GB/T 22964-2008 English PDF

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GB/T 22964-2008: Determination of lincomycin, oleandomycin, erythromycin, tilmicosin, tylosin, spiramycin, kitasamycin and josamycin residues in fugu and eel -- LC-MS-MS method
Status: Valid

Standard ID	USD	BUY PDF	Lead-Days	Standard Title (Description)	Status
GB/T 22964-2008	279	Add to Cart	3 days	Determination of lincomycin, oleandomycin, erythromycin, tilmicosin, tylosin, spiramycin, kitasamycin and josamycin residues in fugu and eel -- LC-MS-MS method	Valid

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Basic data

Standard ID: GB/T 22964-2008 (GB/T22964-2008)
Description (Translated English): Determination of lincomycin, oleandomycin, erythromycin, tilmicosin, tylosin, spiramycin, kitasamycin and josamycin residues in fugu and eel -- LC-MS-MS method
Sector / Industry: National Standard (Recommended)
Classification of Chinese Standard: X04
Classification of International Standard: 67.050
Word Count Estimation: 12,120
Date of Issue: 2008-12-31
Date of Implementation: 2009-05-01
Quoted Standard: GB/T 6379.1; GB/T 6379.2; GB/T 6682
Regulation (derived from): National Standard Approval Announcement 2008 No.26 (Total No.139)
Issuing agency(ies): General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China
Summary: This standard specifies the puffer fish and eels lincomycin, oleandomycin, erythromycin, tilmicosin, tylosin, spiramycin, Kitasamycin and josamycin residues in liquid chromatography-tandem mass spectrometry. This standard applies to puffer fish and eels lincomycin, oleandomycin, erythromycin, tilmicosin, tylosin, spiramycin, determination Kitasamycin and josamycin residues. This standard method detection limit: puffer fish in lincomycin, oleandomycin, erythromycin, tilmicosin, tylosin, spiramycin, Kitasamycin and josamycin are 2. 0��g/kg. Eel in lincomycin, erythromycin, tylosin, kitasamycin are 2. 0��g/kg, spiramycin, oleandomycin, Josamycin, tilmicosin were 5. 0��g/kg.

GB/T 22964-2008: Determination of lincomycin, oleandomycin, erythromycin, tilmicosin, tylosin, spiramycin, kitasamycin and josamycin residues in fugu and eel -- LC-MS-MS method

---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Determination of lincomycin, oleandomycin, erythromycin, tilmicosin, tylosin, spiramycin, kitasamycin and josamycin residues in fugu and eel. LC-MS-MS method ICS 67.050 X04 National Standards of People's Republic of China Puffer fish, eels lincomycin, oleandomycin, Erythromycin, tilmicosin, tylosin, spiramycin, Determination of neomycin guitar, josamycin residues Liquid chromatography - tandem mass spectrometry Posted 2009-05-01 2008-12-31 implementation Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China Standardization Administration of China released

Foreword

The Standard Appendix A, Appendix B is an informative annex. This standard is proposed and managed by the State Administration of Quality Supervision, Inspection and Quarantine. This standard was drafted. People's Republic of China Qinhuangdao Exit Inspection and Quarantine. The main drafters of this standard. Wang Fei, Wang Haiyang, Caoyan Zhong Jia light group, Zhang Jinjie, Shiyu Qiu, Pang Guofang. Puffer fish, eels lincomycin, oleandomycin, Erythromycin, tilmicosin, tylosin, spiramycin, Determination of neomycin guitar, josamycin residues Liquid chromatography - tandem mass spectrometry

1 Scope

This standard specifies the puffer fish and eel lincomycin, oleandomycin, erythromycin, tilmicosin, tylosin, spiramycin, guitar mildew Su and josamycin residues liquid chromatography - tandem mass spectrometry. This standard applies to puffer fish and eel lincomycin, oleandomycin, erythromycin, tilmicosin, tylosin, spiramycin, guitar mildew Su and josamycin residues determination. The standard method detection limit. puffer fish lincomycin, oleandomycin, erythromycin, tilmicosin, tylosin, spiramycin, Kyrgyzstan He neomycin and josamycin were 2.0μg/kg. Eel lincomycin, erythromycin, tylosin, neomycin guitar were 2.0μg/kg, Spiramycin, oleandomycin, josamycin, tilmicosin were 5.0μg/kg.

2 Normative references

The following documents contain provisions which, through reference in this standard and become the standard terms. For dated references, subsequent Amendments (not including errata content) or revisions do not apply to this standard, however, encourage the parties to the agreement are based on research Whether the latest versions of these documents. For undated reference documents, the latest versions apply to this standard. GB/T 6379.1 measurement methods and results of Accuracy (trueness and precision) - Part 1. General principles and definitions (GB/T 6379.1-2004, ISO 5725-1.1994, IDT) GB/T 6379.2 measurement methods and results of Accuracy (trueness and precision) - Part 2. Determine the standard measurement method to repeat Of the basic methods of reproduction (GB/T 6379.2-2004, ISO 5725-2.1994, IDT) GB/T 6682 analytical laboratory use specifications and test methods (GB/T 6682-2008, ISO 3696. 1987, MOD) Principle 3 Puffer fish and eels in lincomycin, oleandomycin, erythromycin, tilmicosin, tylosin, spiramycin, josamycin guitar and neomycin The residue was extracted with Tris buffer solution by OasisHLB SPE column 1) purification, methanol eluate was concentrated to volume liquid Tandem mass spectrometry, internal standard - chromatography. 1) OasisHLB SPE waters is the company's product trade name, this information is given for the convenience of users of this standard, does not mean Endorsement of the product. If other equivalent product has the same effect, you can use these equivalent products.

4 Reagents and materials

Unless otherwise indicated, the reagents used were of analytical grade. 4.1 Water. GB/T 6682, level. 4.2 Methanol. chromatographically pure. 4.3 ammonium acetate. 4.4 acetonitrile. chromatography. 4.5 hydrochloric acid. 4.6 Tris (tris). C4H11NO3. ......

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