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Determination of volatile nitrosamines in cosmetics. Gas chromatography-tandem mass spectrometry method
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Basic data
| Standard ID | SN/T 3607-2013 (SN/T3607-2013) |
| Description (Translated English) | Determination of volatile nitrosamines in cosmetics. Gas chromatography-tandem mass spectrometry method |
| Sector / Industry | Commodity Inspection Standard (Recommended) |
| Classification of Chinese Standard | Y42 |
| Classification of International Standard | 71.100.70 |
| Word Count Estimation | 9,969 |
| Quoted Standard | GB/T 6682 |
| Regulation (derived from) | National quality recognition (2013), No. 464; industry standard filing Notice No. 1 of 2014 (No. 169 overall) |
| Issuing agency(ies) | General Administration of Customs |
| Summary | This standard specifies the volatile nitrosamines in cosmetics by gas chromatography - mass spectrometry/mass spectrometry. This standard applies to creams, liquid, shampoo, lipstick, loose powder cosmetics in N-nitroso dimethyl amine, N-nitroso diethylam |
SN/T 3607-2013: Determination of volatile nitrosamines in cosmetics. Gas chromatography-tandem mass spectrometry method
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Determination of volatile nitrosamines in cosmetics. Gas chromatography-tandem mass spectrometry method
People's Republic of China Entry-Exit Inspection and Quarantine Standards
Determination of volatile nitrosamines in cosmetics
Gas chromatography - mass spectrometry/mass spectrometry
Issued on. 2013-08-30
2014-03-01 implementation
People's Republic of China
The State Administration of Quality Supervision, Inspection and Quarantine released
Foreword
Accordance with the standards GB/T 1.1-2009 "Standardization Guide Part 1. Standard structure and preparation of", GB/T 20001.4-
2001. Rules "Part 4 Rules for drafting standards for chemical analysis method" gives the drafting.
Please note that some of the content of this document may involve patents. Release mechanism of the present document does not assume responsibility for the identification of these patents.
This standard is proposed and managed by the National Certification and Accreditation Administration Committee.
This standard was drafted. Chinese Academy of Inspection and Quarantine, Chongqing, People's Republic of China Exit Inspection and Quarantine.
The main drafters of this standard. Ma Qiang, Wang Chao, birch, Wang Ye, Ding Lan TRANSACTIONS OF Meng double, Jing.
Determination of volatile nitrosamines in cosmetics
Gas chromatography - mass spectrometry/mass spectrometry
1 Scope
This standard specifies the volatile nitrosamines in cosmetics by gas chromatography - mass spectrometry/mass spectrometry.
This standard applies to creams, liquid, shampoo, lipstick, loose Cosmetics N- nitroso dimethylamine, N- nitroso diethylamine, N-
Nitroso dipropyl amine, N- nitroso morpholine, N- nitroso pyrrolidine, N- nitroso piperidine, N- nitroso dibutyl amine, N- nitroso-diphenyl
Yl amine, N- nitroso dicyclohexyl amine, N- nitroso dibenzylamine determination and confirmation.
2 Normative references
The following documents for the application of this document is essential. For dated references, only the dated version suitable for use herein
Member. For undated references, the latest edition (including any amendments) applies to this document.
Laboratory use specifications and test methods GB/T 6682 Analysis
Principle 3
Different types of cosmetic sample with a suitable organic solvent extraction, after solid phase extraction (SPE), by gas chromatography - mass spectrometry/mass spectrometry measurement
Fixed, external standard.
4 Reagents and materials
Unless otherwise indicated, the reagents used were of analytical grade water as a water GB/T 6682 regulations.
4.1 Methanol. chromatographically pure.
4.2 dichloromethane. chromatography.
4.3 acetone. chromatography.
4.4 ethanol. chromatography.
4.5 N- nitroso dimethylamine Standard Substance. CAS No. 62-75-9, purity of greater than or equal to 97%.
4.6 N- nitroso diethylamine Standard Substance. CAS No. 55-18-5, purity of greater than or equal to 98%.
4.7 N- nitroso dipropylamine standard substance. CAS No. 621-64-7, purity of greater than or equal to 99%.
4.8 N- nitroso morpholine Standard Substance. CAS No. 59-89-2, purity of greater than or equal to 99%.
4.9 N- nitrosopyrrolidine standard substance. CAS No. 930-55-2, purity of greater than or equal to 97%.
4.10 N- nitroso piperidine Standard Substance. CAS No. 100-75-4, purity of greater than or equal to 98%.
4.11 N- nitroso-dibutylamine Standard Substance. CAS No. 924-16-3, purity of greater than or equal to 97%.
4.12 N- nitroso-diphenylamine standard substance. CAS No. 86-30-6, purity of greater than or equal to 97%.
4.13 N- nitroso dicyclohexylamine Standard Substance. CAS No. 947-92-2, purity of greater than or equal to 99%.
4.14 N- nitroso dibenzylamine Standard Substance. CAS No. 5336-53-8, purity of greater than or equal to 99%.
4.15 volatile nitrosamines standard stock solution. Weigh accurately respectively 10mg (accurate to 0.0001g) each volatile nitrosamines standard, set
In 100mL flask, diluted with methanol to the mark, mix and concentration of the solution is 100mg/L, at 4 ℃ dark preservation, valid for 3
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