HOME Cart(0) Quotation About-Us Policy PDFs Standard-List
www.ChineseStandard.net Database: 189759 (19 Oct 2025)

GB/T 15076.13-2017 English PDF

US$109.00 · In stock
Delivery: <= 3 days. True-PDF full-copy in English will be manually translated and delivered via email.
GB/T 15076.13-2017: Methods for chemical analysis of tantalum and niobium -- Part 13: Determination of nitrogen content -- Inert gas fusion thermal conductivity method
Status: Valid

GB/T 15076.13: Evolution and historical versions

Standard ID	Contents [version]	USD	STEP2	[PDF] delivered in	Standard Title (Description)	Status	PDF
GB/T 15076.13-2017	English	109	Add to Cart	3 days [Need to translate]	Methods for chemical analysis of tantalum and niobium -- Part 13: Determination of nitrogen content -- Inert gas fusion thermal conductivity method	Valid	GB/T 15076.13-2017
GB/T 15076.13-1994	English	239	Add to Cart	2 days [Need to translate]	Methods for chemical analysis of tantalum and niobium. Determination of nitrogen content in tantalum	Obsolete	GB/T 15076.13-1994

PDF similar to GB/T 15076.13-2017

Standard similar to GB/T 15076.13-2017

GB/T 14635 GB/T 15076.3 GB/T 15076.1 GB/T 15076.6 GB/T 15076.7 GB/T 15076.4

Basic data

Standard ID	GB/T 15076.13-2017 (GB/T15076.13-2017)
Description (Translated English)	Methods for chemical analysis of tantalum and niobium -- Part 13: Determination of nitrogen content -- Inert gas fusion thermal conductivity method
Sector / Industry	National Standard (Recommended)
Classification of Chinese Standard	H14
Classification of International Standard	77.120.99
Word Count Estimation	5,574
Date of Issue	2017-10-14
Date of Implementation	2018-08-01
Older Standard (superseded by this standard)	GB/T 15076.13-1994
Regulation (derived from)	National Standard Announcement 2017 No. 26
Issuing agency(ies)	General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China
Summary	This standard specifies the method for the determination of nitrogen in thorium and yttrium. This standard applies to the determination of nitrogen in cesium and lanthanum. Measurement range: 0.0005% to 0.400%.

GB/T 15076.13-2017: Methods for chemical analysis of tantalum and niobium -- Part 13: Determination of nitrogen content -- Inert gas fusion thermal conductivity method

---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Methods for chemical analysis of tantalum and niobium.Part 13. Determination of nitrogen content.Inert gas fusion thermal conductivity method ICS 77.120.99 H14 National Standards of People's Republic of China Replacing GB/T 15076.13-1994 Chemical analysis method Part 13. Determination of nitrogen content Inert gas fusion heat conduction method Part 13. Determinationofnitrogencontent- Published on October 10,.2017 2018-08-01 Implementation General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China China National Standardization Administration released

Foreword

GB/T 15076 "Chemical Analysis Method for Poria" is divided into 16 parts. --- Part 1 . Determination of germanium content in helium inductively coupled plasma atomic emission spectrometry ; --- Part 2. determination of yttrium in ytterbium extraction, chromatographic separation - DSPCF spectrophotometric method and chromatographic separation gravimetric method; -- Part 3 . Determination of copper content Carbon tetrachloride extraction Separation of sodium diethyldithiocarbamate spectrophotometry ; --- Part 4. Determination of iron content 1,10-Phenanthroline spectrophotometric method; Part 5 . Determination of molybdenum content and tungsten content -- Inductively coupled plasma atomic emission spectrometry ; ---Part 6. Determination of silicon content in cesium - Anion exchange separation - Molybdenum blue spectrophotometric method and separation with 4-methyl-pentanone-[2] Molybdenum blue spectrophotometry; --- Part 7. Determination of phosphorus content in barium 4-Methyl-pentanone-[2] Extraction separation Phosphorus-molybdenum blue spectrophotometric method; --- Part 8. Determination of carbon content and sulfur content - High-frequency combustion infrared absorption method; --- Part 9. Determination of iron, chromium, nickel, manganese, titanium, aluminum, copper, tin, lead, and zirconium content in sputum by direct current arc atomic emission spectrometry; --- Part 10. Determination of iron, nickel, chromium, titanium, zirconium, aluminum, and manganese in rhodium by DC arc carrier fractionation atomic emission spectrometry; --- Part 11. Determination of arsenic, antimony, lead, tin and antimony content in germanium by DC arc carrier fractionation atomic emission spectrometry; Part 12 . Determination of phosphorus content in barium Ethyl acetate extraction separation of phosphomolybdic blue spectrophotometric method ; --- Part 13. Determination of nitrogen content Inert gas fusion thermal conductivity method; --- Part 14. Determination of oxygen content Inert gas fusion infrared absorption method; Part 15 . Determination of hydrogen content ; Inert gas fusion thermal conductivity method ; --- Part 16. Determination of sodium and potassium - Flame atomic absorption spectrometric method. This part is part 13 of GB/T 15076. This section was drafted in accordance with the rules given in GB/T 1.1-2009. This Part replaces GB/T 15076.13-1994 "Determination of nitrogen in cesium by chemical analysis methods". This section and GB/T 15076.13- Compared with.1994, the main technical content changes as follows. --- Changed the method of determination, changed from spectrophotometry to inert gas fusion thermal conductivity method; --- Expanded the measurement range, the measurement range was revised from 0.002% to 0.2% to 0.0005% to 0.400%; --- Added precision and test report terms. This part was proposed by China Nonferrous Metals Industry Association. This part is under the jurisdiction of the National Non-ferrous Metals Standardization Technical Committee (SAC/TC243). This section was drafted by. Ningxia Dongfang Fuye Co., Ltd., Baoti Group Co., Ltd., Western Metal Materials Co., Ltd. Jiang Nonferrous Metal Smelting Company, Northwest Institute of Rare Metal Materials. The main drafters of this section. Zhang Junfeng, Li Jian, Yang Junhong, Yan Wenxia, Wang Juxiang, Kang Qiong, Li Hui, Tong Tongde, Liu Rui, Wang Zhidao, Lu Siyu, Gao Yaming and Chen Hong. The previous versions of the standards replaced in this section were. --- GB/T 15076.13-1994. Chemical analysis method Part 13. Determination of nitrogen content Inert gas fusion heat conduction method

1 Scope

This part of GB/T 15076 specifies the method for the determination of nitrogen in thorium and thorium. This section applies to the determination of nitrogen in cesium and lanthanum. Measurement range. 0.0005% to 0.400%.

2 Method summary

The sample and the flux are added to a high-purity graphite crucible and heated and melted under the protection of an inert gas (helium gas), in which oxygen is combined with carbon in the crucible. A mixture of carbon monoxide and carbon dioxide is formed, and nitrogen is released as nitrogen. Carbon monoxide is partially oxidized to carbon dioxide, one of the gases The carbon oxides and carbon dioxide are absorbed and separated, and the remaining nitrogen enters the thermal conductivity detector with a carrier gas (helium gas). The output signal of the detector is calculated. The nitrogen content is calculated based on the sample mass.

3 Materials

3.1 Helium. The volume fraction is not less than 99.995%. 3.2 Argon/nitrogen (power gas). The volume fraction is not less than 99.9%. 3.3 High purity nickel foil/nickel capsule. wN≤0.0002%, nickel foil thickness≤0.10mm. 3.4 High-purity graphite crucible. 3.5 Reference material/standard sample. The corresponding reference material should be selected. In principle, the chemical composition of the reference material and the analytical sample is similar.

4 Instrument devices

Inert gas fusion thermal conductivity detection system, including an electrode furnace, carrier gas purification and analysis gas flow conversion system, nitrogen thermal conductivity detector, computer And software control system.

5 samples

5.1 The particle size of tantalum powder is less than 180μm; tantalum powder should be vacuum dried in advance at 80°C~150°C for 4 hours, cooled to room temperature, and used with composite aluminum foil bag. Empty packaging. 5.2 The powder sample is loaded into a pre-treated and weighed high-purity nickel foil/nickel capsule (3.3) and sealed to remove the air in the high-purity nickel foil/nickel capsule (3.3). The total mass of the sample and the high-purity nickel foil/nickel capsule (3.3) was again weighed to obtain the difference in the mass of the sample. The sample should be analyzed daily. 5.3 The bulk sample was removed from the epidermis and cut from the sample core and processed into pellets with a mass no greater than 0.03 g, weighed, and loaded with high-purity nickel foil/nickel Bags, seals, and purify air in high-purity nickel foil/nickel capsules (3.3). 5.4 The treated sample should not be contaminated prior to analysis and testing. Clean tweezers should be used during the test.

Tips & Frequently Asked Questions:

Question 1: How long will the true-PDF of GB/T 15076.13-2017_English be delivered?

Answer: Upon your order, we will start to translate GB/T 15076.13-2017_English as soon as possible, and keep you informed of the progress. The lead time is typically 1 ~ 3 working days. The lengthier the document the longer the lead time.

Question 2: Can I share the purchased PDF of GB/T 15076.13-2017_English with my colleagues?

Answer: Yes. The purchased PDF of GB/T 15076.13-2017_English will be deemed to be sold to your employer/organization who actually pays for it, including your colleagues and your employer's intranet.

Question 3: Does the price include tax/VAT?

Answer: Yes. Our tax invoice, downloaded/delivered in 9 seconds, includes all tax/VAT and complies with 100+ countries' tax regulations (tax exempted in 100+ countries) -- See Avoidance of Double Taxation Agreements (DTAs): List of DTAs signed between Singapore and 100+ countries

Question 4: Do you accept my currency other than USD?

Answer: Yes. If you need your currency to be printed on the invoice, please write an email to [email protected]. In 2 working-hours, we will create a special link for you to pay in any currencies. Otherwise, follow the normal steps: Add to Cart -- Checkout -- Select your currency to pay.

Question 5: Should I purchase the latest version GB/T 15076.13-2017?

Answer: Yes. Unless special scenarios such as technical constraints or academic study, you should always prioritize to purchase the latest version GB/T 15076.13-2017 even if the enforcement date is in future. Complying with the latest version means that, by default, it also complies with all the earlier versions, technically.