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YS/T 1115.7-2016 English PDF

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YS/T 1115.7-2016: (Methods for chemical analysis of copper ores and tailings - Part 7: Determination of manganese content - Flame atomic absorption spectrometric method)
Status: Valid
Standard IDUSDBUY PDFLead-DaysStandard Title (Description)Status
YS/T 1115.7-2016139 Add to Cart 3 days (Methods for chemical analysis of copper ores and tailings - Part 7: Determination of manganese content - Flame atomic absorption spectrometric method) Valid

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YS/T 951   SN/T 3510   GB/T 8152.1   YS/T 1115.11   YS/T 1115.1   YS/T 1115.10   

Basic data

Standard ID: YS/T 1115.7-2016 (YS/T1115.7-2016)
Description (Translated English): (Methods for chemical analysis of copper ores and tailings - Part 7: Determination of manganese content - Flame atomic absorption spectrometric method)
Sector / Industry: Nonferrous Metallurgy Industry Standard (Recommended)
Classification of Chinese Standard: D42
Word Count Estimation: 6,63
Date of Issue: 2016-07-11
Date of Implementation: 2017-01-01
Regulation (derived from): Notice of the Ministry of Industry and Information Technology (2016 No. 37)
Issuing agency(ies): Ministry of Industry and Information Technology
Summary: This standard specifies the method for determining the amount of manganese in copper ore and tailings.

YS/T 1115.7-2016: (Methods for chemical analysis of copper ores and tailings - Part 7: Determination of manganese content - Flame atomic absorption spectrometric method)


---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
(Methods for chemical analysis of copper ores and tailings - Part 7. Determination of manganese content - Flame atomic absorption spectrometric method) ICS 73.060 D42 People's Republic of China non-ferrous metal industry standards Copper ores and tailings - Chemical analysis methods Part 7. Determination of manganese content Flame atomic absorption spectrometry Methods for chemical analysis of copperores and tailings Part 7.Determinationofmanganesecontent 2016-07-11 released 2017-01-01 implementation Ministry of Industry and Information Technology of the People's Republic of China

Foreword

YS/T 1115-2016 "Copper ore and tailings chemical analysis method" is divided into the following 14 sections. --- Part 1. Determination of copper content by flame atomic absorption spectrometry; --- Part 2. Determination of lead content by flame atomic absorption spectrometry; --- Part 3. Determination of zinc content by flame atomic absorption spectrometry; --- Part 4. Determination of nickel content by flame atomic absorption spectrometry; --- Part 5. Determination of cobalt content by flame atomic absorption spectrometry; --- Part 6. Determination of cadmium content by flame atomic absorption spectrometry; --- Part 7. Determination of manganese content by flame atomic absorption spectrometry; --- Part 8. Determination of magnesium content by flame atomic absorption spectrometry; --- Part 9. Determination of sulfur content by high-frequency infrared absorption and combustion - potassium iodate titration; --- Part 10. Determination of phosphorus content molybdenum blue spectrophotometry; --- Part 11. Determination of molybdenum content thiocyanate spectrophotometry; --- Part 12. Determination of copper, lead, zinc, nickel, cobalt, cadmium, magnesium and manganese content; Inductively coupled plasma atomic emission spectrometry; --- Part 13. Determination of fluorine content ion selective electrode method and ion chromatography; --- Part 14. Determination of arsenic hydride generation atomic fluorescence spectrometry and potassium bromate titration. This section is the seventh part of YS/T 1115-2016. This section drafted in accordance with GB/T 1.1-2009 given rules. This part of the National Non-ferrous Metal Standardization Technical Committee (SAC/TC243) centralized. This section mainly drafted unit. Beijing Mining and Metallurgy Research Institute. Participate in the drafting of this section. Ningbo Exit Inspection and Quarantine, China Nonferrous Guilin Institute of Mineral Geology Co., Ltd., Hunan Nonferrous Metals Metal Research Institute, Zhejiang Huayou Cobalt Co., Ltd., Zijin Mining Group Co., Ltd., Xiamen Zijin Mining Metallurgical Technology Co., Ltd., Jinchuan Group Co., Ltd. The main drafters of this section. Han Xiao, Liu Runting, Liu in the United States, Shi Honglan, dry line, Qiu Li, Yang Deli, Pang Wenlin, Xie Bohua, Shen Jiayue, Summer Pearl, Zhang Houqiang, Luo Ronggen, Zhang Yuan, Yu Shengjie, Ma Yuping. Copper ores and tailings - Chemical analysis methods Part 7. Determination of manganese content Flame atomic absorption spectrometry

1 Scope

YS/T 1115 provisions of this part of the copper ore and tailings Determination of manganese content. This section applies to the determination of manganese content of copper ore and tailings. The measurement range is from 0.0050% to 0.50%.

2 method summary

Sample with hydrochloric acid, nitric acid, hydrofluoric acid and perchloric acid decomposition. Hydrochloric acid dissolves salts in dilute hydrochloric acid medium at atomic absorption spectrometer wavelength At 279.5 nm, the air-acetylene flame was used to measure the absorbance of manganese and the manganese content was calculated using the working curve method.

3 reagent

Unless otherwise noted, only reagents identified as analytical grade were used in the analysis, all of which used distilled or deionized water or equivalent purity Water. 3.1 Hydrochloric acid (p = 1.19 g/mL). 3.2 Nitric acid (p = 1.42 g/mL). Hydrofluoric acid (ρ = 1.15 g/mL). 3.4 Perchloric acid (ρ = 1.67g/mL). 3.5 Hydrochloric acid (1 1). 3.6 manganese standard stock solution Weigh 1.0000g of metal manganese (wMn ≥ 99.99%) placed in 250mL beaker, add 20mL hydrochloric acid (3.5) heated to dissolve completely, removed and cooled to room temperature, transferred to a 1000mL volumetric flask, was added 80mL hydrochloric acid (3.5), diluted with water until engraved Degree, mix well. 1 mL of this solution contains 1 mg of manganese. 3.7 manganese standard solution Pipette 10.00mL manganese standard stock solution (3.6) placed in 100mL volumetric flask, add 10mL hydrochloric acid (3.5), diluted with water to the mark, mix well. 1 mL of this solution contains 100 μg manganese.

4 instruments

Atomic absorption spectrometer, with manganese hollow cathode lamp. Under the instrument working conditions, any atomic absorption spectrometer that can achieve the following indexes can be used. --- Characteristic concentration. In the solution and the test solution is basically the same, the characteristic concentration of manganese should not exceed 0.040μg/mL; --- Precision. With the highest concentration of standard solution measured 10 times the absorbance, the standard deviation should not exceed 1.0% of the average absorbance; Measure the absorbance 10 times with the lowest concentration of the standard solution (not a "zero" standard solution) with a standard deviation of no more than the highest concentration Standard solution 0.5% of the average absorbance; --- The working curve of the linear. The working curve according to the concentration is divided into 5 segments, the highest segment of the absorbance difference and the lowest segment of the absorbance difference The ratio should not be less than 0.80.
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