SN/T 2570-2010 English PDFUS$209.00 · In stock
Delivery: <= 3 days. True-PDF full-copy in English will be manually translated and delivered via email. SN/T 2570-2010: Determination of short-chain chloinated paraffins in leather. Gas chromatography method Status: Valid
Basic dataStandard ID: SN/T 2570-2010 (SN/T2570-2010)Description (Translated English): Determination of short-chain chloinated paraffins in leather. Gas chromatography method Sector / Industry: Commodity Inspection Standard (Recommended) Classification of Chinese Standard: Y45 Classification of International Standard: 59.140.01 Word Count Estimation: 8,866 Date of Issue: 2010-05-27 Date of Implementation: 2010-12-01 Regulation (derived from): National Quality Inspection (2010) 290; industry standard filing Notice 2010 No. 10 (No. 130 overall) Issuing agency(ies): General Administration of Customs Summary: This standard specifies the leather C10 ~ C13 SCCP residues by gas chromatography detection methods. This standard applies to leather C10 ~ C13 SCCP residues. SN/T 2570-2010: Determination of short-chain chloinated paraffins in leather. Gas chromatography method---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order. Determination of short-chain chloinated paraffins in leather.Gas chromatography method People's Republic of China Entry-Exit Inspection and Quarantine Standards Leather chlorinated paraffin residues in detection of short-chain Gas chromatography Issued on. 2010-05-27 2010-12-01 implementation People's Republic of China The State Administration of Quality Supervision, Inspection and Quarantine released ForewordThis standard was drafted in accordance with GB/T 1.1-2009 given rules. This standard is proposed and managed by the National Certification and Accreditation Administration Committee. This standard was drafted. People's Republic of China Zhejiang Exit Inspection and Quarantine. The main drafters of this standard. Zhu Yu, Ding Huiying, Qin Jiang Ting. Leather chlorinated paraffin residues in detection of short-chain Gas chromatography Warning. dangerous hydrogen gas, attention to indoor air.1 ScopeThis standard specifies the leather C10 ~ C13 gas chromatography method SCCP residues. This standard applies to the determination of C10 ~ C13 leather SCCP residues. Principle 2 Samples were ultrasonic extraction, Florisil column purification, hydrogen as a carrier gas, under the action of hydrogen chloride, palladium-catalyzed after a short chain Chlorinated paraffins into linear paraffins, to detect the amount of internal standard hydrogen flame detector. Catalytic reaction formula. Cl Cl Cl Cl Cl Cl Hydrogen, 300 ℃ → palladium chloride C C 6HCl3 Reagents and materialsUnless otherwise specified, all reagents were of analytical grade, water is deionized water or equivalent purity. 3.1 ammonia. 3.2 Acetic acid. 36%. 3.3 acetic acid solution (5%). Take 14mL acetic acid (3.2) to 100mL volumetric flask with deionized water to volume, shake reserve. 3.4 hexane. pesticide grade. 3.5 ether. 3.6 eluent. n-hexane - diethyl ether (9010, volume ratio). 3.7 cyclopentane. Palladium chloride, 3.8. 3.9 calcium carbonate. 3.10 Glass beads. 60 mesh to 80 mesh. 3.11 Florisil SPE column. 1g, 6mL. 3.12 Deactivated single taper liner. diameter 4mm. 3.13 1,2,4-trimethylbenzene. 3.14 C10 ~ C13 paraffin mixed standard solution. 100μg/mL, 55.5% average degree of chlorination. 3.15 C10, C11, C12, C13 linear alkanes standards. than 99.5% purity. 3.16 linear paraffin mixed standard solution. accurately weighed amount C10, C11, C12, C13 standard linear alkanes (3.15), paired with n-hexane 1.0mg/mL stock solution, and then were drawn C10, C11, C12, C13 straight-chain alkanes dubbed a stock solution of 100μg/mL mixed standard. ...... |
