SN/T 2224-2008 English PDFUS$469.00 · In stock
Delivery: <= 3 days. True-PDF full-copy in English will be manually translated and delivered via email. SN/T 2224-2008: Determination of rifaximin residue in foodstuffs of animal origin for export and import. LC-MS/MS method Status: Valid
Basic dataStandard ID: SN/T 2224-2008 (SN/T2224-2008)Description (Translated English): Determination of rifaximin residue in foodstuffs of animal origin for export and import. LC-MS/MS method Sector / Industry: Commodity Inspection Standard (Recommended) Classification of Chinese Standard: X04 Word Count Estimation: 18,130 Date of Issue: 2008-11-18 Date of Implementation: 2009-06-01 Quoted Standard: GB/T 6682 Regulation (derived from): National Quality Inspection [2008] No. 577 Issuing agency(ies): General Administration of Customs Summary: This standard specifies the animal derived food residues Lifestyle Ximing liquid chromatography mass spectrometry/mass spectrometry. This standard applies to pork, liver, kidney, milk Lifestyle Ximing residue detection and confirmation. SN/T 2224-2008: Determination of rifaximin residue in foodstuffs of animal origin for export and import. LC-MS/MS method---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order. Determination of rifaximin residue in foodstuffs of animal origin for export and import.LC-MS/MS method Exit inspection and quarantine industry standard book People's Republic of China Import and export of food of animal origin Lifestyle Ximing Residue Detection Liquid chromatography - mass spectrometry/mass spectrometry Posted 2008-11-18 2009-06-01 implementation People's Republic of China The State Administration of Quality Supervision, Inspection and Quarantine released ForewordThe Standard Appendix A and Appendix B are informative. This standard is proposed and managed by the National Certification and Accreditation Administration Committee. This standard by the People's Republic of China Liaoning Entry-Exit Inspection and Quarantine is responsible Heilongjiang People's Republic of China Drafted. The main drafters of this standard. Li Yichen, Linwei Xuan, Hong celebrate. This standard is the first release of the entry-exit inspection and quarantine industry standards. Import and export of food of animal origin Lifestyle Ximing Residue Detection Liquid chromatography - mass spectrometry/mass spectrometry1 ScopeThis standard specifies the foods of animal origin Lifestyle Ximing residues LC - MS/MS detection method. This standard applies to pork, liver, kidney, milk Lifestyle Ximing residues in the detection and confirmation.2 Normative ReferencesThe following documents contain provisions which, through reference in this standard and become the standard terms. For dated references, subsequent Amendments (not including errata content) or revisions do not apply to this standard, however, encourage the parties to the agreement are based on research Whether the latest versions of these documents. For undated reference documents, the latest versions apply to this standard. Laboratory use specifications and test methods GB/T 6682 analysis. (GB/T 6682-2008, ISO 3696. 1987, MOD)3 Method summarySamples Lifestyle Ximing residue was extracted with acetonitrile, hexane removed from the extract fat, solid-phase extraction (SPE), eluent nitrogen blow After liquid chromatography tandem mass spectrometry, external standard.4 Reagents and materialsUnless otherwise indicated, the reagents used were of analytical grade water as a water GB/T 6682 regulations. 4.1 acetonitrile. HPLC fractions. 4.2 hexane. HPLC fractions. 4.3 isopropanol. 4.4 formic acid. HPLC fractions. 4.5 anhydrous sodium. 650 ℃ burning 4h, placed in a desiccator. 4.6 acetonitrile saturated with n-hexane. 100mL acetonitrile was added 100mL of n-hexane, followed by sufficient shaking, standing layer, the upper layer of liquid. 4.7 0.1% formic acid solution. Take 1mL exact amount of formic acid (4.4) in 1L flask, water volume to 1L. 4.8 acetonitrile - water (40 + 60, by volume). Measure 40mL of acetonitrile is added 60mL of water and mix. Lifestyle Ximing 4.9 standard (Rifaximin, CASN o.80621-81-4). purity of greater than or equal to 95%. 4.10 Lifestyle Ximing standard stock solution. Weigh about 0.01g Lifestyle Ximing standard (accurate to 0.0001g), dissolved in acetonitrile and dilute to 100mL, this standard solution at a concentration of 100μg/mL, placed in -18 ℃ refrigerator stored. Shelf life of six months. 4.11 Lifestyle Ximing standard solution (1.0μg/mL). draw the right amount of Lifestyle Ximing standard stock solution (4.10), paired with acetonitrile 1.0μg/mL of standard working solution. Standard working solution at 4 ℃ dark storage. 4.12 SPE column. WatersoasisHLB column, 500mg, 6mL, or equivalent person. 4.13 microporous membrane. 0.45μm, organic phase. 5. Apparatus 5.1 High performance liquid chromatography - mass spectrometry/mass spectrometer. with electrospray ionization source. 5.2 Organization mashed machines. ......Tips & Frequently Asked Questions:Question 1: How long will the true-PDF of SN/T 2224-2008_English be delivered?Answer: Upon your order, we will start to translate SN/T 2224-2008_English as soon as possible, and keep you informed of the progress. The lead time is typically 1 ~ 3 working days. The lengthier the document the longer the lead time.Question 2: Can I share the purchased PDF of SN/T 2224-2008_English with my colleagues?Answer: Yes. The purchased PDF of SN/T 2224-2008_English will be deemed to be sold to your employer/organization who actually pays for it, including your colleagues and your employer's intranet.Question 3: Does the price include tax/VAT?Answer: Yes. 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