GB 1886.347-2021 PDF English
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GB 1886.347-2021: National food safety standard - Food additives -4-amino-5,6-dimethylthieno(2,3-d)pyrimidin-2(1H)-one hydrochloride
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GB NATIONAL STANDARD OF THE PEOPLE’S REPUBLIC OF CHINA National food safety standard - Food additives - 4- amino-5,6-dimethylthieno(2,3-d)pyrimidin-2(1H)-one hydrochloride 啶-2(1H)-酮盐酸盐 ISSUED ON: FEBRUARY 22, 2021 IMPLEMENTED ON: AUGUST 22, 2021 Issued by: National Health Commission of PRC; State Administration for Market Regulation.
Table of Contents
1 Scope ... 3 2 Chemical name, molecular formula, structural formula, relative molecular mass ... 3 3 Technical requirements ... 3 Appendix A Determination of the content of 4-amino-5,6-dimethylthieno(2,3- d)pyrimidin-2(1H)-one hydrochloride ... 5 National food safety standard - Food additives - 4- amino-5,6-dimethylthieno(2,3-d)pyrimidin-2(1H)-one hydrochloride1 Scope
This standard is applicable to food additives, 4-amino-5,6-dimethylthieno(2,3- d)pyrimidin-2(1H)-one hydrochloride, which are produced through chemical reaction, by the raw materials of malononitrile, 3-mercapto-2-butanone, etc. 2 Chemical name, molecular formula, structural formula, relative molecular mass 2.1 Chemical name 4-amino-5,6-dimethylthieno(2,3-d)pyrimidin-2(1H)-one hydrochloride 2.2 Molecular formula C8H9N3OS·HCl 2.3 Structural formula 2.4 Relative molecular mass 231.7 (According to 2018 international relative atomic mass)3 Technical requirements
3.1 Sensory requirementsAppendix A
Determination of the content of 4-amino-5,6-dimethylthieno(2,3- d)pyrimidin-2(1H)-one hydrochloride A.1 Reagents and materials A.1.1 Trifluoroacetic acid: Purity ≥ 98%. A.1.1.1 The 0.1% trifluoroacetic acid solution: Pipette 1.00 mL of trifluoroacetic acid (A.1.1). Add it to a 1000 mL volumetric flask. Add water (A.1.3) to dilute it to the mark. Shake well. A.1.1.2 The 0.05% trifluoroacetic acid solution: Pipette 0.50 mL of trifluoroacetic acid (A.1.1). Add it to a 1000 mL volumetric flask. Add water (A.1.3) to dilute it to the mark. Shake well. A.1.2 Acetonitrile: Chromatographically pure. A.1.3 Water: Grade 1 water as specified in GB/T 6682. A.1.4 Control product of 4-amino-5,6-dimethylthieno(2,3-d)pyrimidin-2(1H)-one hydrochloride: Purity ≥ 99.0%. A.2 Instrument and equipment Ultra-high performance liquid chromatograph: Equipped with a diode array detector. A.3 Reference chromatographic conditions A.3.1 Chromatographic column: C18 liquid chromatographic column, which has a length of 100 mm, an inner diameter of 4.6 mm, a particle size of 3.5 μm; OR other equivalent chromatographic column. A.3.2 Mobile phase: Composed of 0.1% trifluoroacetic acid solution (A.1.1.1) and acetonitrile (A.1.2), in a volume ratio of 95:5. A.3.3 Column temperature: 30 °C. A.3.4 Flow rate: 1.0 mL/min. A.3.5 Injection volume: 1 μL. A.3.6 Detection wavelength: 245 nm. ......Source: Above contents are excerpted from the full-copy PDF -- translated/reviewed by: www.ChineseStandard.net / Wayne Zheng et al.
