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YS/T 922-2013 English PDF

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YS/T 922-2013: Methods for chemical analysis of high purity copper. Determination of trace impurity elements content. Glow discharge mass spectrometry
Status: Valid
Standard IDUSDBUY PDFLead-DaysStandard Title (Description)Status
YS/T 922-2013189 Add to Cart 3 days Methods for chemical analysis of high purity copper. Determination of trace impurity elements content. Glow discharge mass spectrometry Valid

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Basic data

Standard ID: YS/T 922-2013 (YS/T922-2013)
Description (Translated English): Methods for chemical analysis of high purity copper. Determination of trace impurity elements content. Glow discharge mass spectrometry
Sector / Industry: Nonferrous Metallurgy Industry Standard (Recommended)
Classification of Chinese Standard: H13
Classification of International Standard: 77.120.30
Word Count Estimation: 7,785
Regulation (derived from): Ministry of Industry and Information Technology Bulletin No. 52, 2013; industry standard for filing Notice No. 1 of 2014 (No. 169 overall)
Issuing agency(ies): Ministry of Industry and Information Technology
Summary: This standard specifies the method for the determination of trace elements in high copper content, the side of a given element are shown in Table 1, this standard applies to the high copper content of trace elements in the side of the set. Determination o

YS/T 922-2013: Methods for chemical analysis of high purity copper. Determination of trace impurity elements content. Glow discharge mass spectrometry


---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Methods for chemical analysis of high purity copper. Determination of trace impurity elements content. Glow discharge mass spectrometry ICS 77.120.30 H13 People's Republic of China Nonferrous Metals Industry Standard Methods for chemical analysis of high copper Determination of trace elemental content Glow Discharge Mass Spectrometry Issued on. 2013-10-17 2014-03-01 implementation Ministry of Industry and Information Technology of the People's Republic of China released

Foreword

This standard was drafted in accordance with GB/T 1.1-2009 given rules. This standard by the national non-ferrous metals Standardization Technical Committee (SAC/TC243) centralized. This standard is drafted by. Beijing Nonferrous Metal Research Institute. Participated in the drafting of this standard. Jinchuan Group Co., Ltd., Dongfang Electric Group Emei Semiconductor Materials Co., Ltd., there is research billion of New Materials Co., Ltd. The main drafters of this standard. Wang Changhua, Qinfang Lin, Wang Panfeng, Liu Ying, Sun Zeming, Li Jidong, Tong Jian, Zang Muwen, Qiu Ping, Wen-ying, Yet again brilliant. Methods for chemical analysis of high copper Determination of trace elemental content Glow Discharge Mass Spectrometry

1 Scope

This standard specifies the method for the determination of trace elements in a high copper content, the determination of elements in Table 1. This standard applies to the determination of trace elements in a high copper content. Determination of the elements as follows. measurement range of sulfur and selenium for 10μg/kg ~ 5000μg/kg, the remaining elements of the measurement range of 1μg/kg ~ 5000μg/kg.

2 principle of the method

Sample as a cathode glow discharge in argon atmosphere, and the surface thereof is sputtered atoms from the sample into the glow discharge plasma In plasma ionized and then introduced into the mass spectrometer. In each element isotope mass number punishable by default scan points and the integration time The corresponding peak integration, the resulting area is the peak intensity of element content by the formula (1) is obtained. When no standard samples, according to the instrument computer software The "typical relative sensitivity factor" automatically calculate the mass fraction of each element; when the standard sample, and the sample required by the same Analytical conditions, the ion source under test conditions and the structure of a standard sample was determined by independent relative sensitivity factor, the application of the relative sensitivity Factor to calculate the mass fraction of the elements.

3 Reagents and materials

Unless otherwise indicated, the reagents used in the analysis are excellent pure; water used as a water. 3.1 nitric acid (11). 3.2 copper standard sample, measured elements mass fraction of between 50μg/kg ~ 500μg/kg. 3.3 Background monitoring instrument samples tested elements mass fraction lower than the above test sample 10 times. 3.4 Argon (purity ≥99.999%). 3.5 Nitrogen (purity ≥99.99%).

4 Instrument

4.1 high resolution glow discharge mass spectrometer, under the resolution mode resolution of up to 3000 to 4000, high-resolution mode resolution Rate of up to 9,000 to 10,000. 4.2 Determination of isotope and resolution shown in Table 1. Requirements isotope 63Cu spectrum measured peak intensity is not less than 5 × 109cps, peak shape in line with points Resolution requirements.
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