GB/T 23607-2009 English PDF

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GB/T 23607-2009: Methods for chemical analysis of copper anode mud -- Determination of arsenic, bismuth, iron, nickel, lead, antimony, selenium and tellurium content -- Inductively coupled plasma-atomic emission spectrometry
Status: Valid

Standard ID	USD	BUY PDF	Lead-Days	Standard Title (Description)	Status
GB/T 23607-2009	189	Add to Cart	3 days	Methods for chemical analysis of copper anode mud -- Determination of arsenic, bismuth, iron, nickel, lead, antimony, selenium and tellurium content -- Inductively coupled plasma-atomic emission spectrometry	Valid

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Basic data

Standard ID: GB/T 23607-2009 (GB/T23607-2009)
Description (Translated English): Methods for chemical analysis of copper anode mud -- Determination of arsenic, bismuth, iron, nickel, lead, antimony, selenium and tellurium content -- Inductively coupled plasma-atomic emission spectrometry
Sector / Industry: National Standard (Recommended)
Classification of Chinese Standard: H13
Classification of International Standard: 77.120.01
Word Count Estimation: 8,865
Date of Issue: 2009-04-15
Date of Implementation: 2010-02-01
Regulation (derived from): National Standard Approval Announcement 2009 No.5 (Total No.145)
Issuing agency(ies): General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China
Summary: This standard specifies the ICP-AES method for the determination of arsenic in copper anode mud, bismuth, iron, Nickel, tellurium content of the method, selenium, antimony, lead. This standard applies to copper anode mud arsenic, bismuth, iron, Nickel, determination of tellurium, antimony, , selenium and lead. Measuring range in Table 1.

GB/T 23607-2009: Methods for chemical analysis of copper anode mud -- Determination of arsenic, bismuth, iron, nickel, lead, antimony, selenium and tellurium content -- Inductively coupled plasma-atomic emission spectrometry

---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Methods for chemical analysis of copper anode mud. Determination of arsenic, bismuth, iron, nickel, lead, antimony, selenium and tellurium content. Inductively coupled plasma-atomic emission spectrometry ICS 77.120.01 H13 National Standards of People's Republic of China Methods for chemical analysis of copper anode slime Determination of arsenic, bismuth, iron, nickel, lead, antimony, selenium, tellurium quantity Inductively coupled plasma atomic emission spectrometry Posted 2009-04-15 2010-02-01 implementation Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China Standardization Administration of China released

Foreword

Appendix A of this standard is an informative annex. The standard proposed by China Nonferrous Metals Industry Association. This standard Nonferrous Metals by the National Standardization Technical Committee. This standard by Tongling Nonferrous Metals Group Holdings Co., Ltd. is responsible for drafting. This standard by the Northern Copper Company Limited Houma Smelter, Jiangxi Copper Corporation, Hubei Daye Nonferrous Metals Company, Yunnan Copper Industry Co., Ltd. participated in the drafting. The main drafters of this standard. Liqin Mei, Jiang Lihong, from Shao and Wang real rich, He Xiumei, will Bai, Yang Hongsheng, Yuangong Qi, Shi Xiaoying, Zheng Wenying. Methods for chemical analysis of copper anode slime Determination of arsenic, bismuth, iron, nickel, lead, antimony, selenium, tellurium quantity Inductively coupled plasma atomic emission spectrometry

1 Scope

This standard specifies the method for the determination by ICP-AES copper anode mud arsenic, bismuth, iron, nickel, lead, antimony, selenium, tellurium content. This standard applies to arsenic, bismuth, iron, nickel, lead, antimony, selenium, tellurium determination of copper anode mud. Determination of the range in Table 1. Table 1 Measuring range As Bi Fe Ni element Content (mass fraction) /% 0.50 to 5.00 0.20 to 4.00 0.05 to 0.50 0.10 to 4.00 Element Pb Sb Se Te Content (mass fraction) /% 1.00 10.0 0.50 8.0 0.50 4.00 0.20 4.00

2 Method summary

Sample by aqua regia and saturated ammonium hydrogen exploded, some acidity control test solution, using inductively coupled plasma emission spectrometry can be measured directly Fixed copper anode slime As, Bi, Fe, Ni, Pb, Sb, Se, Te impurities.

3 Reagents

Unless otherwise indicated in the analysis using only recognized as analytical grade reagents and distilled or deionized water or equivalent purity. 3.1 hydrochloride (ρ1.19g/mL). Nitrate 3.2 (ρ1.42g/mL). 3.3 nitric acid (1 + 1). 3.4 aqua regia. nitric acid + hydrochloric acid (3 + 1). 3.5 tartaric acid solution.200g/L. 3.6 saturated solution of ammonium hydrogen fluoride. 3.7 pure substance. the mass fraction of not less than 99.99% pure bismuth, iron, pure nickel, pure lead, tellurium pure, pure antimony, pure selenium. 3.8 Standard bismuth stock solution (Bi5.0mg/mL). Weigh 1.0000g of pure bismuth (3.7) in the 200mL beaker; 30mL of nitric acid was added (3.3), cover sheet pan, heat until completely dissolved, remove nitrogen oxides boil, remove the cooled and transferred to 200mL volumetric flask and dilute to the mark Degree, and mix. 3.9 iron standard stock solution (Fe0.50mg/mL). Weigh 0.2500g pure iron (3.7) in the 200mL beaker; nitric acid was added 30mL (3.3), cover sheet pan, heat until completely dissolved, remove nitrogen oxides boil, remove the cooled and transferred to 500mL volumetric flask and dilute to the mark Degree, and mix. 3.10 Nickel standard stock solution (Ni5.0mg/mL). Weigh 1.0000g pure nickel (3.7); in 200mL beaker; nitrate was added 30mL Acid (3.3), cover sheet pan, heat until completely dissolved, remove nitrogen oxides boil, remove the cooled and transferred to 200mL volumetric flask and dilute to Volume, and mix. 3.11 lead standard stock solution (Pb15.0mg/mL). Weigh 3.0000g pure lead (3.7); in 200mL beaker; added 50mL Nitric acid (3.3), cover sheet pan, heat until completely dissolved, remove nitrogen oxides boil, remove the cooled and transferred to 200mL volumetric flask and diluted To the mark, and mix. ......

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