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GB 1886.196-2016 English PDF

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GB 1886.196-2016: Food additive -- Ethyl hexanoate
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Basic data

Standard ID GB 1886.196-2016 (GB1886.196-2016)
Description (Translated English) Food additive -- Ethyl hexanoate
Sector / Industry National Standard
Classification of Chinese Standard X40
Word Count Estimation 6,642
Date of Issue 2016-08-31
Date of Implementation 2017-01-01
Older Standard (superseded by this standard) GB 8315-2008
Regulation (derived from) Announcement of the State Administration of Public Health and Family Planning 2016 No.11
Issuing agency(ies) National Health and Family Planning Commission of the People's Republic of China, State Food and Drug Administration

GB 1886.196-2016: Food additive -- Ethyl hexanoate

---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
(Food safety national standard - Food additive - Ethyl hexanoate) National Standards of People's Republic of China National Food Safety Standard Food additive ethyl hexyl Issued on.2016-08-31 2017-01-01 implementation People's Republic of China National Health and Family Planning Commission released

Foreword

This standard replaces GB 8315-2008 "food additive ethyl caproate." This standard compared with GB 8315-2008, the main changes are as follows. --- Solubility (25 ℃) by the "1mL sample soluble in 2mL70% (volume fraction) ethanol" to "1mL sample was dissolved in full 3mL70% (volume fraction) ethanol "; --- Ethyl acetate content was measured by packed column gas chromatography to capillary gas chromatography; --- Delete the words "heavy metal content" and "Arsenic content" requirement. National Food Safety Standard Food additive ethyl hexyl

1 Scope

This standard applies to acid and ethanol as raw materials by a chemical reaction of a food additive ethyl caproate. 2 chemical name, molecular formula, molecular mass and structural formula 2.1 Chemical Name Ethyl hexyl Formula 2.2 C8H16O2 2.3 formula 2.4 relative molecular mass 144.21 (according to 2007 international relative atomic mass)

3 Technical requirements

3.1 Sensory requirements Sensory requirements shall comply with the requirements of Table 1. Table 1 Sensory requirements Project requires test methods Color colorless Liquid state The sample was placed in a cuvette, were visually observed The aroma of the wine-like aroma GB/T 14454.2 3.2 Physical and Chemical Indicators Physical and chemical indicators should be consistent with the provisions of Table 2. Table 2. Physical and chemical indicators Item Index Test Method Solubility (25 ℃) 1mL sample soluble in 3mL70% (volume fraction) ethanol GB/T 14455.3 Ethyl acetate content, w /% ≥ 98.0 Appendix A Acid value (in dollars KOH)/(mg/g) ≤ 1.0 GB/T 14455.5 Refractive index (20 ℃) 1.406 ~ 1.409 GB/T 14454.4 The relative density (25 ℃/25 ℃) 0.867 ~ 0.871 GB/T 11540

Appendix A

Determination of the content of ethyl caproate A.1 instruments and equipment A.1.1 chromatograph. According to GB/T 11538-2006 provisions in Chapter 5. A.1.2 Column. capillary column. A.1.3 Detector. Hydrogen flame ionization detector. A.2 Determination Area normalization method. According to GB/T 11538-2006 10.4 Determination. A.3 repeatability and results are shown According to GB/T 11538-2006 provisions in 11.4, shall comply with the requirements. Food additive ethyl caproate gas chromatograph and operating conditions, see Appendix B.

Appendix B

Food additive ethyl caproate gas chromatograph and operating conditions (Area normalization method) B.1 food additive ethyl hexyl gas chromatogram Food additive ethyl hexyl gas chromatography is shown in Figure B.1. Figure B.1 food additive ethyl hexyl gas chromatogram B.2 operating conditions B.2.1 Column. capillary column length 30m, an inner diameter of 0.53mm. B.2.2 stationary phase. 100% dimethyl polysiloxane. B.2.3 film thickness. 1.5μm. B.2.4 chromatography oven temperature. linear temperature programmed from 70 ℃ to 180 ℃, the rate of 5 ℃/min; then linear temperature program from 180 ℃ to 260 ℃, the rate of 10 ℃/min; and finally at 260 ℃ constant temperature 10min. B.2.5 Inlet temperature. 260 ℃. B.2.6 detector temperature. 260 ℃. B.2.7 Detector. Hydrogen flame ionization detector. B.2.8 carrier gas. nitrogen. Before B.2.9 column pressure. 30kPa B.2.10 Injection volume. 0.2μL. B.2.11 split ratio. 80.1.

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