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YS/T 229.3-2013 English PDF

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Yes. Unless special scenarios such as technical constraints or academic study, you should always prioritize to purchase the latest version YS/T 229.3-2013 even if the enforcement date is in future. Complying with the latest version means that, by default, it also complies with all the earlier versions, technically.

US$159.00 · In stock
Delivery: <= 3 days. True-PDF full-copy in English will be manually translated and delivered via email.
YS/T 229.3-2013: Methods for chemical analysis of high pure lead. Part 3: Determination of antimony content. Atomic fluorescence spectrometry
Status: Valid

YS/T 229.3: Historical versions

Standard ID	USD	BUY PDF	Lead-Days	Standard Title (Description)	Status
YS/T 229.3-2013	159	Add to Cart	3 days	Methods for chemical analysis of high pure lead. Part 3: Determination of antimony content. Atomic fluorescence spectrometry	Valid
YS/T 229.3-1994	199	Add to Cart	2 days	High pure lead. Determination of antimony content. Malachite green photometric method	Obsolete

Similar standards

GB/T 3884.2 GB/T 3884.1 YS/T 252.1 YS/T 229.2 YS/T 229.4 YS/T 229.1

Basic data

Standard ID: YS/T 229.3-2013 (YS/T229.3-2013)
Description (Translated English): Methods for chemical analysis of high pure lead. Part 3: Determination of antimony content. Atomic fluorescence spectrometry
Sector / Industry: Nonferrous Metallurgy Industry Standard (Recommended)
Classification of Chinese Standard: H13
Classification of International Standard: 77.120.60
Word Count Estimation: 6,622
Older Standard (superseded by this standard): YS/T 229.3-1994
Regulation (derived from): Ministry of Industry and Information Technology Bulletin No. 52, 2013; industry standard for filing Notice No. 1 of 2014 (No. 169 overall)
Issuing agency(ies): Ministry of Industry and Information Technology
Summary: This standard specifies the method for the determination of lead in high-purity antimony content. This standard applies to the determination of lead in high-purity antimony content. Determination of antimony content in the range of: 0. 0510 -4% ~ 1. 010-4

YS/T 229.3-2013: Methods for chemical analysis of high pure lead. Part 3: Determination of antimony content. Atomic fluorescence spectrometry

---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Methods for chemical analysis of high pure lead Part 3. Determination of antimony content Atomic fluorescence spectrometry ICS 77.120.60 H13 People's Republic of China Nonferrous Metals Industry Standard Replacing YS/T 229.3-1994 Methods for chemical analysis of high purity lead Part 3. Determination of antimony content Atomic Fluorescence Spectrometry Part 3. Determinationofantimonycontent- Issued on. 2013-10-17 2014-03-01 implementation Ministry of Industry and Information Technology of the People's Republic of China released

Foreword

YS/T 229-2013 "high purity chemical analysis of lead" is divided into four parts. --- Part 1. silver, copper, bismuth, aluminum, nickel, tin, magnesium, and iron - Determination of chemical spectroscopy; --- Part 2. Determination of arsenic content by atomic fluorescence spectrometry; --- Part 3. Determination of antimony content - Atomic Fluorescence Spectrometry; --- Part 4. Determination of trace element contents of glow discharge mass spectrometry. This is Part 3 YS/T 229's. This section drafted in accordance with GB/T 1.1-2009 given rules. The partial replacement of YS/T 229.3-1994 determination of antimony content of lead in high purity (malachite green photometric method). And YS/T 229.3-1994 Compared to the main changes are as follows. --- Changed the measurement method using atomic fluorescence spectrometry; --- Added "precision" clause; --- Added "the test report" requirement. The non-ferrous metal part by the National Standardization Technical Committee (SAC/TC243) centralized. This section is responsible for drafting unit. Zhuzhou Smelter Group Co., Ltd. This section participated in the drafting unit. China Nonferrous Guilin Research Institute of Geology and Minerals Co. Ltd., Beijing General Research Institute of Mining and Metallurgy, Baiyin Nonferrous Group CO., LTD. The main drafters of this section. Jiang Qing, to De Lei, Liu Chuanshi, Chen Zhu Ping, Qiao Xiaofang, Yuan Yuxia, Wanghao Ying, Wang Dongzhen, Wei Wenhui, Ma-li. This part of the standard replaces the previous editions are. --- YS/T 229.3-1994. Methods for chemical analysis of high purity lead Part 3. Determination of antimony content Atomic Fluorescence Spectrometry Warning --- personnel should use this standard regular laboratory work experience. This standard does not point out all possible security asked question. Users have the responsibility to take appropriate safety and health practices and to ensure compliance with the conditions relevant national regulations.

1 Scope

This section YS/T 229 specifies the method for determination of purity lead antimony content. This section applies to the determination of antimony content of lead in high purity. Determination of antimony content range. 0.05 × 10-4% ~ 1.0 × 10-4% (mass fraction number).

2 principle of the method

The sample is dissolved in nitric acid, precipitation of lead chloride, lead body, thiourea - ascorbic acid in the presence of antimony in hydrochloric acid medium is potassium borohydride Hydride reduction of antimony, with argon gas was introduced into the quartz furnace atomizer, the fluorescence intensity was measured antimony on the atomic fluorescence spectrometer.

3 Reagents

Unless otherwise indicated in the analysis using only recognized as a high-purity reagents and water or equivalent purity. 3.1 nitric acid (ρ = 1.42g/mL). 3.2 hydrochloric acid (ρ = 1.19g/mL). 3.3 nitric acid (12). 3.4 hydrochloride (11). 3.5 hydrochloride (14). 3.6 thiourea - ascorbic acid solution (50g/L). Weigh 5g thiourea (excellent pure), 5g ascorbic acid (excellent pure), dissolved in water, dilute Diluted to 100mL, and mix. The time is now equipped with. 3.7 solution of potassium borohydride (25g/L). Weigh 5g potassium borohydride (excellent pure), was added a solution of 1g of potassium hydroxide in advance (excellent pure) of 200mL of water. The time is now equipped with. 3.8 Antimony standard stock solution. Weigh 0.2740g antimony potassium tartrate (excellent pure), placed in 150mL beaker, add water 100mL low Heated dissolved and transferred to 1000mL volumetric flask, add 10mL of nitric acid (3.1), dilute to the mark and mix. This solution containing 1mL Antimony 100μg. 3.9 Antimony standard solution. Pipette 2.50mL antimony standard stock solution (3.8) in 500mL volumetric flask, was added 50mL of hydrochloric acid (3.2), with Dilute with water to volume, and mix. This solution 1mL antimony-containing 0.50μg. 3.10 argon (purity ≥99.99%).

4 Instrument

Atomic fluorescence spectrometer, with high-intensity hollow cathode lamp antimony. ......

Image

Tips & Frequently Asked Questions:

Question 1: How long will the true-PDF of YS/T 229.3-2013_English be delivered?

Answer: Upon your order, we will start to translate YS/T 229.3-2013_English as soon as possible, and keep you informed of the progress. The lead time is typically 1 ~ 3 working days. The lengthier the document the longer the lead time.

Question 2: Can I share the purchased PDF of YS/T 229.3-2013_English with my colleagues?

Answer: Yes. The purchased PDF of YS/T 229.3-2013_English will be deemed to be sold to your employer/organization who actually pays for it, including your colleagues and your employer's intranet.

Question 3: Does the price include tax/VAT?

Answer: Yes. Our tax invoice, downloaded/delivered in 9 seconds, includes all tax/VAT and complies with 100+ countries' tax regulations (tax exempted in 100+ countries) -- See Avoidance of Double Taxation Agreements (DTAs): List of DTAs signed between Singapore and 100+ countries

Question 4: Do you accept my currency other than USD?

Answer: Yes. If you need your currency to be printed on the invoice, please write an email to Sales@ChineseStandard.net. In 2 working-hours, we will create a special link for you to pay in any currencies. Otherwise, follow the normal steps: Add to Cart -- Checkout -- Select your currency to pay.

Question 5: Should I purchase the latest version YS/T 229.3-2013?

Answer: Yes. Unless special scenarios such as technical constraints or academic study, you should always prioritize to purchase the latest version YS/T 229.3-2013 even if the enforcement date is in future. Complying with the latest version means that, by default, it also complies with all the earlier versions, technically.