YS/T 556.11-2011 English PDFUS$159.00 · In stock
Delivery: <= 3 days. True-PDF full-copy in English will be manually translated and delivered via email. YS/T 556.11-2011: Methods for chemical analysis of antimony concentrates. Part 11: Determination of cadmium content. Flame atomic absorption spectrometric method Status: Valid
Basic dataStandard ID: YS/T 556.11-2011 (YS/T556.11-2011)Description (Translated English): Methods for chemical analysis of antimony concentrates. Part 11: Determination of cadmium content. Flame atomic absorption spectrometric method Sector / Industry: Nonferrous Metallurgy Industry Standard (Recommended) Classification of Chinese Standard: D42 Classification of International Standard: 73.060 Word Count Estimation: 6,677 Date of Issue: 2011-12-20 Date of Implementation: 2012-07-01 Regulation (derived from): ?MIIT Announcement 2011 No.43 Issuing agency(ies): Ministry of Industry and Information Technology Summary: This standard specifies the determination of the amount of cadmium antimony concentrate. This standard applies to the determination of the amount of cadmium antimony concentrate. Measurement range: 0. 0010% to 0. 050%. YS/T 556.11-2011: Methods for chemical analysis of antimony concentrates. Part 11: Determination of cadmium content. Flame atomic absorption spectrometric method---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order. Methods for chemical analysis of antimony concentrates.Part 11. Determination of cadmium content.Flame atomic absorption spectrometric method ICS 73.060 D42 People's Republic of China Nonferrous Metals Industry Standard Methods for chemical analysis of antimony concentrates Part 11. Determination of cadmium content Flame Atomic Absorption Spectrometry Part 11. Determinationofcadmiumcontent- Issued on. 2011-12-20 2012-07-01 implementation Ministry of Industry and Information Technology of the People's Republic of China released ForewordThis section is in accordance with GB/T 1.1-2009 given rules drafted. YS/T 556 "Methods for chemical analysis of antimony concentrate," a total of 16 parts. --- Part 1. Determination of antimony content cerium sulfate titration; --- Part 2. Determination of arsenic content potassium bromate titration; --- Part 3. Determination of lead content by flame atomic absorption spectrometry; --- Part 4. Wet water storage Gravimetric method; --- Part 5. Determination of zinc content - Flame atomic absorption spectrometry; --- Part 6. Determination of the amount of selenium by hydride generation - atomic fluorescence spectrometry; --- Part 7. Determination of the amount of mercury atomic fluorescence spectrometry; --- Part 8. Determination of sulfur content - Combustion neutralization method; --- Part 9. Determination of the amount of gold fire assay; --- Part 10. Determination of copper content - Flame atomic absorption spectrometry; --- Part 11. Determination of cadmium content by flame atomic absorption spectrometry; --- Part 12. Determination of bismuth content by flame atomic absorption spectrometry; --- Part 13. Determination of nickel content by flame atomic absorption spectrometry; --- Part 14. Determination of the amount of silver by flame atomic absorption spectrometry; --- Part 16. lead, zinc, copper, cadmium, nickel content - Inductively coupled plasma atomic emission spectrometry. This is Part 11. The non-ferrous metal part by the National Standardization Technical Committee (SAC/TC243) centralized. This standard is drafted by. Tin Mine Twinkling Star Antimony Industry Co., Ltd., Beijing General Research Institute of Mining and Metallurgy. This section is drafted. Beijing General Research Institute of Mining and Metallurgy. Participated in the drafting of this section. Guangzhou Research Institute of Nonferrous Metals, Tin Mine flash-antimony industry limited liability company. The main drafters of this section. Tangshu Fang, Liu Chunfeng, Liu Wei, Dai Fengying, Liutian Ping, Mao Xiaohong, SONG Ying ball. Methods for chemical analysis of antimony concentrates Part 11. Determination of cadmium content Flame Atomic Absorption Spectrometry1 ScopeYS/T 556 This section specifies the determination of antimony concentrates cadmium content. This section applies to the determination of antimony concentrates cadmium content. Determination range of 0.0010% to 0.050%.2 Method summaryA specimen in a hydrochloric acid, nitric acid, perchloric acid dissolved, in addition to volatilization of antimony hydrobromic, hydrochloric acid (119) media, using air - acetylene flame, Atomic absorption spectrometer wavelength 228.8nm measured absorbance cadmium.3 ReagentsUnless otherwise indicated in the analysis using only recognized as analytical grade reagents and distilled or deionized water or equivalent purity. 3.1 ammonium hydrogen fluoride. 3.2 hydrochloric acid (ρ = 1.19g/mL). 3.3 nitric acid (ρ = 1.42g/mL). 3.4 hydrobromide (ρ = 1.38g/mL). 3.5 perchloric acid (ρ = 1.68g/mL). 3.6 hydrochloride (11). 3.7 nitric acid (11). 3.8 cadmium standard stock solution. Weigh 1.0000g metal cadmium (wCd≥99.99%) in 250mL beaker, add 40mL of nitric acid (11), dissolved by heating, boiling rid of nitrogen oxides, remove the cooled to room temperature and transferred to 1000mL volumetric flask, dilute to the mark, Mix well. This solution 1mL containing cadmium 1.000mg. 3.9 Cadmium standard solution. Pipette 5.00mL cadmium standard stock solution (3.8) in 500mL volumetric flask, was added 20mL of hydrochloric acid (3.6), Dilute with water to volume, and mix. This solution 1mL containing cadmium 10μg.4 InstrumentAtomic absorption spectrometer, with a cadmium hollow cathode lamp. Under optimum working conditions for those who can reach the following indicators can be used. --- Characteristic concentration. the test solution and measurement matrix consistent solution, characteristic concentration of cadmium should be less than 0.014μg/mL. --- Linear curve. The curve is divided into five sections according to concentration, absorbance difference between the highest and the lowest section of the absorbance difference between segments Ratio of not less than 0.85. --- Precision. measure 10 times the absorbance of the highest concentration of the standard solution, the standard deviation should not exceed 1% of the average absorbance; with The lowest concentration standard solution (not a "zero" standard solution) absorbance measured 10 times, and the standard deviation should not exceed the standard maximum concentration ......Tips & Frequently Asked Questions:Question 1: How long will the true-PDF of YS/T 556.11-2011_English be delivered?Answer: Upon your order, we will start to translate YS/T 556.11-2011_English as soon as possible, and keep you informed of the progress. The lead time is typically 1 ~ 3 working days. 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