YS/T 556.2-2009 English PDFUS$139.00 · In stock
Delivery: <= 3 days. True-PDF full-copy in English will be manually translated and delivered via email. YS/T 556.2-2009: Methods for chemical analysis of antimony concentrates. Part 2: Determination of arsenic content. Potassium bromate titration method Status: Valid YS/T 556.2: Historical versions
Basic dataStandard ID: YS/T 556.2-2009 (YS/T556.2-2009)Description (Translated English): Methods for chemical analysis of antimony concentrates. Part 2: Determination of arsenic content. Potassium bromate titration method Sector / Industry: Nonferrous Metallurgy Industry Standard (Recommended) Classification of Chinese Standard: D42 Classification of International Standard: 73.060 Word Count Estimation: 5,561 Date of Issue: 2009-12-04 Date of Implementation: 2010-06-01 Older Standard (superseded by this standard): YS/T 556.2-2006 Regulation (derived from): MIIT [2009] No. 66 Issuing agency(ies): Ministry of Industry and Information Technology Summary: This standard specifies: antimony concentrates Determination of arsenic content This standard applies to the amount of arsenic, antimony concentrate measured. Measuring range: 0. 10% to 2. 00 %. YS/T 556.2-2009: Methods for chemical analysis of antimony concentrates. Part 2: Determination of arsenic content. Potassium bromate titration method---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order. Methods for chemical analysis of antimony concentrates.Part 2. Determination of arsenic content.Potassium bromate titration method ICS 73.060 D42 People's Republic of China Nonferrous Metals Industry Standard Replacing YS/T 556.2-2006 Methods for chemical analysis of antimony concentrates Part 2. Determination of arsenic content potassium bromate titration Posted 2009-12-04 2010-06-01 implementation Ministry of Industry and Information Technology of the People's Republic of China released ForewordYS/T 556-2009 "Methods for chemical analysis of antimony concentrate," a total of 16 parts. --- Part 1. Determination of antimony content cerium sulfate titration; --- Part 2. Determination of arsenic content potassium bromate titration; --- Part 3. Determination of lead content by flame atomic absorption spectrometry; --- Part 4. Wet water storage Gravimetric method; --- Part 5. Determination of zinc content - Flame atomic absorption spectrometry; --- Part 6. Determination of the amount of selenium by hydride generation - atomic fluorescence spectrometry; --- Part 7. Determination of the amount of mercury atomic fluorescence spectrometry; --- Part 8. Determination of sulfur content - Combustion neutralization method; --- Part 9. Determination of the amount of gold fire assay; --- Part 10. Determination of copper content - Flame atomic absorption spectrometry; --- Part 11. Determination of cadmium content by flame atomic absorption spectrometry; --- Part 12. Determination of bismuth content by flame atomic absorption spectrometry; --- Part 13. Determination of nickel content by flame atomic absorption spectrometry; --- Part 14. Determination of the amount of silver by flame atomic absorption spectrometry; --- Part 15. antimony, tin measured by hydride generation - atomic fluorescence spectrometry; --- Part 16. Determination of antimony metal content by inductively coupled plasma emission spectrometry. This section YS/T 556 Part 2. "Antimony concentrates - Determination of arsenic content" in this section instead of YS/T 556.2-2006 (formerly GB/T 15080.2-1994). Compared with YS/T 556.2-2006, this part of the following changes. --- Text format has been modified; --- Complements the precision and quality assurance and control provisions. This section arbitration. The non-ferrous metal part by the National Standardization Technical Committee and centralized. This section is responsible for drafting unit. tin mine Twinkling Star Antimony Industry Co., Ltd., Beijing General Research Institute of Mining and Metallurgy. This section was drafted by the tin mining flash-antimony industry limited liability company. Participated in the drafting of this section. Hunan Chenzhou Mining Co., Ltd., Hunan Nonferrous Metal Research Institute, Beijing General Research Institute of Mining and Metallurgy, Guangzhou Nonferrous Metal Research Institute. The main drafters of this section. Cuide Hai, Song should the ball, and then Zhao Ying, Zhang Wei, Liu Tianping, Yang Deli, Wu Shaobo, Dai Fengying. This part of the standard replaces the previous editions are. --- GB/T 15080.2-1994; --- YS/T 556.2-2006. Methods for chemical analysis of antimony concentrates Part 2. Determination of arsenic content potassium bromate titration1 ScopeThis section YS/T 556 specifies the method for determination of the amount of arsenic in antimony concentrate. This section applies to the determination of the amount of arsenic in antimony concentrate. Measuring range. 0.10% to 2.00%.2 Method summarySample with sulfuric acid - potassium sulfate dissolved, filter paper made after carbonation reducing agent and co-solvent, not less than hydrochloric acid solution 9mol/L, the use of benzene Extract arsenic trichloride, arsenic back-extracted with water. In hydrochloric acid medium, methyl orange as indicator, titration titration of trivalent arsenic with potassium bromate standard.3 ReagentsUnless otherwise indicated, the reagents used in this section refer to water and analytical grade and third grade water. 3.1 potassium sulfate. 3.2 sulfate (ρ1.84g/mL). 3.3 hydrochloride (ρ1.19g/mL). 3.4 benzene. 3.5 sulfate (1 + 1). 3.6 HCl (3 + 1). 3.7 HCl (1 + 1). 3.8 methyl orange indicator (1g/L). 3.9 Sodium hydroxide solution (200g/L). 3.10 arsenic standard solution (1mg/mL). Weigh 1.3203g trioxide reference reagent (previously at 100 ℃ ~ 105 ℃ drying 1h, placed in a desiccator, cooled to room Temperature), placed in a beaker of 250mL, 20mL was added sodium hydroxide solution (3.9) was dissolved to a clear, 100mL water was added, 10 mL of sulfuric acid (3.5), cooled to room temperature and transferred to 1000mL volumetric flask, dilute with water to volume, and mix. 3.11 potassium bromate standard titration solution (Ba KBrO3 about 0.2mol/L). 3.11.1 preparation. Weigh 0.28g of potassium bromate placed in 250mL beaker, add 100mL water dissolved and transferred to 1000mL volumetric flask The diluted with water to volume, and mix. 3.11.2 Calibration. Pipette three 10.00mL arsenic standard solution (3.10), were added to 45mL containing hydrochloric acid (3.3) of 125mL liquid separation Funnel, and mix. 5.4.3 - 5.4.6 by the following conduct. Along with the calibration blank test. According to equation (1) calculate the standard volumetric potassium bromate solution (3.11) of the actual concentration. (1) Where. Ba --- potassium bromate standard volumetric solution (3.11) of the actual concentration in units of moles per liter (mol/L); Vp 1 --- titration titration of arsenic consumption of potassium bromate standard solution (3.11) of the volume, in milliliters (mL); V0 --- calibration blank solution volume of consumption of potassium bromate standard titration solution (3.11), expressed in milliliters (mL); ......Tips & Frequently Asked Questions:Question 1: How long will the true-PDF of YS/T 556.2-2009_English be delivered?Answer: Upon your order, we will start to translate YS/T 556.2-2009_English as soon as possible, and keep you informed of the progress. The lead time is typically 1 ~ 3 working days. The lengthier the document the longer the lead time.Question 2: Can I share the purchased PDF of YS/T 556.2-2009_English with my colleagues?Answer: Yes. 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