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SN/T 3925-2014 English PDF

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SN/T 3925-2014: Determination of milbemycins residues in foodstuffs of animal origin for export. LC-MS/MS method
Status: Valid
Standard IDUSDBUY PDFLead-DaysStandard Title (Description)Status
SN/T 3925-2014629 Add to Cart 5 days Determination of milbemycins residues in foodstuffs of animal origin for export. LC-MS/MS method Valid

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GB 5009.271   GB 5009.22   SN/T 2641   SN/T 3928   SN/T 3929   SN/T 3926   

Basic data

Standard ID: SN/T 3925-2014 (SN/T3925-2014)
Description (Translated English): Determination of milbemycins residues in foodstuffs of animal origin for export. LC-MS/MS method
Sector / Industry: Commodity Inspection Standard (Recommended)
Classification of Chinese Standard: X04
Classification of International Standard: 67.120.01
Word Count Estimation: 24,217
Date of Issue: 4/9/2014
Date of Implementation: 11/1/2014
Quoted Standard: GB/T 6682
Regulation (derived from): State inspection certification (2014) 210
Issuing agency(ies): General Administration of Customs
Summary: This standard specifies the residues in food of animal origin liquid chromatography - mass spectrometry/mass spectrometry sent us.

SN/T 3925-2014: Determination of milbemycins residues in foodstuffs of animal origin for export. LC-MS/MS method


---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Determination of milbemycins residues in foodstuffs of animal origin for export. LC-MS/MS method People's Republic of China Entry-Exit Inspection and Quarantine Standards Export of food of animal origin in various milbemycin Residues Determination of liquid chromatography - mass spectrometry/mass spectrometry LC-MS/MSmethod Issued on. 2014-04-09 2014-11-01 implementation People's Republic of China The State Administration of Quality Supervision, Inspection and Quarantine released

Foreword

This standard was drafted in accordance with GB/T 1.1-2009 given rules. Please note that some of the content of this standard may involve patents. The standard release Institutions do not assume the responsibility to identify these patents. This standard is proposed and managed by the National Certification and Accreditation Administration Committee. This standard was drafted. People's Republic of China, Shenzhen CIQ, Shenzhen Inspection and Quarantine Science Research Institute. The main drafters of this standard. Kang Haining, Yuezhen Feng, Li Yong, Ye Gang, Xieli Qi, Lin Li, Hou Yuexi, Chen Jincan, Huahong Hui. Export of food of animal origin in various milbemycin Residues Determination of liquid chromatography - mass spectrometry/mass spectrometry

1 Scope

This standard specifies the foodstuffs of animal origin Mosey Dink, milbemycin A3, milbemycin A4, milbemycin D, nemadectin residues The remaining amount of liquid chromatography - mass spectrometry/mass spectrometry. This standard applies to chicken, pork, beef, chicken, liver, beef liver, chicken kidney, kidney, beef kidney, eggs, milk, fish Mosey Dink, rice Bay ADM A3, milbemycin A4, milbemycin D, nemadectin residues measured and confirmed.

2 Normative references

The following documents for the application of this document is essential. For dated references, only the dated version suitable for use herein Member. For undated references, the latest edition (including any amendments) applies to this document. Laboratory use specifications and test methods GB/T 6682 Analysis

3 Method summary

With tert-butyl methyl ether extract sample (except milk) residues milbemycin drugs, and the extract was concentrated redissolved nitrogen blowing through Silica gel column purification, concentration, liquid chromatography - mass spectrometry/mass spectrometry and confirmed, external standard. Milk milbemycin drug residues extracted with acetonitrile and the extract was concentrated purified by C18 column chromatography - mass spectrometry/mass spectrometry detection Testing and validation, external standard.

4 Reagents and materials

Unless otherwise indicated, the reagents used were of analytical grade water using a water GB/T 6682 regulations. 4.1 tert-butyl methyl ether. 4.2 ethyl acetate. 4.3 n-hexane. 4.4 acetonitrile. high performance liquid chromatography. 4.5 Methanol. HPLC grade. 4.6 dichloromethane. 4.7 formic acid. High performance liquid chromatography. 4.8 over anhydrous sodium. 650 ℃ burning 4h, cooled, placed in a desiccator. 4.9 sodium chloride. 4.10 lysis solution. n-hexane dichloromethane (64 volume), accurately weighed 60mL hexane (4.3), and 40mL dichloromethane (4.6), mix well. 4.11 Eluent. n-hexane ethyl acetate (694, volume ratio) were accurately taken 60mL ethyl acetate (4.2) and 940mL of n-hexane, well mixed.
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