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Basic data
| Standard ID | GA/T 1908-2021 (GA/T1908-2021) |
| Description (Translated English) | Thick solid wood core plywood |
| Sector / Industry | Public Security (Police) Industry Standard (Recommended) |
| Classification of Chinese Standard | B70 |
| Classification of International Standard | 13.310 |
| Word Count Estimation | 12,167 |
| Date of Issue | 2021-10-14 |
| Date of Implementation | 2022-05-01 |
| Issuing agency(ies) | Ministry of Public Security |
GA/T 1908-2021: Thick solid wood core plywood
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ICS 13.310
CCSA92
People's Republic of China Public Security Industry Standards
Triptolide A etc. in Forensic Science Biological Samples
Liquid Chromatography-Mass Spectrometry for Detecting Four Kinds of Tripterygium Toxins
Released on 10-14-2021
2022-05-01 implementation
Released by the Ministry of Public Security of the People's Republic of China
foreword
This document is in accordance with the provisions of GB/T 1.1-2020 "Guidelines for Standardization Work Part 1.Structure and Drafting Rules for Standardization Documents"
drafting.
Please note that some contents of this document may refer to patents. The issuing agency of this document assumes no responsibility for identifying patents.
This document was proposed by the National Criminal Technology Standardization Technical Committee Toxic Analysis Sub-Technical Committee (SAC/TC179/SC1) and submitted
Focus on.
This document was drafted by. Physical Evidence Appraisal Center of the Ministry of Public Security, Hangzhou Public Security Judicial Appraisal Center, Criminal Investigation Directorate of Public Security Department of Guangxi Zhuang Autonomous Region
Team, Yunnan Provincial Public Security Bureau.
The main drafters of this document. Wang Fanglin, Luan Yujing, Ying Jianbo, Huang Kejian, Li Hong.
Triptolide A etc. in Forensic Science Biological Samples
Liquid Chromatography-Mass Spectrometry for Detecting Four Kinds of Tripterygium Toxins
1 Scope
This document specifies the forensic science biological samples (blood, urine, liver, kidney, stomach and stomach contents) of triptolide A, triptolide
Liquid chromatography-mass spectrometry (LC-MS/MS) test method for ketone, triptolide and tripterine.
This document is applicable to triptolide A and triptolide in forensic science biological samples (blood, urine, liver, kidney, stomach and stomach contents)
Qualitative and quantitative analysis of ketone, triptolide and tripterine. Other test materials can be used as reference.
2 Normative references
The contents of the following documents constitute the essential provisions of this document through normative references in the text. Among them, dated references
For documents, only the version corresponding to the date is applicable to this document; for undated reference documents, the latest version (including all amendments) is applicable to
this document.
GB/T 6682 Analytical laboratory water specifications and test methods
GA/T 122 Toxicological Analysis Terminology
3 Terms and Definitions
The terms and definitions defined in GA/T 122 apply to this document.
4 principles
The blank sample and the added sample were used as controls, and the biological samples were extracted, purified and concentrated according to the requirements of parallel operations, and liquid chromatography was used to
Spectrometry-mass spectrometry detection, based on retention time, mass spectrometry characteristic ion pair and ion pair abundance ratio as the basis for qualitative judgment; based on the peak area, the
Quantitative analysis was performed by external standard method.
5 Reagents and Materials
5.1 Reagents
The experimental water should meet the first-class water specified in GB/T 6682.Unless otherwise stated, all reagents used in the analysis were of analytical grade.
Reagents include.
a) Methanol (chromatographically pure);
b) Acetonitrile (chromatographically pure);
c) ethyl acetate;
d) 1% sodium hydroxide solution. weigh 1.0g of sodium hydroxide, add a certain amount of water to dissolve and dilute to 100mL;
e) Phosphate buffer (pH 6.0). Weigh 8.34 g of sodium dihydrogen phosphate and 0.87 g of disodium hydrogen phosphate respectively, add a certain amount of water
Dissolve and dilute to 1000mL;
...
