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National Food Safety Standard -- Food Additives -- Vegetable oil extraction solvent (also known as hexane solvent)
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GB 1886.52-2015
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Basic data | Standard ID | GB 1886.52-2015 (GB1886.52-2015) | | Description (Translated English) | National Food Safety Standard -- Food Additives -- Vegetable oil extraction solvent (also known as hexane solvent) | | Sector / Industry | National Standard | | Classification of Chinese Standard | X40 | | Word Count Estimation | 5,599 | | Date of Issue | 2015-09-22 | | Date of Implementation | 2016-03-22 | | Regulation (derived from) | PRC National Health and Family Planning Commission 2015 No.8 | | Issuing agency(ies) | National Health and Family Planning Commission of the People's Republic of China |
GB 1886.52-2015: National Food Safety Standard -- Food Additives -- Vegetable oil extraction solvent (also known as hexane solvent) ---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
(National food safety standards for food additives vegetable oil extraction solvent (aka hexane solvent))
National Standards of People's Republic of China
National Food Safety Standard
Food additive vegetable oil extraction solvent
(Also known as hexane solvent)
Issued on. 2015-09-22
2016-03-22 implementation
People's Republic of China
National Health and Family Planning Commission released
National Food Safety Standard
Food additive vegetable oil extraction solvent
(Also known as hexane solvent)
1 Scope
This standard applies to straight-run distillate from petroleum refined and prepared food additive vegetable oil extraction solvent (aka hexane solvent), the
Products such as hexane, fat is mainly composed of hydrocarbons.
2 Technical Requirements
2.1 Sensory requirements
Sensory requirements shall comply with the requirements of Table 1.
Table 1 Sensory requirements
Project requires test methods
Color colorless
State transparent liquid without mechanical impurities
Take appropriate sample is placed in a clean, dry cuvette, under natural light, Views
Its color and state police
2.2 Physical indicators
Physical and chemical indicators should be consistent with the provisions of Table 2.
Table 2. Physical and chemical indicators
Item Index Test Method
Distillation Range (IBP to dry point)/℃ 61 ~ 76 GB/T 6536
Benzene, w /% ≤ 0.06 GB/T 17474
Evaporation residue/(mg/L) ≤ 10 GB/T 3209
Sulfur (S)/(mg/kg) ≤ 5.0 SH/T 0253
Lead (Pb)/(mg/kg) ≤ 1.0 GB 5009.12
PAHs experimentally Appendix A A.3
by pH test A.4 in Appendix A
Appendix A
Testing method
A.1 General Provisions
This standard reagents and water, did not indicate when the other requirements, refer to the three water analytical reagent and GB/T 6682 regulations. test
Test used in the standard solution, impurity standard solution, preparations and products, did not indicate when the other requirements, according to GB/T 601, GB/T 602,
GB/T 603 provisions prepared. Solution was used in the tests did not indicate what is formulated with solvent, it refers to an aqueous solution.
A.2 Identification Test
A.2.1 solubility
Insoluble in water, soluble in ether, ethanol and acetone.
A.2.2 Density
Density by GB/T 1884 and the provisions of GB/T 1885 progresses, density range (20 ℃) of 0.655g/cm3 ~ 0.680g/cm3.
A.3 Determination of Polycyclic Aromatic Hydrocarbons
A.3.1 Reagents and materials
A.3.1.1 dimethyl sulfoxide.
A.3.1.2 trimethyl pentane solution of naphthalene. 7.0mg/L.
A.3.2 Analysis step
Pipette 25.0mL sample is placed in a separatory funnel and 125mL, 25mL of hexane was added and mixed. Dimethyl sulfoxide was added 5.0mL, severe
Oscillation 1min, standing stratification. Another solution is to take the lower separating funnel, shaken vigorously after adding 2mL hexane. Still stratification, separation under
Layer solution. While 25mL of hexane was added 5.0mL of dimethyl sulfoxide, after vigorous shaking 1min lower solution was to do a reference in
260nm ~ 420nm measured absorbance.
Another solution of naphthalene-trimethylpentane, trimethyl pentane do reference, the solution was measured at the absorbance at 275nm, as for
According to value.
A.3.3 results found
All samples absorption peaks in the range of 260nm ~ 420nm, absorbance does not exceed one third of the control values, namely through
test.
A.4 pH measurement
A.4.1 Reagents
A.4.1.1 ethanol.
A.4.1.2 buffer solution. with two buffer solutions, the test sample should be close to the expected pH.
A.4.2 Instruments
A.4.2.1 pH meter. including temperature compensation system, the accuracy of at least 0.02.
A.4.2.2 electrode or composite electrode triple.
A.4.3 Analysis step
The electrode was washed with water and a standard buffer solution is placed in a test environment, between ambient temperature and the temperature as close as possible to each other. Select two
Species appropriate standard buffer solution, according to the instrument manual calibration of pH meter.
After instrument calibration, first rinse electrode, then dry with filter paper. Take appropriate sample in a beaker, and carefully insert the electrode in the sample,
The electrode is immersed, to be pH meter reading to stabilize and record the readings.
A.4.4 results found
The measurement results for the arithmetic mean of two parallel determination results of two parallel determination results shall not be greater than the absolute difference 0.1.
pH measurement results within the range of 3.0 to 4.4 experimentally.
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