SN/T 3344-2012 English PDFUS$209.00 · In stock
Delivery: <= 3 days. True-PDF full-copy in English will be manually translated and delivered via email. SN/T 3344-2012: Determination of free glycerin in crude glycerin. Gas chromatography Status: Valid
Basic dataStandard ID: SN/T 3344-2012 (SN/T3344-2012)Description (Translated English): Determination of free glycerin in crude glycerin. Gas chromatography Sector / Industry: Commodity Inspection Standard (Recommended) Word Count Estimation: 8,890 Regulation (derived from): National Quality Inspection (2012) 777; industry standard filing Notice 2013 No. 4 (No. 160 overall) Issuing agency(ies): General Administration of Customs Summary: This standard specifies the crude glycerol of free glycerol content Gas chromatographic method. This standard applies to the mass fraction of less than 95% bio-diesel made crude glycerin byproduct, industrial saponification glycerine and synthetic glyceri SN/T 3344-2012: Determination of free glycerin in crude glycerin. Gas chromatography---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.Determination of free glycerin in crude glycerin.Gas chromatography People's Republic of China Entry-Exit Inspection and Quarantine Standards Crude glycerol free glycerol determination Gas chromatography Issued on. 2012-12-12 2013-07-01 implementation People's Republic of China The State Administration of Quality Supervision, Inspection and Quarantine released ForewordThis standard was drafted in accordance with GB/T 1.1-2009 given rules. This standard is proposed and managed by the National Certification and Accreditation Administration Committee. This standard was drafted. People's Republic of China Jiangsu Entry-Exit Inspection and Quarantine Bureau. The main drafters of this standard. Ding Hua, Li Xidong, Zhouqiu Hong, lord Hing. Crude glycerol free glycerol determination Gas chromatography1 ScopeThis standard specifies the gas chromatographic method crude glycerol free glycerol content. This standard applies to the mass fraction of less than 95% of the by-product bio-diesel made crude glycerin, industrial saponification glycerol synthetic glycerine.2 Method summaryAfter the sample was added acetic anhydride was heated to produce triacetin after derivatization reaction was measured by gas chromatography internal standard method.3 ReagentsUnless otherwise indicated in the analysis using only recognized as analytical reagents. Sample Glycerin 3.1 (C3H8O3). content of more than 99%. Acetic anhydride 3.2 (C4H6O3). content greater than 95%. 3.3 Internal standard. ethyl benzoate (C9H10O2), content greater than 99%.4 Instrument4.1 Gas chromatograph. equipped with a flame ionization detector (FID). 4.2 micro-injector. 10μL. 4.3 Pipette. 1mL, 25mL. 4.4 dropper. 25mL. 4.5 stoppered conical flask. 125mL. 4.6 Analysis of balance. a sense of the amount of 0.1mg.5 SampleCrude glycerin samples were thoroughly mixed, placed in a dropper bottle and set aside. Step 6 Analysis 6.1 Preparation of the sample By Difference Method Weigh 0.4g ~ 0.5g sample of the crude glycerol in stoppered Erlenmeyer flask, accurate to 0.2mg. 6.2 Derivative In a sample containing glycerin stoppered Erlenmeyer flask, 25mL acetic anhydride (3.2), placed in an oven at 120 ℃ reaction 2h. Remove to cooling ......Tips & Frequently Asked Questions:Question 1: How long will the true-PDF of SN/T 3344-2012_English be delivered?Answer: Upon your order, we will start to translate SN/T 3344-2012_English as soon as possible, and keep you informed of the progress. The lead time is typically 1 ~ 3 working days. The lengthier the document the longer the lead time.Question 2: Can I share the purchased PDF of SN/T 3344-2012_English with my colleagues?Answer: Yes. The purchased PDF of SN/T 3344-2012_English will be deemed to be sold to your employer/organization who actually pays for it, including your colleagues and your employer's intranet.Question 3: Does the price include tax/VAT?Answer: Yes. Our tax invoice, downloaded/delivered in 9 seconds, includes all tax/VAT and complies with 100+ countries' tax regulations (tax exempted in 100+ countries) -- See Avoidance of Double Taxation Agreements (DTAs): List of DTAs signed between Singapore and 100+ countriesQuestion 4: Do you accept my currency other than USD?Answer: Yes. If you need your currency to be printed on the invoice, please write an email to Sales@ChineseStandard.net. In 2 working-hours, we will create a special link for you to pay in any currencies. Otherwise, follow the normal steps: Add to Cart -- Checkout -- Select your currency to pay. |