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Determination of boric acid and borates in cosmetics for import-export - ICP-OES method
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Basic data
| Standard ID | SN/T 3826-2014 (SN/T3826-2014) |
| Description (Translated English) | Determination of boric acid and borates in cosmetics for import-export - ICP-OES method |
| Sector / Industry | Commodity Inspection Standard (Recommended) |
| Classification of Chinese Standard | Y42 |
| Classification of International Standard | 71.100.70 |
| Word Count Estimation | 8,888 |
| Quoted Standard | GB/T 6682; SN/T 2192 |
| Regulation (derived from) | AQSIQ notification issued in 2014 on the first batch of 230 industry-standard entry-exit inspection and quarantine |
| Issuing agency(ies) | General Administration of Customs |
| Summary | This Standard specifies the import and export cosmetics boric acid and borate content of inductively coupled plasma emission spectrometry method. This Standard applies to the determination of import and export cosmetics boron content as boric acid or bora |
SN/T 3826-2014: Determination of boric acid and borates in cosmetics for import-export - ICP-OES method
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(Boric acid and borate content and export cosmetics - Determination - Inductively coupled plasma atomic emission spectrometry)
People's Republic of China Entry-Exit Inspection and Quarantine Standards
Determination of the import and export cosmetics boric acid and salt content
Inductively coupled plasma atomic emission spectrometry
ICP-OESmethod
Issued on. 2014-01-13
2014-08-01 implementation
People's Republic of China
The State Administration of Quality Supervision, Inspection and Quarantine released
Foreword
This standard was drafted in accordance with GB/T 1.1-2009 given rules.
Please note that some content of this document may involve patents, publication of this document
Institutions do not assume the responsibility to identify these patents.
This standard is proposed and managed by the National Certification and Accreditation Administration Committee.
This standard was drafted. People's Republic of China Zhejiang Exit Inspection and Quarantine, Zhejiang Inspection and Quarantine Institute of Science and Technology.
The main drafters of this standard. Dai Qi, Jiang Bing Shuai, Han Chao, Lin Xiaonuo, Dayton Yu Hui, Wang Xuqiang, Lou Shi Ming, Song Lei, Fang Cheng, Wu Yanyan,
Chenjun Xiao, Jiang Xiaoying.
Determination of the import and export cosmetics boric acid and salt content
Inductively coupled plasma atomic emission spectrometry
1 Scope
This standard specifies the import and export cosmetics boric acid and borate content by inductively coupled plasma emission spectrometry method.
This standard applies to the determination of import and export cosmetics boron content as boric acid or borate results count.
2 Normative references
The following documents for the application of this document is essential. For dated references, only the dated version suitable for use herein
Member. For undated references, the latest edition (including any amendments) applies to this document.
Laboratory use specifications and test methods GB/T 6682 Analysis
SN/T 2192 Importers and cosmetic laboratory chemical analysis sample preparation Specification
3 Method summary
After the sample digestion, measured spectral intensity in the corresponding element ICP-OES wavelength, using the standard curve internal standard.
4 Reagents and materials
Unless otherwise specified, all reagents superior grade pure water was used a water line with GB/T 6682 stipulated.
Nitrate 4.1 (MOS level, 65%).
4.2 Hydrogen peroxide (30% aqueous solution).
4.3 nitric acid solution (595). Measure 50mL of nitric acid (4.1) slowly added to 950mL of water.
4.4 boron standard stock solution (1000μg/mL). direct use element standard solution standard material certificates are valid within the standard concentration
Of 1000μg/mL.
4.5 yttrium standard stock solution (100μg/mL). As ICP-OES detection of an internal standard, the direct use of reference material certificates valid
Element standard solution, standard solution concentration period of 100μg/mL.
4.6 boron standard solution (10μg/mL). Imbibe 1.0mL boron standard stock solution (4.4) to 100mL volumetric flask, with nitrate
Acid solution (4.3) diluted to volume.
The preparation of the solution should be promptly transferred to a plastic bottle (Do not use glass products, to avoid contamination) and stored at 0 ℃ ~ 5 ℃ refrigerator, effective
Period of one month.
4.7 Argon. purity of greater than or equal to 99.99%.
5. Apparatus
5.1 Inductively coupled plasma atomic emission spectrometer.
5.2 Analysis of balance. a sense of the amount of 1mg.
5.3 microwave digestion system. Containers used are plastic containers, all containers shall be subject to a 20% nitric acid soak overnight.
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