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GB 11960-2008: Food additive -- Oil of spearmint
Status: Obsolete GB 11960: Evolution and historical versions
| Standard ID | Contents [version] | USD | STEP2 | [PDF] delivered in | Standard Title (Description) | Status | PDF |
| GB 11960-2008 | English | 319 |
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Food additive -- Oil of spearmint
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GB 11960-2008
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| GB 11960-1989 | English | 199 |
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Food additive--Oil of spearmint
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PDF similar to GB 11960-2008
Basic data | Standard ID | GB 11960-2008 (GB11960-2008) | | Description (Translated English) | Food additive -- Oil of spearmint | | Sector / Industry | National Standard | | Classification of Chinese Standard | X44 | | Classification of International Standard | 71.100.60 | | Word Count Estimation | 8,832 | | Date of Issue | 2008-12-03 | | Date of Implementation | 2009-06-01 | | Older Standard (superseded by this standard) | GB 11960-1989 | | Quoted Standard | GB/T 5009.74; GB/T 5009.76; GB/T 11540; GB/T 14454.2; GB/T 14454.4; GB/T 14454.5; GB/T 14454.13-2008; GB/T 14455.3 | | Adopted Standard | FCC V-2004, NEQ | | Regulation (derived from) | Announcement of Newly Approved National Standards No. 19 of 2008 (No. 132 overall) | | Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China | | Summary | This Chinese standard specifies the food additive spearmint requirements, test methods, inspection rules, marking, packaging, transportation, storage and shelf life. This standard applies to food additives spearmint (Mentha spicata Linnalus) analysis and evaluation of the quality of the oil. | GB 11960-2008: Food additive -- Oil of spearmint---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Food additive.Oil of spearmint
ICS 71.100.60
X44
National Standards of People's Republic of China
Replacing GB 11960-1989
Food Additives spearmint
Posted 2008-12-03
2009-06-01 implementation
Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China
Standardization Administration of China released
Foreword
Chapter 4 of this standard are mandatory, the rest are recommended.
This standard with the US Food Chemicals Codex FCC (Ⅴ).2004 "spearmint" in non-equivalent.
This standard replaces GB 11960-1989 "Food Additives spearmint oil."
This standard compared with GB 11960-1989, the main modifications are as follows.
--- Added "3 Terms and Definitions" chapter;
--- 80% of spearmint refractive index from "1.4900 ~ 1.4960" to "1.4880 ~ 1.4960", polarimetry by the "-60 ° ~
-55 ° "to" -59 ° ~ -50 ° "; 60% spearmint optical rotation by the" -70 ° ~ -55 ° "to" -70 ° ~ -53 ° ";
--- Increased health indicators;
--- Added Appendix A typical gas chromatogram.
Appendix A of this standard is an informative annex.
The standard proposed by China National Light Industry Council.
This standard by the National Standardization Technical Committee on Food Additives.
The standard by the Shanghai Institute of perfumes, perfumery Lu'an, Anhui Province and Anhui Fengle spices limited liability company responsible for drafting.
The main drafters of this standard. Zhangxin Jun, Xu Yi, Jinqi Zhang, Duan Kai Ling, Sun Qinghua.
This standard replaces the standards previously issued as follows.
--- GB 11960-1989.
Food Additives spearmint
1 Scope
This standard specifies the food additive spearmint requirements, test methods, inspection rules, marking, packaging, transportation, storage and shelf life.
2 Normative references
The following documents contain provisions which, through reference in this standard and become the standard terms. For dated references, subsequent
Amendments (not including errata content) or revisions do not apply to this standard, however, encourage the parties to the agreement are based on research
Whether the latest versions of these documents. For undated reference documents, the latest versions apply to this standard.
GB/T 5009.74 limit test of heavy metals in food additives
Determination of GB/T 5009.76 arsenic in food additives
GB/T 11540 Determination of relative density of spices (GB/T 11540-2008, ISO 279.1998, MOD)
GB/T 14454.2 spice aroma evaluation method
GB/T 14454.4 spices refractive index measurement (GB/T 14454.4-2008, ISO 280.1998, MOD)
GB/T 14454.5 Determination of spices optical rotation (GB/T 14454.5-2008, ISO 592.1998, MOD)
GB/T 14454.13-2008 Determination of carbonyl value and carbonyl compounds content (ISO 1271. 1983, ISO 1279.1996,
MOD)
GB/T 14455.3 spices dissolved in ethanol (mixed) to assess the degree (GB/T 14455.3-2008, ISO 875.1999, MOD)
3 Terms and Definitions
The following terms and definitions apply to this standard.
3.1
Processing distillate obtained ketone containing a minimum amount of 60% and 80% of the two specifications of spearmint oil.
4 Requirements
Food Additives spearmint technical requirements should be consistent with Table 1.
Table 1
project
Claim
Containing 60% of the amount of ketone ketone containing an amount of 80%
Appearance light yellow to greenish yellow liquid
Aroma of spearmint leaf aroma and flavor characteristics
The relative density (20 ℃/20 ℃) 0.918 ~ 0.938 0.942 ~ 0.954
Refractive index (20 ℃) 1.4850 ~ 1.4910 1.4880 ~ 1.4960
Optical rotation (20 ℃) -70 ° ~ -53 ° -59 ° ~ -50 °
Miscibility (20 ℃) 1 volume of the sample soluble in 1 vol of 80% (volume fraction) ethanol as a clear solution
Ketone containing an amount ≥60.0% ≥80.0%
Heavy metal content (Pb) ≤10mg/kg
Arsenic content ≤3mg/kg
5 Test methods
5.1 Verification of Appearance
The sample is placed in color than the inner tube, were visually observed.
5.2 Evaluation aroma
According to the provisions of GB/T 14454.2 of.
5.3 Determination of relative density
According to GB/T 11540 regulations.
5.4 Determination of refractive index
According to GB/T 14454.4 of the provisions.
5.5 Determination of the optical rotation
According to GB/T 14454.5 of the provisions.
5.6 Assessment of miscibility
According to the provisions of GB/T 14455.3 of.
Determination of the amount of ketone containing 5.7
According to GB/T 14454.13-2008 third law provisions.
Food Additives spearmint typical gas chromatogram (area normalization method) See Appendix A.
5.8 Determination of heavy metal content (P Chou basis)
According to GB/T 5009.74 of the provisions.
5.9 Determination of Arsenic
According to GB/T 5009.76 of the provisions.
6 Inspection rules
6.1 Food additives spearmint plant by the quality inspection department inspection, the manufacturer shall ensure that products conform to this standard
Requirements, each batch of products should be accompanied by quality certificate. Appearance, aroma, relative density, refractive index, optical rotation, miscibility, including the amount of ketone
Factory inspection items, and arsenic content, heavy metal content (Pb) for the type of test items, test once every six months.
6.2 Acceptance shall be entitled in accordance with the provisions of this standard of product quality inspection received meets the requirements of this standard, for each batch
Once acceptance, acceptance of different batches respectively.
6.3 Sampling Method. each batch of packaging units 1 to 2, total pumping; 3 ~ 100 extract 2; 100 more than the increase taking further part
3%. Sampler with a sample drawn from a uniform 50mL ~ 100mL per package unit, all the extracted sample is placed within MIXER
Mix well, respectively, into two clean, dry, inert sealed containers, protected from light. Container attach a label stating. manufacturer name, product
Name, date of production, batch number, number and date of sampling, with a bottle for examination, another bottle retained for future reference.
6.4 As a result there is an indicator of acceptance does not meet the requirements of this standard, it can be doubled again in conjunction with the production plant to extract a sample reinspection. As retest knot
If there are indicators of failure, then the product can not be accepted.
6.5 When both supply and demand on product quality objection occurs, resolve by mutual agreement or arbitration by the statutory inspection bodies.
7 signs, packaging, transportation, storage and shelf life
7.1 marks
Packing of products should be marked. "food additive" word, product name, manufacturer name and address, trademark, batch number, net weight, date of manufacture
And shelf life, standard number and license number. For special customer requirements, and other custom manufacturers protocol.
7.2 Packaging
Food Additives spearmint oil should be installed in clean and free of miscellaneous taste of galvanized iron, food-grade plastic bucket, or according to customer requirement.
7.3 Transport
During transport should be light light disposal to prevent the sun and rain, can not be mixed with toxic and hazardous substances, mixed operation, and shall conform to the relevant departments
Provisions.
7.4 Storage
Products should be stored in a cool, dry, ventilated warehouse, avoid mixed air pollution, away from fire.
7.5 Shelf Life
Subject to the conditions of storage, packaging integrity, without the unsealing, the product shelf life of one year. Late re-examine whether the operator
Combined requirements of this standard, qualified can still be used.
Appendix A
(Informative)
Food Additives spearmint typical gas chromatogram
(Area normalization method)
A. 1 Food additives spearmint typical gas chromatogram
See Figure A. 1.
Peak number.
1 --- α- pinene;
2 --- β- pinene;
3 --- limonene;
4 --- 1,8 cineole;
5 --- octanol -3;
6 --- menthone;
7 --- new menthol;
8 --- dihydro-carvone;
. 9 --- menthol;
10 --- carvone;
. 11 --- trans-carvone;
12 --- cis carvone.
Figure A. 1
A. 2 Operating conditions
A. 2.1 Column. length 25m ~ 50m, diameter of about 0.24mm capillary column.
A. 2.2 stationary phase. PEG-20M.
A. 2.3 Chromatography furnace temperature. linear temperature programmed from 70 ℃ to 180 ℃, the rate of 2 ℃/min.
A. 2.4 Inlet temperature. 230 ℃.
A. 2.5 Detector temperature. 230 ℃.
A. 2.6 Detector. Hydrogen flame ionization detector.
A. 2.7 Carrier gas. nitrogen.
A. 2.8 Injection volume. about 0.2μL.
A. 2.9 Split ratio. 100/1.
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