YS/T 74.10-2010 English PDF

US$159.00 · In stock
Delivery: <= 3 days. True-PDF full-copy in English will be manually translated and delivered via email.
YS/T 74.10-2010: Methods of chemical anaysis of cadmium. Part 10: Determination of silver content. Flame atomic absorption spectrometry
Status: Valid

YS/T 74.10: Historical versions

Standard ID	USD	BUY PDF	Lead-Days	Standard Title (Description)	Status
YS/T 74.10-2010	159	Add to Cart	3 days	Methods of chemical anaysis of cadmium. Part 10: Determination of silver content. Flame atomic absorption spectrometry	Valid
YS/T 74.10-1994	199	Add to Cart	2 days	Methods for chemical analysis of cadmium. The atomic absorption spectrophotometric method for the determination of silver content	Obsolete

Similar standards

GB/T 3884.2   GB/T 3884.1   YS/T 252.1   YS/T 74.3   YS/T 74.4   YS/T 74.1   

Basic data

Standard ID: YS/T 74.10-2010 (YS/T74.10-2010)
Description (Translated English): Methods of chemical anaysis of cadmium. Part 10: Determination of silver content. Flame atomic absorption spectrometry
Sector / Industry: Nonferrous Metallurgy Industry Standard (Recommended)
Classification of Chinese Standard: H13
Classification of International Standard: 77.120.70
Word Count Estimation: 6,631
Date of Issue: 2010-11-22
Date of Implementation: 2011-03-01
Older Standard (superseded by this standard): YS/T 74.10-1994
Regulation (derived from): MIIT (2010) No. 126
Issuing agency(ies): Ministry of Industry and Information Technology
Summary: This standard specifies the amount of silver cadmium determination. This standard applies to the determination of cadmium in silver. Measuring range: 0. 00020% to 0. 0050%.

YS/T 74.10-2010: Methods of chemical anaysis of cadmium. Part 10: Determination of silver content. Flame atomic absorption spectrometry

---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Methods of chemical anaysis of cadmium.Part 10. Determination of silver content.Flame atomic absorption spectrometry ICS 77.120.70 H13 People's Republic of China Nonferrous Metals Industry Standard Replacing YS/T 74.10-1994 Methods for chemical analysis of cadmium Part 10. Determination of silver content Flame Atomic Absorption Spectrometry Part 10. Determinationofsilvercontent- Issued on. 2010-11-22 2011-03-01 implementation Ministry of Industry and Information Technology of the People's Republic of China released

Foreword

YS/T 74-2010 "cadmium chemical analysis method" is divided into 11 parts. --- Part 1. Determination of arsenic content by hydride generation - atomic fluorescence spectrometry; --- Part 2. Determination of antimony content hydride generation - atomic fluorescence spectrometry; --- Part 3. Determination of nickel content by electrothermal atomic absorption spectrometry; --- Part 4. Determination of lead content by flame atomic absorption spectrometry; --- Part 5. Determination of the amount of copper diethyl dithiocarbamate spectrophotometry lead; --- Part 6. Determination of zinc content - Flame atomic absorption spectrometry; --- Part 7. Determination of iron content of 1,10 phenanthroline spectrophotometry; --- Part 8. Determination of thallium content of crystal violet spectrophotometry; --- Part 9. Determination of tin content by hydride generation - atomic fluorescence spectrometry; --- Part 10. Determination of the amount of silver by flame atomic absorption spectrometry; --- Part 11. Inductively coupled plasma atomic arsenic, antimony, nickel, lead, copper, zinc, iron, thallium, tin and silver content of the emitted light Spectroscopy. This section section 10. This section drafted in accordance with GB/T 1.1-2009 given rules. The partial replacement of YS/T 74.10-1994 "cadmium chemical analysis by flame atomic absorption spectrometry silver amount", this part of the original standard Quasi compared to the main changes are as follows. --- Text format has been modified; --- Complements the precision, quality assurance and control provisions; --- Increase the warning prompt; --- Increasing the test report clause. The non-ferrous metal part by the National Standardization Technical Committee (SAC/TC243) centralized. This section is responsible for drafting unit. MCC Huludao Nonferrous Metals Group Co., Ltd. This section is drafted. Shenzhen Lingnan Nonferrous Metals Co., Ltd. Shaoguan smelter. Participated in the drafting of this section. Zhuzhou Smelter Group Co., Ltd., MCC Huludao Nonferrous Metals Group Co., Ltd., Beijing Mining and Metallurgy Research Institute, Henan Yuguang Gold & Lead Co., Ltd. The main drafters of this section. Zhuoyu Rui, Deng Zhihui, Zhang Yi, to De Lei, Liu Limin, Xi Hongjie, Yindong Xia, Chen Dianqiu, Wang Haoying, Ren Xiaodong. This part of the standard replaces the previous editions are. --- YS/T 74.10-1994; --- GB/T 3826-1983. Methods for chemical analysis of cadmium Part 10. Determination of silver content Flame Atomic Absorption Spectrometry Warning --- Use this section a person shall be regular laboratory work experience, and have the use of atomic absorption spectrophotometer Skills, in strict accordance with safety procedures atomic absorption spectrophotometer operation.

1 Scope

YS/T of the provisions of section 74 of the method for the determination of cadmium in silver content. This section applies to the determination of cadmium in silver content. Measurement range. 0.00020% to 0.0050%.

2 principle of the method

Sample decomposition with nitric acid, in dilute nitric acid medium, using air - acetylene flame atomic absorption spectrometer measured at a wavelength of 328.1nm Absorbance, using a calibration curve obtained by the amount of silver.

3 Reagents

Production of solutions and experiments with water are double-distilled water. Nitrate 3.1 (ρ1.42g/mL). 3.2 nitric acid (11). 3.3 Cadmium matrix solution. Weigh 20g metal cadmium (wCd≥99.99% and wAg0.0001%), placed in 500mL beaker, fractional total Was added 80mL of nitric acid (3.2), until the vigorous reaction was heated to dissolve completely, purge nitrogen oxides micro-boiling, cooled, transferred to 100mL capacity Dilution bottle with water to volume, and mix. This solution 1mL containing 200mg cadmium. 3.4 Silver standard stock solution. Weigh 0.1000g of metallic silver (wAg≥99.99%), placed in a beaker of 200mL, 10mL of nitric acid was added (3.2), cover sheet pan, heated slowly to dissolve completely removed, washed with water and dish table cup wall, cooled and transferred to 1000mL volumetric flask. 100mL nitric acid (3.2), dilute to the mark and mix. This solution 1mL containing 100μg silver. 3.5 silver standard solution. Pipette 10.00mL silver standard stock solution (3.4) in 1000mL volumetric flask 2mL nitric acid (3.2), Dilute with water to volume, and mix. This solution 1mL containing 10μg silver.

4 Instrument

Atomic absorption spectrometer, with a silver hollow-cathode lamp. Under optimum working conditions, who can reach the following indicators are, it can be used. --- Sensitivity. measurement solution matrix consistent solution, features silver concentration should be less than 0.022μg/mL. --- Precision. standard solution with the highest concentration of 10 times the absorbance measurements, the standard deviation should not exceed the average absorbance of 1.0% The lowest concentration of standard solution used (instead of "zero" standard solution) absorbance measured 10 times, and the standard deviation should not exceed the maximum concentration ......

Image     

Tips & Frequently Asked Questions:

Question 1: How long will the true-PDF of YS/T 74.10-2010_English be delivered?

Answer: Upon your order, we will start to translate YS/T 74.10-2010_English as soon as possible, and keep you informed of the progress. The lead time is typically 1 ~ 3 working days. The lengthier the document the longer the lead time.

Question 2: Can I share the purchased PDF of YS/T 74.10-2010_English with my colleagues?

Answer: Yes. The purchased PDF of YS/T 74.10-2010_English will be deemed to be sold to your employer/organization who actually pays for it, including your colleagues and your employer's intranet.

Question 3: Does the price include tax/VAT?

Answer: Yes. Our tax invoice, downloaded/delivered in 9 seconds, includes all tax/VAT and complies with 100+ countries' tax regulations (tax exempted in 100+ countries) -- See Avoidance of Double Taxation Agreements (DTAs): List of DTAs signed between Singapore and 100+ countries

Question 4: Do you accept my currency other than USD?

Answer: Yes. If you need your currency to be printed on the invoice, please write an email to Sales@ChineseStandard.net. In 2 working-hours, we will create a special link for you to pay in any currencies. Otherwise, follow the normal steps: Add to Cart -- Checkout -- Select your currency to pay.

Question 5: Should I purchase the latest version YS/T 74.10-2010?

Answer: Yes. Unless special scenarios such as technical constraints or academic study, you should always prioritize to purchase the latest version YS/T 74.10-2010 even if the enforcement date is in future. Complying with the latest version means that, by default, it also complies with all the earlier versions, technically.