GB/T 11134: Historical versions
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| GB/T 11134-2025 | 209 |
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Determination of kauri-butanol value of hydrocarbon solvents
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| GB 11134-1989 | RFQ |
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Hydrocarbon solvents--Determination of kauri-butanol value
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| GB/T 11134-1989 | 139 |
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Hydrocarbon solvents. Determination of kauri-butanol value
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Basic dataStandard ID: GB/T 11134-2025 (GB/T11134-2025) Description (Translated English): Determination of kauri-butanol value of hydrocarbon solvents Sector / Industry: National Standard (Recommended) Classification of Chinese Standard: E30 Classification of International Standard: 75.080 Word Count Estimation: 10,127 Date of Issue: 2025-10-05 Date of Implementation: 2026-05-01 Older Standard (superseded by this standard): GB/T 11134-1989 Issuing agency(ies): State Administration for Market Regulation and Standardization Administration of China
GB/T 11134-2025: Determination of kauri-butanol value of hydrocarbon solvents---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
ICS 75.080
CCSE30
National Standards of the People's Republic of China
Replaces GB/T 11134-1989
Determination of Butanol Value of Pinecone Resin as a Hydrocarbon Solvent
Published on 2025-10-05
Implemented on May 1, 2026
State Administration for Market Regulation
The State Administration for Standardization issued a statement.
Foreword
This document complies with the provisions of GB/T 1.1-2020 "Standardization Work Guidelines Part 1.Structure and Drafting Rules of Standardization Documents".
Drafting.
This document supersedes GB/T 11134-1989 "Determination of Butanol Value of Pinecone Resin as a Hydrocarbon Solvent" and is consistent with GB/T 11134-1989.
Compared to previous versions, aside from structural adjustments and editorial changes, the main technical changes are as follows.
a) The scope of application has been changed (see Chapter 1, Chapter 1 of the 1989 edition);
b) A definition for "Shellspine resin butanol value" has been added (see Chapter 3);
c) The description of the method summary has been revised (see Chapter 4, Chapter 3 of the 1989 edition);
d) Technical requirements for balances, electromagnetic stirrers, Buchner funnels, and thermometers have been added (see 5.2, 5.3, 5.4, and 5.10);
e) The technical requirements for turbidity observation cards have been changed (see 5.12, 5.6 of the 1989 edition);
f) Added pine resin-n-butanol solution and n-heptane-toluene mixed solution (see Chapter 6);
g) The chapter on "Preparation" has been deleted (see Chapter 7 in the 1989 edition);
h) A new chapter on "Sampling" has been added (see Chapter 7);
i) The test temperature was changed from "25℃±1℃" to "25℃±5℃" (see Chapter 8, Chapter 8 of the 1989 edition);
j) The volume correction formula for the solvent in the burette has been removed (see 9.2 in the 1989 edition);
k) The terminology for precision has been revised (see Chapter 10, Chapter 10 of the 1989 edition);
l) Added report content such as sample name and number (see Chapter 11).
Please note that some content in this document may involve patents. The issuing organization of this document assumes no responsibility for identifying patents.
This document was proposed and is under the jurisdiction of the National Technical Committee on Standardization of Petroleum Products and Lubricants (SAC/TC280).
This document was drafted by. Lanzhou Petrochemical Branch of China National Petroleum Corporation and Huizhou Municipal Petroleum Product Quality Supervision Bureau of Guangdong Province.
Inspection Center, Sinopec Petrochemical Research Institute Co., Ltd., Shandong Provincial Institute of Product Quality Inspection, Liaoning Provincial Institute of Product Quality Supervision and Inspection
The hospital.
The main drafters of this document are. Zhu Dongmei, Pei Xinjie, Song Dan, Leng Haoze, Liu Huiqin, Xu Hualing, Zhao Yue, Dai Yingjuan, Wang Ting, and Zhao Zhenhai.
Dong Hailong, Wang Shuo, Chen Panpan, Feng Lizu, Xue Hua.
This document was first published in 1989, and this is its first revision.
Determination of Butanol Value of Pinecone Resin as a Hydrocarbon Solvent
Warning---Personnel using this document should have practical experience in formal laboratory work. The use of this document may involve certain hazardous activities.
Regarding the materials, equipment, and operations, this document does not specify all potential safety issues. Users are responsible for taking appropriate safety, health, and environmental precautions.
Measures shall be taken to ensure compliance with relevant national laws and regulations.
1 Scope
This document specifies a method for determining the relative solubility of hydrocarbon solvents used in paints, varnishes and related products.
This document applies to the determination of the butanol value of pine resin in hydrocarbon solvents with an initial boiling point greater than 40℃ and a dry point less than 300℃. Its determination range...
The range is 30 to 90; this document also applies to samples with butanol values outside this range, but the precision is not determined.
2 Normative references
The contents of the following documents, through normative references within the text, constitute essential provisions of this document. Dated citations are not included.
For references to documents, only the version corresponding to that date applies to this document; for undated references, the latest version (including all amendments) applies.
This document.
GB/T 4756 Manual Sampling Method for Petroleum Liquids
GB/T 6680 General Rules for Sampling of Liquid Chemical Products
GB/T 8170 Rules for rounding off numerical values and the representation and determination of limiting values
GB/T 24988 Copy paper
3 Terms and Definitions
The following terms and definitions apply to this document.
3.1
Kauri-butanol value (Kauri-butanol value)
At 25°C, a hydrocarbon solvent was added to 20g of pine resin-n-butanol solution, and the amount of hydrocarbon solvent consumed when the specified turbidity was achieved was recorded.
The number of milliliters is a value calculated using a formula.
Note. The pine resin-n-butanol solution was standardized using a toluene and n-heptane-toluene mixture (75% n-heptane and 25% toluene by volume) as a reference.
The value of toluene is set at 105, and the value of the n-heptane-toluene mixed solution is set at 40.
4.Method Overview
At 25℃, a mixed solution of toluene (with a concentration of 105) and 75% n-heptane (with a concentration of 40) and 25% toluene was used to treat 20g of seashells.
The pine resin-n-butanol solution was standardized, and the concentration of the pine resin-n-butanol solution was adjusted to a suitable level. Under the same conditions, the sample was titrated.
For a pine resin-n-butanol solution, record the number of milliliters of sample required to produce the specified turbidity. Calculate the pine resin butanol content of the sample using a formula.
Alcohol value.
5.Instruments and Materials
5.1 Water bath. capable of maintaining a constant temperature of 25℃±5℃. Other environments capable of maintaining a constant temperature of 25℃±5℃ may also be used.
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