| SN/T 1986-2007 English PDFUS$609.00 · In stock Delivery: <= 4 days. True-PDF full-copy in English will be manually translated and delivered via email. SN/T 1986-2007: Determination of chlorfenapyr residues in food for import and export Status: Valid 
 Basic dataStandard ID: SN/T 1986-2007 (SN/T1986-2007)Description (Translated English): Determination of chlorfenapyr residues in food for import and export Sector / Industry: Commodity Inspection Standard (Recommended) Classification of Chinese Standard: X04 Classification of International Standard: 67.050 Word Count Estimation: 19,120 Date of Issue: 2007-08-06 Date of Implementation: 2008-03-01 Regulation (derived from): National-accreditation-Science [2011] 63 Issuing agency(ies): General Administration of Customs Summary: This standard specifies the food Chlorfenapyr residues in sample preparation, gas chromatography and gas chromatography detection methods Mass Spectrometry methods. This standard applies to beans, tea, soybeans, cabbage, apples, vinegar, chicken, pork, fish, beef and other residues Chlorfenapyr determination. SN/T 1986-2007: Determination of chlorfenapyr residues in food for import and export---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.Determination of chlorfenapyr residues in food for import and export Exit inspection and quarantine industry standard book People's Republic of China Imported and exported food chlorfenapyr Residue Detection Posted 2007-08-06 2008-03-01 implementation People's Republic of China The State Administration of Quality Supervision, Inspection and Quarantine released ForewordAppendix A of this standard is an informative annex. This standard is proposed and managed by the National Certification and Accreditation Administration Committee. This standard was drafted. Tianjin People's Republic of China Entry-Exit Inspection and Quarantine of Zhejiang People's Republic of China Bureau, People's Republic of China Fujian Exit Inspection and Quarantine, Chinese Academy of Inspection and Quarantine. The main drafters of this standard. Linan Qing, Zhang Man, Xu Hong, Wu Yanhui, Zhang Hua, HE Jia, Gu Long, Xiaoya Bing, Bao Xiaoxia, Yang Fang, LI Shu-juan. This is the first issue of inspection and quarantine industry standards. Imported and exported food chlorfenapyr Residue Detection1 ScopeThis standard specifies the sample preparation, gas chromatography and gas chromatography detection methods in food chlorfenapyr Residues of - and MS methods. This standard applies to chlorfenapyr residues in beans, tea, soybeans, cabbage, apple, vinegar, chicken, pork, fish, beef and other measurement.2 Method summarySample chlorfenapyr residues extracted with acetonitrile, neutral alumina SPE or GCB SPE column purification, eluent After concentration constant volume, gas phase chromatography and gas chromatography - mass spectrometry confirmed, external standard.3 Reagents and materialsUnless otherwise specified, the reagents were of analytical grade, water is distilled water. 3.1 acetonitrile. HPLC fractions. 3.2 hexane. HPLC fractions. 3.3 acetone. HPLC fractions. 3.4 anhydrous sodium sulfate. After burning 650 ℃ 4h, placed in a desiccator. 3.5 sodium chloride. 3.6 sodium chloride solution (100g/L). Weigh 100g of sodium chloride, add water to 1L. 3.7 phosphate buffer solution (1mol/L, pH7.0). Weigh 105g (± 0.1g) and dipotassium hydrogen phosphate 61g (± 0.1g) dihydrogen phosphate Potassium, adding about 500mL dissolved in water, adjusted pH7.0 with 1mol/L sodium hydroxide or 1mol/L hydrochloric acid, and add water to 1L. 3.8 extract. hexane saturated with acetonitrile + acetonitrile (1 + 1, volume ratio). 3.9 eluent. n-hexane + acetone (1 + 1, volume ratio). 3.10 chlorfenapyr (Chlorfenapyr, C15H11BrClF3N2O, CAS. 122453-73-0) Standard. 99% or greater purity. 3.11 chlorfenapyr standard solution. Accurately weigh an adequate amount of chlorfenapyr standards, paired with n-hexane at a concentration of 100μg/mL standard stock liquid. Needed with n-hexane diluted to the appropriate concentration of the working standard solution. Note. Standard stock solution and working standard solution stored in 0 ℃ ~ 4 ℃ refrigerator. 3.12 neutral alumina SPE. 3mL, 500mg. 3.13 GCB SPE. 3mL, 500mg. 3.14 anhydrous sodium sulfate column. 80mm × 40mm (inner diameter) cylindrical funnel, bottom cushion height about 5mm cotton, refill 20g dry sulfur Sodium.4 instruments and equipment4.1 Gas chromatography with electron capture detector. 4.2 Gas chromatography - mass spectrometry with negative chemical ionization. 4.3 filtration device. 4.4 rotary evaporator. 4.5 nitrogen blowing instrument. 4.6 high-speed homogenizer. 4.7 Centrifuge. 3000r/min. 4.8 Solid phase extraction device. 4.9 vortex mixer. ......Tips & Frequently Asked Questions:Question 1: How long will the true-PDF of SN/T 1986-2007_English be delivered?Answer: Upon your order, we will start to translate SN/T 1986-2007_English as soon as possible, and keep you informed of the progress. The lead time is typically 2 ~ 4 working days. 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