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YS/T 710.3-2009 English PDF

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YS/T 710.3-2009: Method for chemical analysis of cobalt oxide. Part 3: Determination of sulphur content. High frequency combustion-infrared absorption method
Status: Valid
Standard IDUSDBUY PDFLead-DaysStandard Title (Description)Status
YS/T 710.3-2009139 Add to Cart 2 days Method for chemical analysis of cobalt oxide. Part 3: Determination of sulphur content. High frequency combustion-infrared absorption method Valid

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Basic data

Standard ID: YS/T 710.3-2009 (YS/T710.3-2009)
Description (Translated English): Method for chemical analysis of cobalt oxide. Part 3: Determination of sulphur content. High frequency combustion-infrared absorption method
Sector / Industry: Nonferrous Metallurgy Industry Standard (Recommended)
Classification of Chinese Standard: H13
Classification of International Standard: 77.120.70
Word Count Estimation: 4,461
Date of Issue: 2009-12-04
Date of Implementation: 2010-06-01
Older Standard (superseded by this standard): YS/T 256-2000
Regulation (derived from): MIIT [2009] No. 66
Issuing agency(ies): Ministry of Industry and Information Technology
Summary: This standard specifies: Determination of sulfur content Cobalt Oxide. This standard applies to the amount of sulfur in cobalt oxide measured. Measurement range: 0. 0050% to 0. 100 %.

YS/T 710.3-2009: Method for chemical analysis of cobalt oxide. Part 3: Determination of sulphur content. High frequency combustion-infrared absorption method


---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Method for chemical analysis of cobalt oxide.Part 3. Determination of sulphur content.High frequency combustion-infrared absorption method ICS 77.120.70 H13 People's Republic of China Nonferrous Metals Industry Standard Methods for chemical analysis of cobalt oxide Part 3. determination of sulfur content Frequency combustion infrared absorption method Posted 2009-12-04 2010-06-01 implementation Ministry of Industry and Information Technology of the People's Republic of China released

Foreword

YS/T 710 "cobalt oxide chemical analysis method" is divided into six sections. --- Part 1. Determination of cobalt content potentiometric titration; --- Part 2. Determination of sodium content by flame atomic absorption spectrometry; --- Part 3. Determination of the amount of sulfur by high frequency combustion infrared absorption method; --- Part 4. Determination of arsenic content by atomic fluorescence spectrometry; --- Part 5. Determination of silicon content - Molybdenum blue spectrophotometric method; --- Part 6. calcium, cadmium, copper, iron, magnesium, manganese, nickel, lead and zinc content - Inductively coupled plasma atomic emission spectrometry. This section YS/T Part 3 710. The partial replacement of YS/T 256-2000 "cobalt oxide" in Appendix C. Compared with YS/T 256-2000 "cobalt oxide" Appendix C, Part The main changes are as follows. --- Using high-frequency combustion infrared absorption method alternative polarography with; --- Complements the precision and quality assurance and control provisions. The non-ferrous metal part by the National Standardization Technical Committee and centralized. This section is responsible for drafting unit. Zhuzhou Smelter Group Co., Ltd. It participated in the drafting of this section. CRIMM, Zhejiang Huayou Cobalt Co. Ltd.. The main drafters of this section. Long Yu Yu, Cai Jun, Zhang Zhiyong, Yang Lin, Huang Xiaoting, Zhu Zhenqing, Xie Bohua. Methods for chemical analysis of cobalt oxide Part 3. determination of sulfur content Frequency combustion infrared absorption method

1 Scope

YS/T of the provisions of section 710 of the method for the determination of the sulfur content of cobalt oxide. This section applies to the determination of sulfur in the amount of cobalt oxide. Measurement range. 0.0050% to 0.100%.

2 Method summary

In the presence of flux, high-frequency induction furnace and the oxygen flow, so that the sample burned at high temperatures, to generate sulfur dioxide gas into the red External absorption cell, after which the instrument automatically measure the absorption of infrared energy to calculate and display the results.

3 Reagents and materials

3.1 scavenger 3.1.1 Anhydrous calcium chloride. 3.1.2 cotton. 3.2 flux 3.2.1 sulfur, tin, tungsten. tungsten + Sn (0.2g + 1.5g). 3.2.2 low-sulfur tin, iron. Sn + Fe (0.20g + 0.40g), iron sulfur content should be < 0.0010 percent. 3.2.3 tungsten particles. 3.3 Crucible Ceramic crucible (24mm × 24mm), before using a burning 2h at > 1100 ℃ high temperature furnace, cooling backup taken placed in the dryer (Valid for two days). 3.4 standard steel samples 3.4.1 standard steel samples. a sulfur content of 0.0050% to 0.10%. 3.4.2 standard steel or iron standard sample. a sulfur content of < 0.0010%.

4 Instrument

High-frequency infrared carbon and sulfur analyzer. Table 1 instrument reference operating conditions Oxygen purity oxygen pressure/MPa Oxygen flow L/min Analysis of gas flow L/min Carrying oxygen pressure valve MPa Oxygen Time/s analysis time/s High purity oxygen from 0.2 to 2.0 4.0 0.25 0.08 1535 Step 5 Analysis 5.1 Instrument Preparation Recommended by instrument instruments stand ready condition. 5.2 Stability Instrument 5.2.1 to adjust and stabilize the instrument by burning several similar kind of sample to be tested.
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