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Plastics -- Polyamides -- Accelerated conditioning of test specimens
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GB/T 36790-2018
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Basic data Standard ID | GB/T 36790-2018 (GB/T36790-2018) | Description (Translated English) | Plastics -- Polyamides -- Accelerated conditioning of test specimens | Sector / Industry | National Standard (Recommended) | Classification of Chinese Standard | G31 | Classification of International Standard | 83.080.20 | Word Count Estimation | 6,612 | Date of Issue | 2018-09-17 | Date of Implementation | 2019-04-01 | Issuing agency(ies) | State Administration of Markets and China National Standardization Administration |
GB/T 36790-2018: Plastics -- Polyamides -- Accelerated conditioning of test specimens---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Plastics - Polyamides - Accelerated conditioning of test specimens
ICS 83.080.20
G31
National Standards of People's Republic of China
Plastic polyamide sample acceleration state adjustment
(ISO 1110.1995, MOD)
Published on.2018-09-17
Implementation of.2019-04-01
State market supervision and administration
China National Standardization Administration issued
Foreword
This standard was drafted in accordance with the rules given in GB/T 1.1-2009.
This standard uses the redrafting method to modify the use of ISO 1110.1995 "plastic polyamide sample acceleration state adjustment".
The technical differences between this standard and ISO 1110.1995 and their reasons are as follows.
---About the normative reference documents, this standard has made technical adjustments to adapt to China's technical conditions, specific tune
The whole is.
● Replaced ISO 291.1977 with GB/T 2918 equivalent to the international standard;
● Replaced ISO 483.1988 with ISO 483.
This standard was proposed by the China Petroleum and Chemical Industry Federation.
This standard is under the jurisdiction of the National Plastics Standardization Technical Committee Engineering Plastics Subcommittee (SAC/TC15/SC9).
This standard was drafted. Blonde Technology Co., Ltd., Zhonglan Chenguang Chemical Research and Design Institute Co., Ltd., Shanghai Blonde Technology Development
Co., Ltd., Guangzhou Jusailong Engineering Plastics Co., Ltd.
The main drafters of this standard. Yuan Shaoyan, Huang Xianbo, Zheng Wen, Liu Lirong, Liu Qixiang, Li Jianjun, Xia Jianmeng, Shi Xin, Yuan Haibing.
Introduction
The water content of polyamide (hereinafter referred to as PA) affects its properties. The PA performance test value is only in the case of the specified water content of the sample.
It is reproducible. The sample is adjusted in state and reaches equilibrium in a specific temperature and relative humidity environment. The test value is heavy.
Present.
The rate of state adjustment is affected by the rate of water absorption and is a function of temperature. The rate of water absorption is very low at room temperature. For example, a thick
The 4mm PA66 sample can be used in a standard environment (temperature 23 ° C/relative humidity 50%, see GB/T 2918), it takes more than 1 year to reach
To its equilibrium water content. Increasing the temperature allows the sample to reach equilibrium in a relatively short period of time. This standard gives the sample accelerated state.
The method of adjustment.
Plastic polyamide sample acceleration state adjustment
1 Scope
This standard specifies the acceleration state adjustment method for homopoly polyamide and copolymer polyamide test specimens.
This standard applies to polyamides containing fillers and other additives, but not for extracts greater than 2% (mass fraction)
Polyamide variety.
2 Normative references
The following documents are indispensable for the application of this document. For dated references, only dated versions apply to this article.
Pieces. For undated references, the latest edition (including all amendments) applies to this document.
Standard environment for GB/T 2918 plastic sample conditioning and testing (GB/T 2918-1988, ISO 291.1997, IDT)
ISO 483 Plastics maintain a constant humidity Small sealed container for conditioning and testing with aqueous solutions
3 Principle
The test sample is placed in an environment with a temperature of 70 ° C ± 1 ° C and a relative humidity of (62 ± 1)% (the difference between the dry and wet bulbs is 10 ° C ± 0.3 ° C).
Until the sample absorbs more than 95% of its equilibrium value.
The method is similar to the equilibrium water content adjusted in a standard environment (temperature 23 ° C/relative humidity 50%). Speed up the sample
The value of the mechanical properties measured after the state adjustment is not significantly different from the value adjusted by the standard environmental state (temperature 23 ° C/relative humidity 50%).
4 instruments
4.1 Constant temperature and humidity chamber. with fan to achieve airtight circulation, the temperature can be maintained at 70 °C ± 1 °C, the relative humidity can be maintained at
(62 ± 1)% (dry and wet bulb temperature difference is 10 ° C ± 0.3 ° C).
4.2 If there is no constant temperature and humidity chamber as described in 4.1, then.
4.2.1 The oven can maintain a temperature of 70 °C ± 1 °C.
4.2.2 A closed container, such as a dryer, is partially filled with a saturated aqueous solution of potassium iodide according to the general procedure given in ISO 483. In the whole shape
During the conditioning, leave enough salt in the solution. The sample may slightly fade due to iodine absorption.
4.3 Analyze the balance to the nearest 0.1 mg.
5 test steps
Place the sample in a preheated constant temperature and humidity chamber (4.1) or in a closed container (4.2.2) in an oven (4.2.1). Through the right
Methods, such as stents, ensure that the surface of each specimen is almost completely in contact with the surrounding air.
After the sample has been adjusted for a certain period of time t1 (see Table 1), it is taken out from the constant temperature and humidity chamber or the closed container and placed in a standard environment (warm
The temperature was 23 ° C/humidity 50%, see GB/T 2918) for 1 h, weighing (accurate to 0.1 mg). Then, follow the above method and continue to accelerate
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