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YS/T 869-2013 English PDF

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YS/T 869-2013: Chemical analysis of 4A-Zeolite. X-ray fluorescence spectrometric method
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YS/T 869-2013English189 Add to Cart 3 days [Need to translate] Chemical analysis of 4A-Zeolite. X-ray fluorescence spectrometric method Valid YS/T 869-2013

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Basic data

Standard ID YS/T 869-2013 (YS/T869-2013)
Description (Translated English) Chemical analysis of 4A-Zeolite. X-ray fluorescence spectrometric method
Sector / Industry Nonferrous Metallurgy Industry Standard (Recommended)
Classification of Chinese Standard H12
Classification of International Standard 77.150.10
Word Count Estimation 7,710
Regulation (derived from) Ministry of Industry and Information Technology Bulletin 2013 No. 23; industry standard filing Notice 2013 No. 7 (No. 163 overall)
Issuing agency(ies) Ministry of Industry and Information Technology
Summary This standard specifies the chemical composition of 4A Zeolite X-ray fluorescence analysis. This standard applies to the determination of the chemical composition of 4A Zeolite SiO2, Al2O3, Na2O content.

YS/T 869-2013: Chemical analysis of 4A-Zeolite. X-ray fluorescence spectrometric method

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Chemical analysis of 4A-Zeolite. X-ray fluorescence spectrometric method ICS 77.150.10 H12 People's Republic of China Nonferrous Metals Industry Standard 4A Zeolite Chemical Component Analysis X-ray fluorescence method Issued on. 2013-04-25 2013-09-01 implementation Ministry of Industry and Information Technology of the People's Republic of China released

Foreword

This standard was drafted in accordance with GB/T 1.1-2009 given rules. This standard by the national non-ferrous metals Standardization Technical Committee (SAC/TC243) centralized. This standard is drafted by. Aluminum Corporation of China Shandong Branch. Participated in the drafting of this standard. Aluminum Corporation of China Zhengzhou Research Institute, Aluminum Corporation of China Guangxi Branch. The main drafters of this standard. Qi Yanli, Li Linhai, Zhong Yi Mei, Zhang Aifen, Deng Wenjun, Chen Lijun, Xu good text, Mahui Xia, Liu Jing, Shuai. 4A Zeolite Chemical Component Analysis X-ray fluorescence method

1 Scope

This standard specifies the chemical composition of 4A Zeolite X-ray fluorescence analysis. This standard applies to the determination of the chemical composition of 4A Zeolite SiO2, Al2O3, Na2O content. Determination of the range in Table 1. Table 1 Component SiO2 Al2O3 Na2O Mass fraction /% ~ 31.00 33.00 27.00 - 29.00 17.00 - 19.00

2 principle of the method

After burning the sample 2h at 1000 ℃, dry basis molten lithium mixed solvent of anhydrous lithium tetraborate and metaborate, to eliminate the effect of mineral and Size effect, and cast for X-ray fluorescence spectrometer to measure the shape of the glass, glass measuring the fluorescent X-ray intensity measured elements degree. In each series of standard reference material formulated samples, establish a standard curve elements in its X-ray fluorescence intensity between. Sample Measurement According to series of standards to correct, on the basis of loss on ignition and to calculate the actual content of the sample.

3 Reagents

3.1 mixed solvent (65Li2B4O7 25LiBO2 10LiF). AR. 3.2 ammonium iodide solution (500g/L). 3.3 anhydrous sodium carbonate (reference material). 3.4 alumina (spectroscopically pure). 3.5 Silica (spectroscopically pure).

4 Instrument

Platinum 4.1 - gold alloy crucible (95% Pt 5% Au). Note. The sample in the crucible directly after melt molding, the bottom surface of the inner wall of the crucible requires smooth. Recommended Specifications. upper inner diameter 45mm, the lower end of the inner diameter of 33mm, high 25mm. Melting furnace-like 4.2. Maximum temperature 1300 ℃, control accuracy ± 15 ℃. 4.3 X-ray fluorescence spectrum analyzer. wavelength dispersion. 4.4 high-temperature furnace. can be controlled at 1000 ℃ ± 10 ℃, the furnace can ensure air flow. 4.5 porcelain crucible. 30mL. 4.6 dryer. filled within silicone.

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