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SN/T 2461-2010 English PDF

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SN/T 2461-2010: Determination of the phenoxy acid pesticide residues in textiles. LC-MS/MS method
Status: Valid
Standard IDUSDBUY PDFLead-DaysStandard Title (Description)Status
SN/T 2461-2010319 Add to Cart 3 days Determination of the phenoxy acid pesticide residues in textiles. LC-MS/MS method Valid

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Basic data

Standard ID: SN/T 2461-2010 (SN/T2461-2010)
Description (Translated English): Determination of the phenoxy acid pesticide residues in textiles. LC-MS/MS method
Sector / Industry: Commodity Inspection Standard (Recommended)
Classification of Chinese Standard: W04
Classification of International Standard: 59.080.01
Word Count Estimation: 12,173
Date of Issue: 2010-01-10
Date of Implementation: 2010-07-16
Quoted Standard: GB/T 6682
Regulation (derived from): National Quality Inspection (2010) No. 13
Issuing agency(ies): General Administration of Customs
Summary: This standard specifies the use of liquid chromatography tandem mass spectrometry (LC-MS/MS) determination of textiles seven kinds of pesticide residues phenoxy acid method. This standard applies to textiles seven kinds of phenoxy acid pesticide residues.

SN/T 2461-2010: Determination of the phenoxy acid pesticide residues in textiles. LC-MS/MS method


---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Determination of the phenoxy acid pesticide residues in textiles.LC-MS/MS method Exit inspection and quarantine industry standard book People's Republic of China Textiles - Determination of phenoxy acid Pesticide Residues Liquid chromatography - tandem mass spectrometry Issued on. 2010-01-10 2010-07-16 implementation People's Republic of China The State Administration of Quality Supervision, Inspection and Quarantine released

Foreword

Appendix A of this standard is a normative appendix, Appendix B, Appendix C and Appendix D is an informative annex. This standard is proposed and managed by the National Certification and Accreditation Administration Committee. This standard was drafted. People's Republic of China Shandong CIQ, Qingdao Textile Fiber Testing. The main drafters of this standard. Cattle Zengyuan, Luo Xin, Ye Xi Wen, Tangzhi Xu, Ning Xia Wang, Cao Wenqing. This standard is the first release of the entry-exit inspection and quarantine industry standards. Textiles - Determination of phenoxy acid Pesticide Residues Liquid chromatography - tandem mass spectrometry

1 Scope

This standard specifies the use of liquid chromatography - tandem mass spectrometry (LC-MS/MS) Textiles - Determination of Seven Phenoxyacid pesticide residues Methods. This standard applies to the determination of seven kinds of textiles phenoxy acid pesticide residues.

2 Normative references

The following documents contain provisions which, through reference in this standard and become the standard terms. For dated references, subsequent Amendments (not including errata content) or revisions do not apply to this standard, however, encourage the parties to the agreement are based on research Whether the latest versions of these documents. For undated reference documents, the latest versions apply to this standard. Laboratory use specifications and test methods GB/T 6682 Analysis Principle 3 The sample was acidic acetone extraction, the extract was concentrated volume, low temperature impurity precipitation, liquid chromatography - tandem mass spectrometry (LC- Determination of MS/MS) and confirmed, external standard.

4 Reagents and materials

Unless otherwise specified, the reagents used were of analytical grade. The water used in line with GB/T 6682 provided a water. 4.1 Methanol. HPLC grade. 4.2 acetone. HPLC grade. 4.3 formic acid. 88%. Ammonium acetate 4.4. HPLC grade. 4.5 ammonium acetate solution. 5mmol/L. 4.6 phenoxy acid pesticide standards. purity ≥98%, see Appendix A. 4.7 standard stock solution. namely, accurately weighed amount of each pesticide standards phenoxy acid with methanol were formulated into mass concentration 100μg/mL standard stock solution. 4.8 negative sample extracts. phenoxy acids containing no pesticide residues in samples of different substrates prepared in accordance with 6.1 negative sample extract. 4.9 matrix-matched standard solution. A standard stock solution (4.7) diluted with negative sample extract (4.8) needs to be adapted according to the concentration The matrix-matched standard working solution. Reference linear range. 1ng/mL ~ 100ng/mL.

5 instruments and equipment

5.1 Liquid chromatography - tandem mass spectrometer. with electrospray ionization (ESI). 5.2 Balance. a sense of the amount of 0.1mg and 0.01g. 5.3 ultrasonic generator. 100W, operating frequency 40kHz. 5.4 rotary evaporator. 5.5 conical flask. a grinding gag, 100mL.
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