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SN/T 1850.2-2006 English PDF

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SN/T 1850.2-2006: Determination of alkylphenol polyethoxylates in textiles. Part 2: High performance liquid chromatography-mass chromatography method
Status: Valid
Standard IDUSDBUY PDFLead-DaysStandard Title (Description)Status
SN/T 1850.2-2006259 Add to Cart 3 days Determination of alkylphenol polyethoxylates in textiles. Part 2: High performance liquid chromatography-mass chromatography method Valid

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Basic data

Standard ID: SN/T 1850.2-2006 (SN/T1850.2-2006)
Description (Translated English): Determination of alkylphenol polyethoxylates in textiles. Part 2: High performance liquid chromatography-mass chromatography method
Sector / Industry: Commodity Inspection Standard (Recommended)
Classification of Chinese Standard: W04
Classification of International Standard: 59-010
Word Count Estimation: 8,841
Date of Issue: 2006-11-10
Date of Implementation: 2007-05-16
Regulation (derived from): Chinese industry standards for record 2007 of 3 (total of 87)
Issuing agency(ies): General Administration of Customs
Summary: This standard specifies the textile phenols and Wan Wan benzene phenol polyoxyethylene ethers of high performance liquid chromatography mass spectrometry. This standard applies to textiles and Wan Wan benzene phenol phenol polyoxyethylene ethers determination.

SN/T 1850.2-2006: Determination of alkylphenol polyethoxylates in textiles. Part 2: High performance liquid chromatography-mass chromatography method


---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Determination of alkylphenol polyethoxylates in textiles. Part 2. High performance liquid chromatography-mass chromatography method Book of the People's Republic of China Entry and Exit Inspection and Quarantine Alkylphenols and alkylphenols in textiles Determination of polyoxyethylene ethers Part 2. high performance liquid chromatography-mass spectrometry Released on.2006-11-10 2007-05-16 implementation People's Republic The General Administration of Quality Supervision, Inspection and Quarantine issued

Foreword

SN/T 1850 "Determination of alkyl phenols and alkyl phenol ethoxylates in textiles" is divided into two parts. --- Part 1. High performance liquid chromatography; --- Part 2. High performance liquid chromatography-mass spectrometry. This part is the second part of the SN/T 1850. Appendix A and Appendix B of this part are informative annexes. This part is proposed and managed by the National Certification and Accreditation Administration. This part is drafted by the Shenzhen Entry-Exit Inspection and Quarantine Bureau of the People's Republic of China. The main drafters of this section. Zhang Weiya, Li Lixia, Liu Caiming, Wang Chengyun, Fan Xiurong, Tang Lichun. This section is the first industry standard for entry-exit inspection and quarantine. Alkylphenols and alkylphenols in textiles Determination of polyoxyethylene ethers Part 2. high performance liquid chromatography-mass spectrometry

1 Scope

This part of SN/T 1850 specifies high performance liquid chromatography-mass spectrometry for alkyl phenols and alkyl phenol ethoxylates in textiles. test methods. This section applies to the determination of alkylphenols and alkylphenol ethoxylates in textiles.

2 Terms and definitions

The following terms and definitions apply to this part of the SN/T 1850. 2.1 The molecular structure of the alkylphenols is. R-C6H4-OH. This class of substances, commonly found in textiles, is octylphenol (C8H17- C6H4-OH, abbreviated as OP) and nonylphenol (C9H19-C6H4-OH, abbreviated as NP). 2.2 The molecular structure of the alkylphenol ethoxylates is. R-C6H4-(OC2H4)nOH. This type of substance is common in textiles. Octylphenol polyoxyethylene ether (C8H17-C6H4-(OC2H4)nOH, referred to as OPEO) and nonylphenol polyoxyethylene ether [C9H19-C6H4- (OC2H4)nOH, referred to as NPEO]. Alkylphenol ethoxylates can be used as surfactants in textiles, and alkylphenols are alkylphenol ethoxylates. Degradation products.

3 Principle

The sample was extracted by Soxhlet using methanol as the extraction solvent, the extract was concentrated, and the membrane was filtered and then subjected to high performance liquid chromatography-mass spectrometry. Conduct qualitative and quantitative analysis.

4 reagents and materials

Unless otherwise specified, only analytically pure reagents and distilled or deionized water or water of comparable purity were used in the analysis. 4.1 Methanol. Chromatographically pure. 4.2 Acetonitrile. chromatographically pure. 4.3 Octylphenol standard (purity. 97%). 4.4 Nonylphenol standard (purity. technical). 4.5 Octylphenol polyoxyethylene ether standard (purity. extra grade pure). 4.6 Nonylphenol ethoxylate standard (purity. ≥99.0%). 4.7 Alkylphenol standard stock solution. accurately weigh the appropriate amount of octylphenol (4.3) and nonylphenol (4.4) standards, with methanol (4.1) Prepared as a standard stock solution at a concentration of 10 mg/mL. 4.8 Alkylphenol polyoxyethylene ether standard stock solution. accurately weigh the appropriate amount of octylphenol polyoxyethylene ether (4.5) and mercaptobenzene Phenol polyoxyethylene ether (4.6) standard was prepared with methanol (4.1) as a standard stock solution at a concentration of 10 mg/mL.
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