YS/T 539.12-2009 English PDFYS/T 539.12: Historical versions
Basic dataStandard ID: YS/T 539.12-2009 (YS/T539.12-2009)Description (Translated English): Methods for chemical analysis of nickel base alloy powder. Part 12: Determination of phosphorus content. N-butyl alacohol-chloroform extraction spectrophotometry Sector / Industry: Nonferrous Metallurgy Industry Standard (Recommended) Classification of Chinese Standard: H71;H14 Classification of International Standard: 77.120.40 Word Count Estimation: 6,653 Date of Issue: 2009-12-04 Date of Implementation: 2010-06-01 Older Standard (superseded by this standard): YS/T 539.12-2006 Regulation (derived from): MIIT [2009] No. 66 Issuing agency(ies): Ministry of Industry and Information Technology Summary: This standard specifies the nickel- base alloy powder Determination of phosphorus content. This standard applies to nickel-base alloy powder in the determination of phosphorus content, measuring range: 0. 001% to 0. 05%. YS/T 539.12-2009: Methods for chemical analysis of nickel base alloy powder. Part 12: Determination of phosphorus content. N-butyl alacohol-chloroform extraction spectrophotometry---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order. Methods for chemical analysis of nickel base alloy powder.Part 12. Determination of phosphorus content.N-butyl alacohol-chloroform extraction spectrophotometry ICS 77.120.40 H71 People's Republic of China Nonferrous Metals Industry Standard Replacing YS/T 539.12-2006 Nickel-based alloy powder chemical analysis Part 12. determination of phosphorus content N-butyl alcohol - chloroform extraction photometric Posted 2009-12-04 2010-06-01 implementation Ministry of Industry and Information Technology of the People's Republic of China released ForewordYS/T 539 "nickel-based alloy powder chemical analysis method" is divided into 13 parts. --- Part 1. Determination of the amount of boron acid-base titration; --- Part 2. Determination of the amount of chrome aluminum Azure S Spectrophotometry; --- Part 3. Determination of silicon content of perchloric acid dehydration gravimetric method; --- Part 4. Determination of chromium content of ammonium persulfate oxidation titration; --- Part 5. Determination of manganese content of sodium periodate (K) oxidation spectrophotometry; --- Part 6. Determination of iron content of titanium trichloride - potassium dichromate titration; --- Part 7. Determination of cobalt content nitroso R salt spectrophotometric method; --- Part 8. Determination of copper content Neocuproine - chloroform extraction spectrophotometric method; --- Part 9. Determination of copper content of sodium thiosulfate iodometry; --- Part 10. Determination of molybdenum content - Thiocyanate spectrophotometric method; --- Part 11. Determination of cinchonine gravimetric method tungsten content; --- Part 12. Determination of phosphorus content of n-butyl alcohol - chloroform extraction spectrophotometric method; --- Part 13. Determination of oxygen pulse heating inert gas fusion - infrared absorption method. This section is YS/T 539 Part 12. The partial replacement of YS/T 539.12-2006 "nickel-based alloy powder chemical analysis of n-butyl alcohol - chloroform extraction photometric measurements Given the amount of phosphorus. " This portion of YS/T 539.12-2006 phase comparator major changes are as follows. --- Increasing the foreword; --- Complements the repeatability limit. The non-ferrous metal part by the National Standardization Technical Committee and centralized. This section is responsible for drafting unit. Beijing Nonferrous Metal Research Institute, China Nonferrous Metals Industry Institute of Standards and Metrology and Quality. This section is drafted. Beijing Nonferrous Metal Research Institute, Steel Research Institute. The main drafters of this section. Liu Fang, Plant Protection]. This part of the standard replaces the previous editions are. --- GB/T 8638.12-1988; --- YS/T 539.12-2006. Nickel-based alloy powder chemical analysis Part 12. determination of phosphorus content N-butyl alcohol - chloroform extraction photometric1 ScopeYS/T 539 This part specifies the method for determination of nickel-base alloy powder phosphorus content. This section applies to the determination of nickel-base alloy powder phosphorus content measurement range. 0.001% to 0.05%.2 Method summarySample by mixed acid is dissolved in nitric acid medium, ortho-phosphoric acid and ammonium molybdate generated phosphomolybdic heteropoly acid is n-butanol - chloroform extraction, chlorine Stannous phosphorus molybdenum heteropoly acid reduction and back-extracted into the aqueous phase, at a wavelength of 680nm spectrophotometer measured absorbance.3 ReagentsUnless otherwise indicated in the analysis using only recognized as analytical grade reagents and distilled or deionized water or equivalent purity. 3.1 sodium hydroxide. 3.2 hydrochloride (ρ1.19g/mL). Nitrate 3.3 (ρ1.42g/mL). 3.4 Hydrofluoric acid (ρ1.15g/mL). 3.5 perchloric acid (ρ1.67g/mL). 3.6 ammonium molybdate solution (100g/L). 3.7 sodium nitrite solution (300g/L). 3.8 nitric acid (1 + 1). nitrate (3.3) to boil 3min ~ 5min, formulated after the flooding exhausted nitrogen oxides. 3.9 citric acid solution (100g/L). Per 100mL solution with an aqueous solution containing 3.5g of sodium hydroxide in the formulation. 3.10 butanol - a mixture of chloroform. n-butanol and a mixed three chloroform. 3.11 stannous chloride solution (10g/L). 1g stannous chloride (SnCl2 · 2H2O) was dissolved in 8mL hydrochloric acid (3.2), diluted with water to 100mL, the time is now equipped with. 3.12 P standard stock solution. Weigh in advance by 105 ℃ ~ 110 ℃ drying 0.2195g potassium dihydrogen phosphate reference reagents dissolved in water, Plus 10mL of nitric acid (3.3) and transferred to 1000mL volumetric flask, dilute to the mark, mix and store in a plastic bottle. This solution 1mL Phosphorus-containing 50μg. 3.13 Phosphorus standard solution. Pipette 20.00mL phosphorus standard stock solution (3.12) into 1000mL flask, add 5mL nitric acid (3.3), dilute to the mark and mix. This solution 1mL containing 1μg phosphorus.4 InstrumentSpectrophotometer. Step 5 Analysis 5.1 Sample Weigh 0.10g ~ 0.50g sample, accurate to 0.0001g. 5.2 Determination of the number of Independent of the two measurements, the mean value. ......Tips & Frequently Asked Questions:Question 1: How long will the true-PDF of YS/T 539.12-2009_English be delivered?Answer: Upon your order, we will start to translate YS/T 539.12-2009_English as soon as possible, and keep you informed of the progress. The lead time is typically in 9 seconds (download/delivered in 9 seconds). The lengthier the document the longer the lead time.Question 2: Can I share the purchased PDF of YS/T 539.12-2009_English with my colleagues?Answer: Yes. 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