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SN/T 2454-2010 English PDF

Standard IDUSDBUY PDFLead-DaysStandard Title (Description)Status
SN/T 2454-2010359 Add to Cart 3 days Determination of dimethyl fumarate in mildew preventives. Gas chromatography spectrometry Obsolete

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Basic data

Standard ID: SN/T 2454-2010 (SN/T2454-2010)
Description (Translated English): Determination of dimethyl fumarate in mildew preventives. Gas chromatography spectrometry
Sector / Industry: Commodity Inspection Standard (Recommended)
Classification of Chinese Standard: Y44
Classification of International Standard: 71.100.99
Word Count Estimation: 9,989
Date of Issue: 2010-03-02
Date of Implementation: 2010-09-16
Quoted Standard: GB/T 6283
Regulation (derived from): National Quality Inspection (2010) 98; industry standard filing Notice 2010 No. 5 (No. 125 overall)
Issuing agency(ies): General Administration of Customs
Summary: This standard specifies the fungicide dimethyl fumarate gas chromatography detection methods. This standard method a suitable organic purity dimethyl fumarate, not less than 95 % of the fungicide in the determination of dimethyl fumarate, methods, two for naphthalene content of 10 % to 95% of fungicide Determination of dimethyl fumarate.

SN/T 2454-2010: Determination of dimethyl fumarate in mildew preventives. Gas chromatography spectrometry


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Determination of dimethyl fumarate in mildew preventives.Gas chromatography spectrometry Exit inspection and quarantine industry standard book People's Republic of China Determination of dimethyl fumarate in fungicide Gas chromatography Issued on. 2010-03-02 2010-09-16 implementation People's Republic of China The State Administration of Quality Supervision, Inspection and Quarantine released

Foreword

Appendix A of this standard is an informative annex. This standard is proposed and managed by the National Certification and Accreditation Administration Committee. This standard is drafted by. People's Republic of China Guangdong Entry-Exit Inspection and Quarantine Bureau, People's Republic of China Fujian Entry-Exit Inspection and Quarantine Bureau. The main drafters of this standard. Li Dan, ZHOU Ming-hui, Di Cuiping, Homocysteine on Linbi Fen, Liu Yingfeng, Yueda Lei, Xiaoda Hui, Zheng Jianguo. This standard is the first release of the entry-exit inspection and quarantine industry standards. Determination of dimethyl fumarate in fungicide Gas chromatography

1 Scope

This standard specifies the fungicide dimethyl fumarate by gas chromatography detection methods. This standard applies to a method of dimethyl fumarate organic purity of not less than 95% of fungicide dimethyl fumarate determination method Not applicable to the content of dimethyl fumarate, dimethyl fumarate, measured in 10% to 95% of the fungicide.

2 Normative references

The following documents contain provisions which, through reference in this standard and become the standard terms. For dated references, subsequently Some amendments (not including errata content) or revisions do not apply to this standard. However, encourage the parties to the agreement Research on whether to use the latest versions of these documents. For undated reference documents, the latest versions apply to this standard. GB/T 6283 Determination of moisture content of chemical products Karl Fischer method (General method)

3 Terms and Definitions

The following terms and definitions apply to this standard. Dimethyl fumarate (Dimethylfumarate, CAS Code. 624-49-7) Its structural formula is shown in Figure 1. Formula 1 dimethyl fumarate Method 4 a 4.1 Principle of the method First, according to GB/T 6283 Determination of sample moisture content by the Karl Fischer method, the sample is then determined gravimetrically ethyl acetate Insolubles content; determination of organic purity dimethyl fumarate by gas chromatography and then, after deduction of water and ethyl acetate insoluble content meter Operators sample of dimethyl fumarate content. 4.2 Reagents Ethyl acetate. analytical purity ≥99.5%, over 5 molecular sieve dehydration process?. By GC assay, in dimethyl fumarate peaks No interference peak appears at a retention time. 4.3 instruments and equipment 4.3.1 Gas Chromatograph (GC). with a FID detector. 4.3.2 Glass beaker. 25mL. 4.3.3 Filter crucible. G4 type, 30mL. 4.3.4 Electronic balance. a sense of the amount of 0.1mg. 4.3.5 Micro Injector. 10μL. 4.3.6 blast oven. 4.3.7 ultrasonic extractor.
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