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GB/T 3139-2005 PDF English

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GB/T 3139-2005: Fiber-reinforced plastics composites -- Determination of thermal conductivity
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GB/T 3139: Evolution and historical versions

Standard IDContents [version]USDSTEP2[PDF] deliveryName of Chinese StandardStatus
GB/T 3139-2005English115 Add to Cart 0-9 seconds. Auto-delivery Fiber-reinforced plastics composites -- Determination of thermal conductivity Valid
GB/T 3139-1982English199 Add to Cart 2 days Test method for thermal conductivity of glassfiber reinforced plastics Obsolete

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GB/T 3139-2005: Fiber-reinforced plastics composites -- Determination of thermal conductivity

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GB NATIONAL STANDARD OF THE PEOPLE’S REPUBLIC OF CHINA ICS 83.120 Q 23 Replacing GB/T 3139-1982 Fiber-reinforced plastics composites - Determination of thermal conductivity ISSUED ON: MAY 18, 2005 IMPLEMENTED ON: DECEMBER 01, 2005 Issued by: General Administration of Quality Supervision, Inspection and Quarantine; Standardization Administration of PRC.

Table of Contents

Foreword ... 3 1 Scope ... 4 2 Normative references ... 4 3 Terms and definitions ... 4 4 Test principle ... 5 5 Specimen ... 5 6 Test equipment ... 6 7 Test conditions ... 7 8 Test procedures ... 7 9 Calculation ... 8 10 Test report ... 9

Foreword

This standard replaces GB/T 3139-1982 "Test method for thermal conductivity of glass fiber reinforced plastics". Compared with GB/T 3139-1982, the main changes of this standard are as follows: - CHANGE the title from "Test method for thermal conductivity of glass fiber reinforced plastics" to "Fiber-reinforced plastics composites - Determination of thermal conductivity"; - ADD a chapter of normative references (see Chapter 2); - ADD a chapter of terms and definitions (see Chapter 3); - ADD a chapter of test principles (see Chapter 4); - CHANGE the unit of thermal conductivity coefficient from calories/cm • sec • °C to Watt per meter [Kelvin] [W/ (m • K)]; - MODIFY the sample pretreatment conditions (1.4 of the 1982 edition; 8.2 of this edition); - ADD a schematic diagram of the test equipment (see Figure 1). This standard was proposed by China Building Materials Industry Association. This standard shall be under the jurisdiction of the National Fiber Reinforced Plastics Standardization Technical Committee. Drafting organization of this standard: Beijing FRP Research and Design Institute. The main drafters of this standard: Zhao Guangfu, Zhang Liping, Ji Guodong. This standard was first published in July 1982 and revised for the first time in May 2005. Fiber-reinforced plastics composites - Determination of thermal conductivity

1 Scope

This standard specifies the test principles, specimens, test instruments, test conditions, test procedures, calculation results and test reports for determining the thermal conductivity of fiber-reinforced plastics by the guard hot plate method. This standard applies to the determination of the thermal conductivity of fiber- reinforced plastics.

2 Normative references

The provisions in following documents become the provisions of this Standard through reference in this Standard. For the dated references, the subsequent amendments (excluding corrections) or revisions do not apply to this Standard; however, parties who reach an agreement based on this Standard are encouraged to study if the latest versions of these documents are applicable. For undated references, the latest edition of the referenced document applies. GB/T 1446-2005 Fiber-reinforced plastics composites - The generals

3 Terms and definitions

The following terms and definitions apply to this standard. 3.1 Heat flow rate The heat passing through a surface per unit time. [GB/T 3102.4-1993, definition 4-7] 3.2 Density of heat flow rate The heat flow rate per unit area perpendicular to the direction of heat flow. [GB/T 4132-1996, definition 6.2.3] 3.3 Thermal conductivity A physical indicator of the thermal conductivity of a material. The value is equal to the density of heat flow rate divided by the negative temperature gradient. [GB/T 4132-1996, definition 6.2.5] 3.4 Mean temperature In the steady state, the arithmetic average of the high-temperature surface’s temperature and low-temperature surface’s temperature of the specimen; it can also be referred to as the average temperature for short. 3.5 Temperature difference In the steady state, the difference between the high-temperature surface’s temperature and the low-temperature surface’s temperature of the specimen.

4 Test principle

The guard hot plate method is in a steady state to make a one-way heat flow flows vertically through a plate-shaped specimen; by measuring the one- dimensional constant heat flow in the specified heat transfer area and the temperature difference between the cold and hot surfaces of the specimen, it can calculate the thermal conductivity of the specimen.

5 Specimen

5.1 The specimen preparation shall be in accordance with the provisions of Chapter 4 of GB/T 1446-2005. 5.2 The specimen size shall meet the following requirements: 5.2.1 The side length or diameter of the specimen shall be equal to the heating plate, usually 100 mm. 5.2.2 The thickness of the specimen is at least 5 mm; the maximum is not more than 1/10 of its side length or diameter. 5.3 The surface of the specimen shall be smooth; the surface unevenness shall not be greater than 0.50 mm/m; the two sides of the specimens shall be parallel. 5.4 Each group of specimens shall not be less than 3 pieces.

6 Test equipment

The test equipment is as shown in Figure 1. 1 - Cooling water jacket; 2 - Cold plate; 3 - Specimen; 4 - Main heating plate; 5 - Thermal insulation materials; 6 - Guard heating plate; 7 - Thermal insulation materials; 8 - Bottom heating plate. Figure 1 -- Schematic diagram of test equipment 6.1 Heating plate The heating plate is composed of a main heating plate, a guard heating plate with a certain gap surrounding the main heating plate, a bottom heating plate. Each heating plate has an independent heater and a surface plate. 6.1.1 The side length or diameter of the heating plate is generally 100 mm; the width of the guard heating plate is 1/4 of the side length or diameter of the heating plate, with proper insulation measures. If there are special measures to ensure that the measurement error of the thermal conductivity coefficient is within 8%, this value can also be changed appropriately. 6.1.2 The temperature difference at each point on the surface of the heating plate is not more than 2% of the temperature difference between the two sides of the specimen under the steady state, meanwhile the maximum shall not be Water inlet Water outlet more than 0.5 °C. The temperature difference at each point on the surface of the guard heating plate shall not be more than 5% of the temperature difference between the two sides of the specimen in the steady state; meanwhile the maximum shall not be more than 1 °C. 6.1.3 The unevenness of the heating plate surface shall not be greater than 0.25 mm/m. 6.2 Cooling plate The cooling plate shall have an internal threaded two-way liquid loop; the size of the cooling plate and the surface state of the contact specimen are the same as the heating plate, but the cooling plate is not spaced. 6.3 Temperature and power measurement accuracy The temperature measurement shall be accurate to 1% of the temperature difference between the two sides of the specimen in the steady state; but the maximum shall not be greater than 0.5 °C. Measure the power of the main heating plate, which shall be accurate to 1%.

7 Test conditions

7.1 Test environment The test environmental conditions shall comply with the provisions of Chapter 3 of GB/T 1446-2005. 7.2 Specimen temperature and temperature difference The temperature of the heating plate generally does not exceed 260 °C; the temperature of the cold plate rises from room temperature to the required temperature. The temperature difference between the two sides of the specimen is not less than 10 °C.

8 Test procedures

8.1 Visual inspection of specimen The appearance inspection of the specimen is in accordance with the provisions of 4.2 in GB/T 1446-2005; the unevenness of the specimen surface is inspected with a knife-shaped flat ruler. 8.2 Conditioning of specimen state The state of the specimen is conditioned according to the provisions of 4.4 in GB/T 1446-2005, or according to the technical requirements of the product. 8.3 Measurement of specimen thickness Measure the thickness of the specimen at least 4 times, accurate to 0.01 mm; take the arithmetic average. 8.4 Specimen installation When installing the specimen, pay attention to eliminate the air interlayer and apply a certain pressure to the specimen. 8.5 Conditioning balance Adjust the temperature difference between the main heating plate and the guard heating plate and between the main heating plate and the bottom heating plate to achieve a balance. The test error of thermal conductivity coefficient as caused by the imbalance shall not exceed 1%. 8.6 Measurement After reaching a steady state, measure the power of the main heating plate and the temperature difference between the two sides of the specimen, then the test can be ended. The so-called steady state means that the fluctuation of surface temperature of the specimen within 30 min is not more than 1% of the temperature difference between the two sides of the specimen under the condition that the power of the main heating plate remains unchanged; meanwhile the maximum shall not be greater than 1 °C.

9 Calculation

The thermal conductivity coefficient is calculated according to formula (1), taking 2 significant figures. Where: λ - Thermal conductivity coefficient, in watts per meter Kelvin [W/ (m • K)]; Φ - The power when the main heating plate is stable, in watts (W); d - The thickness of specimen, in meters (m); A - The calculated area of the main heating plate (for a certain test device, the value is a fixed value), in square meters (m2); t1 - The high temperature of the specimen, in degrees Celsius (°C); t2 -The low temperature of the specimen, in degrees Celsius (°C). Calculate the thermal conductivity coefficient of each specimen; calculate the average value of each group of specimens.

10 Test report

According to Chapter 7 of GB/T 1446-2005, the test results only need to provide the thermal conductivity coefficient of each specimen and the arithmetic mean value of each group of specimens; indicate the high-temperature surface’s temperature of the specimen or the average temperature of the specimen. __________ END __________ ......
Source: Above contents are excerpted from the full-copy PDF -- translated/reviewed by: www.ChineseStandard.net / Wayne Zheng et al.


      

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