2007)

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GB 20952-2020English759 Add to Cart 6 days [Need to translate] Emission Standard of Air Pollutants for Gasoline Filling Stations Valid GB 20952-2020
GB 20952-2007English360 Add to Cart 0--9 seconds. Auto-delivery Emission standard of air pollutant for gasoline filling stations Obsolete GB 20952-2007


BASIC DATA
Standard ID GB 20952-2020 (GB20952-2020)
Description (Translated English) Emission Standard of Air Pollutants for Gasoline Filling Stations
Sector / Industry National Standard
Word Count Estimation 41,467
Date of Issue 2020-12-28
Date of Implementation 2021-04-01
Older Standard (superseded by this standard) GB 20952-2007
Drafting Organization Chinese Academy of Environmental Sciences
Administrative Organization Ministry of Ecology and Environment
Regulation (derived from) Ministry of Ecology and Environment Announcement No. 74 (2020)

BASIC DATA
Standard ID GB 20952-2007 (GB20952-2007)
Description (Translated English) Emission standard of air pollutant for gasoline filling stations
Sector / Industry National Standard
Classification of Chinese Standard Z60
Classification of International Standard 13.040.40
Word Count Estimation 29,238
Date of Issue 2007-06-22
Date of Implementation 2007-08-01
Quoted Standard GB 50156; GB/T 16157; HJ/T 38
Drafting Organization Beijing Academy of Environmental Sciences
Administrative Organization State Environmental Protection Administration of Science, Technology
Regulation (derived from) GB Notice 2007 No. 6 (Total No. 106)(GB Commission)
Summary This Chinese standard specifies the petrol stations gas emission limits, control technology requirements and test methods. This standard applies to existing petrol stations gas emissions management, as well as new construction, renovation, expansion gas station project's environmental impact assessment, design, and after the completion of final acceptance of gasoline hydrocarbon emissions management.


GB 20952-2020 (Emission Standard of Air Pollutants for Gas Stations) Emission standard of air pollutants for gas stations Emission standard of air pollutant for gasoline filling stations ICS 13.040.40 Z 60 National Standards of People's Republic of China Replace GB 20952-2007 2020-12-28 release 2021-04-01 implementation Ministry of Ecology and Environment State Administration for Market Regulation release Table of contents Foreword...II 1 Scope of application...1 2 Normative references...1 3 Terms and definitions...1 4 Oil and gas emission control requirements...4 5 Emission limits...5 6 Air pollutant monitoring...7 7 Implementation and supervision...7 Appendix A (Normative Appendix) Liquid Resistance Detection Method...9 Appendix B (Normative Appendix) Airtightness Testing Method...12 Appendix C (Normative Appendix) Gas-liquid ratio detection method...15 Appendix D (Normative Appendix) Testing Methods of Oil and Gas Treatment Equipment...21 Appendix E (Informative Appendix) Technical Requirements for Online Monitoring System...22 Appendix F (informative appendix) on-line monitoring system accuracy check method...28 Appendix G (Informative Appendix) Gas Station Inspection Report...29 Emission standard of air pollutants for gas stations 1 Scope of application This standard specifies the requirements for the control and monitoring of oil and gas emissions during the unloading, storage and refueling of gasoline (including alcohol-containing gasoline) at gas stations. Test and supervise management requirements. This standard is applicable to the management of oil and gas emissions from gasoline (including alcohol-containing gasoline) at existing gas stations, as well as new, rebuilt, and expanded gas stations Environmental impact assessment, design, completion acceptance of the project, the issuance of pollution discharge permits and the management of oil and gas emissions after completion. After the implementation of the new emission standard, if the content stipulated in the existing enterprise’s emission permit is inconsistent with the new standard, it shall be stipulated in the new standard. Change the pollution discharge permit before the effective time limit. 2 Normative references This standard quotes the following documents or their clauses. For dated reference documents, only the dated version applies to this standard quasi. For undated references, the latest version (including all amendments) applies to this standard. GB 16297 Comprehensive Emission Standard of Air Pollutants GB 18352.6 Light-duty vehicle pollutant emission limits and measurement methods (China Phase 6) GB 50156 Code for Design and Construction of Automobile Refueling Station GB/T 16157 Determination of particulate matter in exhaust from stationary sources and sampling method for gaseous pollutants HJ 38 Determination of total hydrocarbons, methane and non-methane total hydrocarbons in stationary pollution sources gas chromatography HJ/T 55 Technical Guidelines for Monitoring Unorganized Emissions of Air Pollutants HJ 212 Pollutant online monitoring (monitoring) system data transmission standard HJ/T 373 Fixed pollution source monitoring quality assurance and quality control technical specifications (trial implementation) HJ/T 397 Fixed source exhaust gas monitoring technical specification HJ 604 Determination of Ambient Air Total Hydrocarbons, Methane and Non-Methane Total Hydrocarbons Direct Sampling-Gas Chromatography HJ 733 Leakage and open liquid level emission of volatile organic compounds detection technology guide HJ 819 General Rules of Technical Guidelines for Self-monitoring of Pollutant Discharge Units HJ 1118 Pollutant Discharge Permit Application and Issuing Technical Specifications for Oil Storage Depots and Gas Stations "Environmental Monitoring Management Measures" (State Environmental Protection Administration Order No. 39) "Measures for the Disclosure of Environmental Information of Enterprises and Institutions" (Order No. 31 of the Ministry of Environmental Protection) 3 Terms and definitions The following terms and definitions apply to this standard. 3.1 Gasoline filling station The new construction, reconstruction and expansion of oil and gas recovery facilities of the station shall be implemented in accordance with the requirements of newly-built enterprises. 4 Oil and gas emission control requirements 4.1 Basic requirements 4.1.1 The oil and gas discharged during unloading, storage and refueling at gas stations shall be controlled by means of oil and gas recovery based on closed collection. 4.1.2 Gas stations shall establish technical files such as oil and gas recovery construction drawings, oil and gas recovery system testing and verification, system parameter settings, etc. Gas station oil and gas recovery system management, operating procedures, regular inspection, maintenance, repair and record keeping. 4.1.3 Gas stations shall design, construct, and maintain sampling ports or sampling test flats in accordance with the requirements of environmental monitoring management regulations and technical specifications. station. 4.1.4 The oil and gas recovery system, oil and gas processing device, and online monitoring system shall adopt standardized connections. 4.1.5 During the design and construction of oil and gas recovery including the control of oil and gas emissions from refueling, the online monitoring system, oil and gas treatment Equipment pipelines such as equipment are buried in advance. 4.2 Unloading oil and gas emission control 4.2.1 The submerged oil unloading method shall be adopted, and the height of the oil outlet of the unloading pipe from the bottom of the tank shall be less than.200 mm. 4.2.2 The oil unloading and vapor recovery interface should be installed with a shutoff valve (or sealed quick coupling) and cap with a nominal diameter of 100 mm. Some gas stations have taken unloading oil and gas emission control measures, but the interface size does not match, the variable diameter connection can be adopted. 4.2.3 The connecting hose shall be connected to the unloading truck with a sealed quick connector with a nominal diameter of 100 mm. 4.2.4 All oil and gas pipeline discharge ports should be equipped with pressure/vacuum valves according to the requirements of GB 50156.If there are valves, the valves should be kept open Status; gasoline discharge pipe without pressure/vacuum valve should be kept normally closed. 4.2.5 The underground pipeline connecting the exhaust pipe should slope towards the oil tank, the slope should not be less than 1%, and the nominal diameter of the pipeline should not be less than 50 mm. 4.2.6 When unloading oil, ensure that the unloading oil vapor recovery system is airtight. Before unloading the oil, the unloading hose and the vapor recovery hose should be connected with the oil transport vehicle tank The vehicle and the buried oil tank are tightly connected, and then the oil and gas recovery pipeline valve is opened, and then the oil unloading pipeline valve is opened for oil unloading operation. 4.2.7 After unloading the oil, close the valves related to the unloading hose and the vapor recovery hose, and then disconnect the unloading hose and the vapor recovery hose. 4.3 Control of oil and gas emissions from storage 4.3.1 All components that affect the tightness of oil and gas storage, including oil and gas pipelines and connected flanges, valves, quick connectors, and other related components The related components should be kept tightly closed under normal working conditions, and the concentration of oil and gas leakage meets the requirements of the closed point limit of the oil and gas recovery system of this standard. 4.3.2 When infrared cameras are used to detect the airtight points of the oil and gas recovery system, there should be no oil and gas leakage. 4.3.3 Buried oil tanks should use electronic level gauges for gasoline tightness measurement. 4.3.4 Oil spill control measures that meet the relevant regulations of GB 50156 shall be adopted. 4.4 Refueling oil and gas emission control 4.4.1 The oil and gas generated by refueling shall be collected in a closed manner with vacuum assist. 4.4.2 The oil and gas recovery pipeline should be sloped towards the oil tank, and the slope should not be less than 1%. The liquid collection can be set if it cannot meet the slope requirements due to the terrain limitation The condensate in the collector and the liquid collector should be sealed and recovered to a low-grade gasoline tank. 4.4.3 The fueling hose should be equipped with a pull-off stop valve to prevent oil spilling and dripping when fueling. 4.4.4 When the light vehicles using ORVR in the jurisdiction reach 20% of the vehicle population, the oil and gas recovery system and online monitoring system should Appendix A (Normative appendix) Liquid resistance detection method A.1 Scope of application This appendix is applicable to the detection of the liquid resistance of the underground oil and gas recovery pipeline from the tanker to the buried oil tank, and it is applicable to the ground from each tanker to the buried tank. Lower the oil and gas recovery pipeline for liquid resistance detection. Special attention. The safety production regulations of gas stations should be strictly followed during testing. A.2 Detection principle and overview A.2.1 Fill the oil and gas recovery pipeline with nitrogen at the specified nitrogen flow rate to simulate the oil and gas passing through the oil and gas recovery pipeline. A.2.2 Use a pressure gauge or equivalent device to detect the liquid resistance of the gas passing through the pipeline, and understand the resistance to the gas due to various reasons in the pipeline The degree is used to judge whether it affects the oil and gas recovery. A.3 Deviation and interference A.3.1 Any leaks in related oil and gas pipelines will result in lower liquid resistance measurements. A.3.2 If you wait for the nitrogen flow to stabilize for less than 30s before starting the test, an incorrect liquid resistance measurement value will be generated. A.4 Testing equipment A.4.1 Nitrogen and nitrogen cylinders. Use commercial grade nitrogen, a high-pressure nitrogen cylinder with a two-stage pressure regulator and a 6.9kPa pressure relief valve. A.4.2 Pressure gauge. Use the pressure gauges described in A.5.1, A.5.2 and A.5.3. A.4.3 Flowmeter. Use the flowmeter described in A.5.4 and assemble it with the pressure gauge to form a liquid resistance detection device (see Figure A.1). A.4.4 Stopwatch. Use the stopwatch described in A.5.5. A.4.5 Three-way detection connector. Equipment reserved for testing on the refueling vapor recovery standpipe (see Figure A.2). A.4.6 Hose. It is used to connect the nitrogen outlet of the liquid resistance detection device to the three-way detection joint, and fill the gas recovery pipeline with nitrogen through a hose. A.4.7 Grounding device. Equipment and installation methods should comply with relevant regulations. The minimum scale is 5 Pa. A.5.3 The full scale range of the electronic pressure measuring device (0~2.5) kPa, the maximum allowable error is 0.5% of the full scale; the full scale range (0~2.5) 5.0) kPa, the maximum allowable error is 0.25% of full scale. A.5.4 The range of the flow meter is (0~100) L/min, the maximum allowable error is 2% of the full range, and the minimum scale is 2L/min. A.5.5 The maximum allowable error of the stopwatch is within 0.2s. A.5.6 All measuring instruments should be calibrated in accordance with measurement standards. A.6 Testing procedures A.6.1 Open the bottom basin of the inspected fuel dispenser and find the tee and inspection joints reserved on the refueling vapor recovery standpipe. A.6.2 Connect the liquid resistance detection device with the three-way detection joint through a hose. A.6.3 Ground the nitrogen cylinder and connect the nitrogen pipe to the nitrogen inlet connector of the liquid resistance detection device. A.6.4 Open the oil and gas interface valve of the unloading oil and gas recovery system of the corresponding oil tank. A.6.5 Open the nitrogen cylinder and set the pressure of the low pressure regulator to 35 kPa. Use the flow meter control valve to adjust the nitrogen flow rate, the lowest from Table 1 The nitrogen flow starts, and the liquid resistances corresponding to the 3 flows are detected respectively. Before reading the pressure gauge value, the time for the nitrogen flow to stabilize should be longer than 30s. A.6.6 If any of the 3 liquid resistance test values is greater than the maximum pressure limit specified in Table 1, the gas station liquid resistance test fails. If the test value cannot be determined due to the jitter of the pressure gauge pointer, the fluid resistance test is deemed to be unqualified. A.6.7 Remove the hose connected to the three-way detection joint and restore the original connection of the oil and gas recovery pipeline. A.6.8 Close the oil and gas interface valve of the corresponding oil tank. A.7 Inspection records Refer to Table G.1 in Appendix G for the record of liquid resistance test results of oil and gas recovery pipelines. Appendix B (Normative appendix) Tightness detection method B.1 Scope of application This appendix is applicable to the airtightness testing of gas station oil and gas recovery systems. Special attention. The safety production regulations of gas stations should be strictly followed during testing. B.2 Detection principle and overview B.2.1 Use nitrogen to pressurize the oil and gas recovery system to 500 Pa, allowing the system pressure to decay. The residual pressure value after detecting 5min is in accordance with Table 2 Set the minimum residual pressure limit for comparison. If it is lower than the limit, it indicates that the system leakage is beyond the allowable range. B.2.2 For new, renovated, or expanded gas stations, the inspection should be carried out after the oil and gas recovery system is installed and meets the requirements for use. B.2.3 The inspection is carried out at the refueling vapor recovery standpipe. B.2.4 For non-connected buried oil tanks, each buried oil tank shall be tested for tightness. B.3 Deviation and interference B.3.1 Only gaseous nitrogen can be used for detection. The nitrogen flow rate charged into the system exceeds 100L/min, which will cause deviation of the test results. B.3.2 If an oil and gas treatment device is connected to the oil and gas recovery system, the power supply of the collection unit and the oil and gas treatment device should be turned off during testing. B.3.3 If the electronic pressure gauge has thermal deviation, there should be at least a 15min warm-up process, and then a 5min drift check should be done. in case If the drift exceeds 2.5Pa, this instrument cannot be used. B.4 Testing equipment B.4.1 Nitrogen and nitrogen cylinders. Same as A.4.1. B.4.2 Pressure gauge. Use the pressure gauges described in B.5.1 and B.5.2. B.4.3 Flowmeter. Same as A.4.3, assembled together with the pressure gauge to form a tightness testing device (see Figure A.1). B.4.4 Stopwatch. Same as A.4.4. B.4.5 Three-way detection connector. Same as A.4.5. B.4.6 Hose. Same as A.4.6. B.4.7 Grounding device. Same as A.4.7. B.4.8 Leak detection solution. Any solution that can be used to detect gas leakage is used to test the tightness of system components. B.5 Sensitivity, range and accuracy B.5.1 The minimum diameter of the dial of the mechanical pressure gauge is 100 mm, the range (0~750) Pa, and the maximum allowable error is 2% of the full range. The minimum scale is 25Pa. B.5.2 The full scale range of the electronic pressure measuring device (0~2.5) kPa, the maximum allowable error is 0.5% of the full scale; the full scale range (0~2.5) 5.0) kPa, the maximum allowable error is 0.25% of full scale. B.5.3 The minimum oil and gas space of a single oil tank should be 3800L or 25% of the tank volume, whichever is less. The maximum joint of the connected oil tank The calculated oil and gas space should not exceed 95000L. The above does not include the volume of all oil and gas pipelines. B.5.4 The flow range of the nitrogen gas charged is (30-100) L/min. B.5.5 The flowmeter is the same as A.5.4. B.5.6 The stopwatch is the same as A.5.5. B.5.7 All measuring instruments should be calibrated in accordance with measurement standards. B.6 Pre-test procedures B.6.1 Safety warnings to be followed B.6.1.1 Only nitrogen is allowed to pressurize the system. B.6.1.2 The nitrogen cylinder used for testing should be equipped with a 6.9kPa pressure relief valve. B.6.1.3 The ground wire should be grounded during the process of filling nitrogen into the system. B.6.2 Preparation before testing B.6.2.1 Within 3 hours before the test or during the test, no large quantities of oil should enter or leave the oil storage tank. B.6.2.2 There shall be no refueling operation 30 minutes before and during the test. B.6.2.3 All fueling guns are correctly hung on the fueling machine. B.6.2.4 If a check valve is used on the oil and gas recovery pipeline or an oil and gas recovery pump is used so that the gas cannot be reversed in the system, it can be set Set up a short bypass line with a shut-off valve for tightness testing. B.6.2.5 Confirm that the oil level of the oil storage tank is higher than the bottom outlet of the submerged oil discharge pipe. B.6.2.6 All pressure measuring devices should be calibrated with standard pressure gauges or inclined pressure gauges before testing. Respectively for full scale 20%, 50% and 80% are calibrated, the accuracy should be within 2% of each calibration point, and the calibration frequency should not exceed 90 days. B.6.2.7 Any electronic pressure gauge should be preheated and drift checked before use (see B.3.3). B.6.3 Obtain the current oil storage capacity of each buried oil tank, and obtain the actual volume of each buried oil tank from the gas station records. Practical The current oil storage capacity is subtracted from the volume to calculate the oil and gas space of each buried oil tank. B.6.4 Use formula B.1 to calculate the approximate time required to pressurize the system to 500Pa. B.6.5 The inspection is carried out at the riser of the oil and gas recovery pipeline. Open the bottom basin of the inspected fuel dispenser and find the reserved tee and inspection joints. B.6.6 Connect the tightness test device with the nitrogen cylinder and the three-way test joint with a hose. Open the shut-off valve on the short-circuit pipeline. Read tank And the initial pressure of the underground pipeline, if the initial pressure is greater than 550Pa, first check according to the corresponding pressure drop limit in Table 2, such as If the pressure drop value meets the corresponding limit requirements, it is determined that the airtightness meets the standard; if the pressure drop value exceeds the corresponding limit value, the pressure is released Make the pressure of the oil tank and underground pipeline less than 550Pa before testing. B.7 Testing procedures B.7.1 Pressurize the oil and gas recovery system (or independent subsystem). Open the valve of the nitrogen cylinder and set the pressure of the low pressure regulator to 35kPa, Adjust the nitrogen flow rate in the range of (30~100) L/min and start the stopwatch. Fill it to about 550Pa, if it reaches 500Pa during the filling process If the required time exceeds 2 times the value calculated in formula B.1, the detection is stopped, indicating that the system does not have the detection conditions. B.7.2 When the pressure reaches about 550Pa, close the nitrogen valve, and adjust the pressure relief valve to turn on the stopwatch when the pressure drops to the initial pressure of 500Pa. B.7.3 Record the system pressure every 1 minute. After 5 minutes, record the final system pressure. B.7.4 Release the pressure of the gas recovery system according to the safety regulations of the gas station. B.7.5 Remove the hose connected to the three-way detection joint and restore the original connection of the oil and gas recovery pipeline. B.7.6 If the oil and gas recovery system consists of several independent oil and gas recovery subsystems, then each independent subsystem shall be tested for tightness. Appendix C (Normative appendix) Gas-liquid ratio detection method C.1 Scope of application This appendix applies to the gas-liquid ratio detection of the gas-liquid-gas recovery system of gas stations. Special attention. The safety production regulations of gas stations should be strictly followed during testing. C.2 Detection principle and overview Install a close-fitting adapter at the nozzle of the fuel gun. The adapter is connected to the gas flow meter, and the gas flow passes through the gas flow meter first. Then enter the vapor collection hole on the nozzle of the fuel gun. The ratio of the measured gas volume to the gasoline volume measured by the dispenser at the same time is called gas-liquid ratio. Through the detection of gas-liquid ratio, the recovery effect of the oil and gas recovery system can be understood. C.3 Deviation and interference C.3.1 If the nozzle of the fuel gun and the adapter cannot be matched well for various reasons, the test cannot be performed. C.3.2 If the fueling flow of the tested fueling gun cannot reach more than 20L/min, the test cannot be performed. C.3.3 If the detected fuel nozzle causes gasoline to enter the detection device, the gas-liquid ratio detection value of this fuel nozzle will be regarded as invalid. C.3.4 Before testing, do not empty the gasoline in the gas path of the refueling hose and the gas pipe of the dispenser, otherwise the test results will be biased. C.3.5 Before the gas-liquid ratio test, the O-ring of the gas-liquid ratio adapter should be lubricated correctly, otherwise the test result will be biased. C.4 Testing equipment C.4.1 Adapter. Use a gas-liquid ratio adapter that matches the fueling gun. The adapter should be able to isolate the gas-liquid collection hole of the fueling gun. It is connected to the gas flow meter through an oil-resistant hose, and the adapter installation is shown in Figure C.1. C.4.2 Gas flow meter. Use a positive displacement flow meter to measure the volume of the recovered gas. The installation of the gas flow meter is shown in Figure C.1. C.4.3 The gas flow meter inlet tee. The three-way pipe is used to connect the oil and gas loop pipe and the gas balance pipe (see Figure C.1). C.4.4 Liquid flow meter. Use the flow meter on the fuel dispenser to measure the volume of gasoline added during the test. C.4.5 Oil drums for testing. A portable container that meets fire safety and is used to contain the gasoline added during the test. The materials and use should be full Meet the fire safety requirements. The oil drums and supporting pipelines and components used for testing are shown in Figure C.2 and Figure C.3. C.4.6 Stopwatch. Same as A.4.4. C.4.7 Lubricants. Grease or spray-type lubricant to ensure the air-to-liquid ratio between the O-ring of the adapter and the nozzle of the nozzle. The maximum allowable error is ±2%, and the pressure drop when the gas flow is 7.5 L/min and 375 L/min is not more than 10 Pa and 175 Pa, respectively. C.5.2 The length of the hose connecting the adapter and the gas flow meter is in the range of 1000 to 1800 mm. C.5.3 The inner diameter of the inlet connecting pipe of the gas flow meter shall be at least 50 mm, and the length of the inlet pipe of the connecting pipe shall be in the range of 150-450 mm. C.5.4 The capacity of the oil drum for testing shall be at least 80 L. C.5.5 The stopwatch is the same as A.5.5. C.5.6 All measuring instruments should be calibrated in accordance with measurement standards. C.6 Pre-test procedures Before starting the following inspection procedures, check item by item according to the list of equipment for the oil and gas recovery system listed in the assessment report. The gas-liquid ratio test cannot be performed. C.6.1 Install the oil drum components and gas flowmeter for testing according to Figure C.3, and ensure that the grounding device is correctly connected. C.6.2 If there are other fueling guns sharing the same vacuum pump with the tested fueling gun, the gas-liquid ratio test should be performed when the other fueling guns are not sealed. Under the circumstances. For the vapor recovery system with "one pump with multiple guns (< 4 guns)", it should be tested when at least 2 fueling guns are being refueled at the same time; For the "one pump with multiple guns (≥4 guns)" oil and gas recovery s... ......


GB 20952-2007 NATIONAL STANDARD OF THE PEOPLE’S REPUBLIC OF CHINA ICS 13.040.40 Z 60 Emission standard of air pollutant for gasoline filling stations ISSUED ON: JUNE 22, 2007 IMPLEMENTED ON: AUGUST 01, 2007 Issued by: State Environmental Protection Administration; General Administration of Quality Supervision, Inspection and Quarantine. Table of Contents Foreword ... 4  1 Scope ... 5  2 Normative references ... 5  3 Terms and definitions ... 5  4 Gasoline vapor emission control and limit ... 7  5 Technical measures ... 11  6 Standard implementations ... 13  Annex A (normative) Testing methods for liquid resistance ... 15  Annex B (normative) Testing methods for vapor recovery system tightness .. 19  Annex C (normative) Testing methods for air to liquid volume ratio ... 24  Annex D (normative) Testing methods for vapor emission processing equipment ... 33  Annex E (informative) Calibration method for on-line monitoring system ... 36  Annex F (informative) Testing report of gasoline filling station ... 39  Emission standard of air pollutant for gasoline filling stations 1 Scope This Standard specifies gasoline vapor emission limits of gasoline filling stations, control technical requirements and testing methods. This Standard is applicable to gasoline vapor emission management of existing gasoline filling stations as well as environmental impact assessment, design, completion acceptance of new, modified and expanded gasoline filling station projects and gasoline vapor emission management after completion. 2 Normative references The provisions in the following documents become part of this Standard, through reference in this Standard. For undated documents, the latest version applies to this Standard. GB 50156, Code for design and construction of automobile gasoline and gas filling station GB/T 16157 The determination of particulates and sampling methods of gaseous pollutants emitted from exhaust gas of stationary source HJ/T 38 Stationary source emission - Determination of nonmethane hydrocarbons - Gas chromatography 3 Terms and definitions For the purposes of this document, the following terms and definitions apply. 3.1 gasoline filling station A special place for filling gasoline into car fuel tank. 3.2 gasoline vapor Volatile organic compounds (non-methane total hydrocarbons) generated during the filling, unloading and storage of gasoline at gasoline filling stations. 3.3 vapor emission concentration Under standard conditions (temperature is 273K, pressure is 101.3kPa), the mass of non-methane total hydrocarbons contained in every m3 of dry gas discharged, in g/m3. 3.4 vapor recovery system for gasoline filling station A vapor recovery system for gasoline filling station is composed of vapor recovery system for unloading, closed storage of gasoline, vapor recovery system for filling, online monitoring system, and vapor emission processing equipment. The role of this system is to TRANSFER the gasoline vapor generated during the unloading, storage and filling of the gasoline filling station, through closed collection, storage and sending into the tank of a tank car, and TRANSPORT to the oil storage depot for centralized recovery into gasoline. 3.5 vapor recovery system for unloading gasoline A system that collects the gasoline vapor generated when a tank car unloads gasoline, through a closed manner, into the tank of the tank car. 3.6 vapor recovery system for filling gasoline A system that collects the gasoline vapor generated when a tank car fills gasoline, through a closed manner, into the underground storage tank. 3.7 overfill protection measurement The overfill that might happen when controlling gasoline unloading by using shut-off valve or float valve or other anti-overflow measures. 3.8 underground storage tank A fully-buried storage tank under the ground. 3.9 pressure/vacuum valve Also known as P/V valve, vent valve, mechanical breathing valve, which can adjust the pressure difference between the inside and outside of the tank so that the gas inside and outside the tank can communicate. 3.10 dynamic back pressure The resistance when condensate liquid stays in the gasoline vapor pipeline or causes gas to pass through the pipeline for other reasons. 3.11 vapor recovery system tightness The sealing degree of vapor recovery system under certain gas pressure. 3.12 air to liquid volume ratio The ratio of the volume of gasoline vapor collected when filling to the volume of gasoline added to the tank at the same time. 3.13 vacuum-assist In the vapor recovery system for filling gasoline, use the vacuum generator to assistant recovering the gasoline vapor generated during gasoline filling. 3.14 on-line monitoring system The system that online monitors whether the air to liquid volume ratio in the vapor recovery process for filling gasoline as well as the vapor recovery system tightness of the vapor recovery system and pipeline liquid resistance are normal. When abnormality is found, it can remind the operator to take corresponding measures, and can record, store, process and transmit monitoring data. 3.15 vapor emission processing equipment The device that recovers the gasoline vapor discharged from the vapor recovery system for gasoline filling station, through methods such as attaching, absorption, condensation, membrane separation. 4 Gasoline vapor emission control and limit 4.1 The gasoline vapor emitted during unloading, storing and filling of gasoline filling station shall use the gasoline vapor recovery method based on closed collection to control. 4.2 Technical assessment 4.2.1 The vapor recovery system for filling gasoline shall conduct technical assessment and issue a report. The assessment mainly includes: investigating and analyzing technical information, verifying relevant certification documents, evaluating air to liquid volume ratio of multiple flows and guns, testing operations of at least 3 months in concession, providing rang of air to liquid volume ratio of which the control efficiency is greater than or equal to 90%, listing equipment of vapor recovery system. 4.2.2 The vapor emission processing equipment (hereinafter referred to as the processing equipment) and on-line monitoring system shall conduct technical assessment and issue a report. The assessment mainly includes: investigating and analyzing technical information, verifying relevant certification documents, providing proof of actual use in China or abroad, testing operations of at least 3 months in concession. 5 Technical measures 5.1 Emission control of gasoline vapor of unloading gasoline 5.1.1 It shall use submersible unloading method. The height of the gasoline outlet of the unloading pipe from the bottom of the tank shall be less than 200mm. 5.1.2 The gasoline unloading and oil recovery interface shall be installed with DN100mm shut-off valve, sealed quick connector and cap. For the exiting gasoline filling stations, if unloading emission control measures have been taken but the interface size does not match, it may use a reducing diameter one to connect. 5.1.3 The connecting hose shall be connected to the unloading truck with a DN100mm sealed quick connector. No residual oil can be left in the connecting hose after unloading. 5.1.4 All gasoline vapor pipeline emission ports shall be equipped with pressure/vacuum valves according to the requirements of GB 50156. 5.1.5 The underground pipeline connected to the exhaust pipe shall slope to the oil tank. The slope shall not be less than 1%. The pipeline diameter is not less than DN50mm. 5.1.6 For gasoline filling stations that have not taken technical measures for filling and storage of gasoline vapor recovery, when unloading, the gasoline measuring hole and other parts that may cause gas short circuit shall be sealed, so as to ensure that the gasoline vapor generated by unloading gasoline is sealed and replaced in the tank of tank car. 5.2 Gasoline vapor emission control of gasoline storage 5.2.1 All components that affect the tightness of gasoline vapor stored, including gasoline vapor pipelines and connected flanges, valves, quick couplings, and other related components shall be guaranteed to be free of air leakage when less than 750Pa. 5.2.2 The underground storage tank shall use electronic liquid level gauge to measure the tightness of gasoline. The electronic liquid level measurement system with leak detection function shall be selected. 5.2.3 It shall adopt overfill protection measurements that meet relevant requirements. 5.3 Emission control of vapor recovery for filling gasoline Annex A (normative) Testing methods for liquid resistance A.1 Application scope This appendix is applicable to the liquid resistance testing of the underground vapor recovery pipeline from the gasoline dispenser to underground storage tank. It shall test the liquid resistance of the underground vapor recovery pipeline from each gasoline dispenser to underground storage tank. Special attention: the regulations on safety production of gasoline filling stations shall be strictly implemented during testing. A.2 Testing principle and overview A.2.1 Fill the vapor recovery pipeline with nitrogen at the specified nitrogen flow. Simulate gasoline vapor through gasoline vapor recovery pipelines. A.2.2 Use a pressure gauge or equivalent device to detect the liquid resistance of the gas through the pipeline. Know the degree of resistance to gas in the pipeline due to various reasons and use to judge whether it shall affect the vapor recovery. A.3 Deviation and interference A.3.1 Any leaks in the relevant vapor pipelines shall result in low fluid resistance measurement. A.3.2 If it starts testing when nitrogen flow stabilizes less than 30s, it shall produce erroneous liquid resistance measurement. A.4 Testing equipment A.4.1 Nitrogen and nitrogen bottles. Uses commercial grade nitrogen, high- pressure nitrogen cylinder with two-level pressure regulator and a 6.9kPa relief valve. A.4.2 Pressure gauge. Use the pressure gauge described in A.5.1, A.5.2 and A.5.3. A.4.3 Float flowmeter. Use the float flowmeter described in A.5.4. It and the pressure gauge shall form the testing equipment for liquid resistance (see Figure A.1). A.6 Testing procedures A.6.1 Open the bottom pot of the gasoline dispenser being tested. Find the three-way and testing joints reserved on the vapor recovery riser pipe for filling gasoline. A.6.2 Connect the liquid resistance testing device to the three-way testing connector through a hose. A.6.3 Ground the nitrogen bottle. Connect the nitrogen pipe to the nitrogen inlet connector of the liquid resistance testing device. A.6.4 Open the vapor interface valve of vapor recovery system for unloading gasoline of corresponding tank. A.6.5 If testing new, modified and expanded gasoline filling stations, 10L gasoline shall be injected into the pipeline before soil coverage on vapor pipelines and ground hardening construction. A.6.6 Turn on the nitrogen bottle. Set the pressure of the low-pressure regulator to 35kPa. Use a float flow control valve to regulate the nitrogen flow. Starting with the lowest nitrogen flow in Table 1, respectively test the liquid resistance corresponding to 3 flows. Before reading the pressure gauge value, the nitrogen flow shall be stable for more than 30s. A.6.7 If any one of the three liquid-resistance tested values is greater than the maximum pressure limit specified in Table 1, the liquid resistance of the gasoline filling station shall be nonconforming. If the test value cannot be determined due to the jitter of the pressure gauge, the liquid resistance test is deemed nonconforming. A.6.8 Remove the hose connected to the three-way testing connector. Restore the connection of the original vapor recovery pipeline. A.6.9 Close the vapor interface valve of the corresponding tank. A.7 Testing record See Table F.1 in Annex F for liquid resistance testing result record of vapor recovery pipelines. which shall affect the vapor recovery system tightness testing of the entire system, it shall set up a short-circuit pipeline with a shut-off valve. B.4 Testing equipment B.4.1 Nitrogen and nitrogen bottle, same with A.4.1. B.4.2 Pressure gauge. Use the pressure gauge described in B.5.1 and B.5.2. B.4.3 Float flowmeter. Same with A.4.3. It and the pressure gauge shall form the testing device for vapor recovery system tightness (see Figure A.1). B.4.4 Stopwatch. Same with A.4.4. B.4.5 Three-way testing connector. Same with A.4.5. B.4.6 Hose. Same with A.4.6. B.4.7 Grounding device. Same with A.4.7. B.4.8 Leak detection solution. Any solution that can be used to detect gas leaks, used to inspect the vapor recovery system tightness of system components. B.5 Sensitivity, range and accuracy B.5.1 The minimum diameter of mechanical pressure gauge dial is 100mm. The measuring range is 0~750Pa. The accuracy is 2% of full measuring range. The minimum scale is 25Pa. B.5.2 When the full measuring range of electronic pressure measuring device is 0~2.5kPa, the accuracy is 0.5% of full measuring range. When the full measuring range is 0~5.0kPa, the accuracy is 0.25% of full measuring range. B.5.3 The minimum vapor space of a single oil tank shall be 3800L or 25% of the volume of the oil tank. Take the smaller value of the two. The maximum total vapor space to connect the oil tank shall not exceed 95000L. The above does not include the volume of all vapor pipelines. B.5.4 The flow rate of filled nitrogen is 30~100L/min. B.5.5 Float flowmeter is the same as A.5.4. B.5.6 Stopwatch same as A.5.5. B.5.7 All measuring instruments shall be calibrated according to measuring standards. B.6 Procedures before testing calibration point. The calibration frequency shall not exceed 90d. B.6.8 Use formula B.1 to calculate the time required to pressurize the system to 500Pa. B.6.9 Use a hose to connect the testing device of vapor recovery system tightness and the nitrogen bottle, three-way testing connector. Open the cut-off valve on the short circuit. Read the initial pressure of oil tank and underground pipeline. If the initial pressure is greater than 125Pa, release the pressure to make the pressure of the oil tank and underground pipeline less than 125Pa. B.6.10 Any electronic pressure gauge shall be preheated and drift checked before use (see B.3.4). B.7 Testing procedures B.7.1 Pressurize the vapor recovery system (or independent sub-system). Open the nitrogen cylinder valve. Set the pressure of the low-pressure regulator to 35kPa. Adjust the nitrogen flow rate in the range of 30~100L/min. Start the stopwatch. Pressurize to about 550Pa. During the pressurizing process, if the time required to reach 500Pa has exceeded 2 times the calculated value of formula B.1, then stop testing and indicate that the system does not have the testing conditions. B.7.2 Close the nitrogen valve when charging to about 550Pa. Adjust the pressure relief valve to reduce the pressure to 500Pa and start the stopwatch. B.7.3 Record the system pressure every 1min. After 5min, record the final system pressure. B.7.4 Release the pressure of the vapor recovery system according to the safety regulations of the gasoline filling station. B.7.5 Remove the hose connected to the three-way testing connector. Restore the connection of the original vapor recovery pipeline. B.7.6 If the vapor recovery system consists of several independent vapor recovery subsystems, then each independent subsystem shall be tested for vapor recovery system tightness. B.8 Procedures after testing Compare the system pressure testing value after 5min with the minimum residual pressure limit in Table 2 to determine if the gasoline filling station complies with the standard. If the actual vapor space value is between the two vapor space values listed in Table 2, then use the interpolation formula B.2 to calculate the minimum residual pressure limit. Annex C (normative) Testing methods for air to liquid volume ratio C.1 Application scope This appendix is applicable to the air to liquid volume ratio testing of vapor recovery system for gasoline filling station. Special attention: the regulations on safety production of gasoline filling stations shall be strictly implemented during testing. C.2 Testing principle and overview Install a tight adapter at the nozzle of the refueling gun. The adapter is connected to the gas flow meter. The air flow first passes through the gas flow meter, and then enters the vapor collection hole on the nozzle of the refueling gun. The ratio of the measured gas volume to the gasoline volume measured simultaneously by the gasoline dispenser is called the air to liquid volume ratio. Through the testing of the air to liquid volume ratio, the recovery effect of the vapor recovery system can be known. C.3 Deviations and interference C.3.1 If the nozzle of the refueling gun and the adapter cannot be matched well for various reasons, the test cannot be performed. C.3.2 If the filling flow rate of the tested refueling gun cannot reach more than 20L/min, the test cannot be performed. C.3.3 If other refueling guns that share a vacuum pump with the refueling gun being tested are sealed, the test results shall be deviated. C.3.4 If the tested refueling gun brings gasoline into the testing device, the air to liquid volume ratio test value of the refueling gun shall be considered invalid. C.3.5 Before testing, do not empty the gasoline in the gas line of the refueling hose and the vapor pipe of the refueling machine, otherwise the test results shall be deviated. C.3.6 Before the air to liquid volume ratio test, the O-ring of the air to liquid volume ratio adapter shall be properly lubricated, otherwise the test results shall be deviated. C.7.8 If the air to liquid volume ratio calculated according to formula C.1 is within the standard limits, the air to liquid volume ratio of the tested refueling gun is up to the standard. C.7.9 If the air to liquid volume ratio is not within the standard limits, and the difference between the air to liquid volume ratio detection value and the limit is less than or equal to 0.1, two more air to liquid volume ratio tests shall be performed. But do not make any adjustments to the filling pipeline or the vapor recovery pipeline. In order to ensure the accuracy of the measurement, the necessary adjustments to the gas-liquid ratio detection device are allowed, including the air to liquid volume ratio adapter and the refueling gun. If the air to liquid volume ratio testing device is adjusted, the previous test result of this gun shall be invalid. Take the arithmetic average of 3 test results. If the average value of the air to liquid volume ratio is within the given limits, the air to liquid volume ratio of the refueling gun is up to the standard. If the average value is outside the limit range, it means that the air to liquid volume ratio test of the refueling gun is not up to the standard. C.7.10 If the air to liquid volume ratio is not within the specified limit range, and the difference between the tested value of the air to liquid volume ratio and the limit value is greater than 0.1, the air to liquid volume ratio test of the tested refueling point does not meet the standard. C.7.11 In order to avoid the accumulation of gasoline, after each test, drain the condensed gasoline in the hose between the gas flowmeter and the oil barrel component for testing and the hose between the air to liquid volume ratio adapter and the gas flowmeter. C.8 Procedures after testing C.8.1 Remove the air to liquid volume ratio adapter from the refueling gun. C.8.2 Carefully pour the filled gasoline back to the corresponding gasoline storage tank Keep the testing barrel grounded before pouring gasoline. Without the consent of the owner of the gasoline filling station, do not mix different grades of gasoline in the oil barrel. If different grades of gasoline are mixed in the oil barrel, the mixed gasoline shall be poured back to the lower grade oil storage tank. C.8.3 Before finally determining whether the air to liquid volume ratio test meets the standard, perform a leak check on the adapter according to C.6.6. If the testing device fails the leak check, all data obtained during the air to liquid volume ratio test shall be invalid. C.8.4 Before transportation, carefully seal the inlet and outlet of the gas flowmeter to prevent foreign matter from entering the flowmeter. 1.1m high guardrail. The sampling hole is 1.2~1.3m above the platform. If the sampling position is less than 1.5m above ground level, the monitoring operation platform and guardrail may not be set. D.2.5 The installation of the sampling hole and operation platform shall be completed and accepted at the same time as the vapor recovery and treatment project. D.3 Testing method D.3.1 The testing of the emission concentration of the processing equipment shall be carried out during the period when the ambient temperature is not lower than 20°C and when the filling is relatively concentrated. D.3.2 Each processing equipment shall be tested. The sampling time of each processing equipment is not less than 30min. It can conduct continuous sampling or equal time interval sampling. The number of samples collected at equal intervals is not less than 3. D.3.3 Other sampling requirements shall be implemented according to GB/T 16157. D.3.4 The analysis method is implemented according to HJ/T 38. D.4 Testing equipment D.4.1 Sampling joint. There shall be a universal sampling joint connected to the outlet sampling hole of the processing equipment. The connection method of the sampling joint and the sampling hole can be designed according to different sampling methods. However, the length of the sampling tube placed in the sampling hole tube on the sampling joint shall not be less than 56mm. The distance that the sample enters the collector through the sampling tube and other components shall not exceed 300mm. The inner diameter of the sampling tube is 5mm. D.4.2 For sampling with a syringe, refer to the sampling joint below. The sampling joint is a flange cover. The size is consistent with the sampling hole flange. At the center position of the flange cover, seal and weld a section of sampling tube through the flange cover. The length of the sampling tube inserted into the sampling hole tube is 56mm. The length of the other side is 20mm, and the inner diameter of the sampling tube is 5mm. D.4.3 Sampling joint material. Sampling joint shall use copper, aluminum or other materials that do not generate sparks and static electricity. D.5 Testing record Refer to Table F.4 in Annex F for the record of vapor emission test results of Annex E (informative) Calibration method for on-line monitoring system E.1 Application scope This appendix is applicable to the calibration of the on-line monitoring system of vapor recovery system for gasoline filling station. E.2 Principle and overview of on-line monitoring system E.2.1 A gas flowmeter is connected in series on the vapor recovery pipeline in the gasoline dispenser. By measuring the recovered vapor volume and comparing with the volume of liquid gasoline corresponding to the vapor volume, monitor the air to liquid volume ratio during vapor recovery process. E.2.2 Install a pressure sensor on the vapor recovery pipeline in the connected vapor storage space. By measuring the change of pressure value, monitor the vapor recovery system tightness. E.2.3 The data collected by the flowmeter and pressure sensor is sent to the data processing system. When the vapor recovery system is in an abnormal working state, the monitoring system shall issue a warning. If no processing measures are taken within the warning period, the system shall alarm and take measures to stop filling gasoline. E.3 Pressure sensor calibration test procedures Step 1: Record the serial number of the gasoline dispenser and installed pressure sensor. Step 2: Remove the cap from the pressure sensor environmental reference port valve. Rotate the valve 90° to open it. Make the valve accessed with air. Step 3: Open the diagnostic mode menu on the front panel of the console. Enter the smart sensor calibration menu. Record the pressure value. Step 4: Observe whether the pressure value is within ± 50Pa. If the pressure valve is not within this range, leave the valve position as described in step 2. Replace the sensor according to the pressure sensor installation guide. Then repeat the test according to step 3 to meet the pressure range. Step 5: Cover the cap of the pressure sensor environmental reference port ......

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