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GB 474-2008 PDF English

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GB 474-2008: [GB/T 474-2008] Method for preparation of coal sample
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GB 474: Historical versions

Standard IDUSDBUY PDFDeliveryStandard Title (Description)Status
GB 474-2008135 Add to Cart Auto, 9 seconds. [GB/T 474-2008] Method for preparation of coal sample Valid
GB 474-1996319 Add to Cart 3 days Preparation of coal sample Obsolete
GB 474-1983RFQ ASK 3 days Methods for the preparation of coal sample Obsolete

Similar standards

GB/T 479   GB/T 480   GB 475   

GB 474-2008: [GB/T 474-2008] Method for preparation of coal sample

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D 21 NATIONAL STANDARD OF THE PEOPLE'S REPUBLIC OF CHINA GB474-2008 Replacing GB 474-1996 Method for Preparation of Coal Sample (ISO 18283.2006, Hard Coal and Coke-Manual Sampling, MOD) Issued on. DECEMBER 04, 2008 Implemented on. MAY 01, 2009 Jointly Issued by. General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China; Standardization Administration of the People's Republic of China. GB

Table of Contents

Foreword... I 1 Scope... 1 2 Normative References... 1 3 Terms and Definitions... 1 4 General and Precision of Sample Preparation... 2 4.1 General of Sample Preparation... 2 4.2 Sample Preparation Precision... 3 5 Apparatus... 3 6 Constitution of Sample... 4 7 Division... 5 7.1 General... 5 7.2 Minimum Mass of the Divided Sample... 5 7.3 Mechanical Methods... 6 7.4 Manual Methods... 12 8 Reduction... 15 9 Mixing... 16 10 Air-drying... 16 11 Preparation of Various Coal Samples... 17 11.1 Types of Coal Sample... 17 11.2 Moisture Sample of Coal... 17 11.3 General-analysis Test Sample of Coal... 19 11.4 Common Sample of Coal... 21 11.5 Size Analysis Sample of Coal... 22 11.6 Coal Samples for other Tests... 22 12 Reserve Sample... 23 Appendix A (Informative) Comparison of Chapter and Article Numbers between this Standard and ISO 18283.2006(E)... 24 Appendix B (Informative) Technical Differences between this Standard and ISO 18283. 2006(E) and the Reasons... 26 Appendix C (Normative) Verification for Precision of Sample Preparation and Assays and Bias Test... 28 Appendix D (Normative) Method for Flotation of Coal Sample... 30 IForeword Chapter 4, Chapter 6, Chapter 7, Chapter 10 and Chapter 11 of this standard are mandatory and the others are recommendatory. This standard is modified in relation to ISO 18283.2006(E) "Hard Coal and Coke-Manual Sampling" (English version). This standard was re-drafted mainly according to ISO 18283.2006(E). The list for comparison of chapter and article numbers between this standard and ISO 18283.2006(E) is given in Appendix A. In consideration of the national condition of China, this standard is subjected to some modifications in the adoption of ISO 18283.2006(E). Technical differences have already been incorporated into the text and marked with perpendicular single line at the margin of relevant clauses. The list for these technical differences and their reasons is given in Appendix B for reference. For convenient application, some editorial changes are made to ISO 18283.2006(E) as follows. ——"This international standard" is replaced by "this standard"; ——Introduction of ISO 18283.2006(E) is modified; ——Comma ",", which serves as decimal point in ISO standard, is replaced by ".". This standard replaces GB 474-1996 "Preparation of Coal Sample". Compared with GB 474-1996, main changes of this standard are as follows. ——Contents on general and precision of sample preparation (Chapter 3 of the original edition and Chapter 4 of this edition) are improved; ——Contents on sample constitution are added (Chapter 6 of this edition); ——"Coal sample greater than 25mm (particle size) shall not be divided before being crushed" is modified into "division may be carried out at any stage and the minimum mass of divided sample shall meet those specified in 7.2" (6.3 of the original edition and 7.1 of this edition); ——The minimum mass of divided sample at each particle size level is modified (6.7 of the original edition and 7.2 of this edition); ——Contents on mechanical dividing method and mechanical divider are added (7.3 of this edition); ——Two manual dividing methods are added (7.4.2 and 7.4.3 of this edition); ——Detailed explanations and specifications on division, reduction, mixing and air-drying etc. are added (Chapter 7, Chapter 8, Chapter 9 and Chapter 10 of this edition); ——Preparation methods of various coal samples are added (Chapter 11 of this edition); ——Operating requirements for extracting moisture sample of coal from common sample of coal with the nine-point picking out method are defined (11.4.1 of this edition). Appendix A and Appendix B of this standard are informative, Appendix C and Appendix D of this standard are normative. This national standard is proposed by the China National Coal Association. This standard is under the jurisdiction of the National Technical Committee on Coal Chemical Industry of Standardization Administration of China. Drafting organization of this standard. Coal Analysis and Test Laboratory of China Coal Research Institute (National Quality Supervision and Inspection Center for Coal). Chief drafting staff of this standard. Han Liting, Pi Zhongyuan, Duan Yunlong. The previous editions replaced by this standard are. ——GB 474-1964; GB 474-1975; GB 474-1983; GB 474-1996. 1NATIONAL STANDARD OF THE PEOPLE'S REPUBLIC OF CHINA Method for Preparation of Coal Sample

1 Scope

This standard specifies terms and definitions, sample constitution, reduction, mixing, division and air-drying for coal sample preparation, the preparation of various coal samples and reserve sample. This standard is applicable to lignite, bitumite and hard coal.

2 Normative References

The following documents contain provisions which, through reference in this standard, constitute provisions of this standard. For dated references, subsequent amendments to (excluding correction to), or revisions of, any of these publications do not apply. However, parties to agreements based on this standard are encouraged to investigate the possibility of applying the most recent editions of the standards indicated below. For undated references, its latest editions apply. GB/T 211 "Determination of Total Moisture in Coal" (GB/T 211-2007, ISO 589-2003, NEQ)

3 Terms and Definitions

Terms and definitions specified in GB 475 and those below are applicable to this standard. Method of sample division in which the mass retained is predetermined and independent of the mass of the divided sample.

4 General and Precision of Sample Preparation

According to formulae given in GB 475, and in continuous sampling, the fiducial probability, at 95%, of the precision estimated (absolute) value PL for the determination results of coal in one lot is shown in Formula (1).

5 Apparatus

The sample preparation room shall have cement floor. And the cement floor in the area for coning-and-mixing division shall also be paved with the steel plate with the thickness greater than 6mm. The room storing coal sample shall be free from heat source, highlighting or any chemicals.

6 Constitution of Sample

Individual increments are usually constituted to form a sample. a single sample may be constituted by combination of increments taken from a complete sampling unit or by constituting increments taken from individual parts of a sampling unit (see Figure 1). Under some circumstance, e.g. size analysis and bias test, the sample consists of one single increment.

7 Division

Division is the most important procedure for sample preparation, and the purpose is to reduce the sample amount. Division can be carried out mechanically or manually. Wherever possible, mechanical methods are preferred to manual methods to minimize human error. This method is only applied to extract total moisture sample. As shown in Figure 8, the sample shall be spread into circular shape with the thickness not greater than 3 times the nominal top size after being blended with coning and quartering method, then nine increments shall be taken from nine points shown in Figure 8 with the sampling scoop and operation similar to those used in flattened-heap method (7.4.2) so as to constitute into a total moisture sample.

8 Reduction

The discharge size of the crusher depends on the type of crusher, the dimension of crushing opening (jaw crusher and roll crusher) or the speed (hammer crusher and ball crusher).

9 Mixing

Mixing is carried out to make the coal sample uniform as much as possible. In theory, thorough mixing of a sample prior to its division reduces errors due to sample preparation In practice, this is not entirely true. For example, where the mechanical divider is adopted, mixing prior to division will not only be unnecessary to ensure the division precision but also result in loss of moisture. ......

Source: Above contents are excerpted from the full-copy PDF -- translated/reviewed by: www.ChineseStandard.net / Wayne Zheng et al.
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