SN/T 3852-2014 English PDFUS$599.00 · In stock
Delivery: <= 4 days. True-PDF full-copy in English will be manually translated and delivered via email. SN/T 3852-2014: Determination of metaflumizone residues in food for export. LC-MS/MS method Status: Valid
Basic dataStandard ID: SN/T 3852-2014 (SN/T3852-2014)Description (Translated English): Determination of metaflumizone residues in food for export. LC-MS/MS method Sector / Industry: Commodity Inspection Standard (Recommended) Classification of Chinese Standard: X04 Classification of International Standard: 67.050 Word Count Estimation: 23,256 Quoted Standard: GB/T 6682 Regulation (derived from): AQSIQ notification issued in 2014 on the first batch of 230 industry-standard entry-exit inspection and quarantine Issuing agency(ies): General Administration of Customs Summary: This Standard specifies the metaflumizone export of food and its metabolites (3-trifluoromethyl benzoate) residual amount of liquid chromatography - mass spectrometry/mass spectrometry and confirmation methods. This Standard applies to corn, rice, grapes, SN/T 3852-2014: Determination of metaflumizone residues in food for export. LC-MS/MS method---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.Determination of metaflumizone residues in food for export. LC-MS/MS method People's Republic of China Entry-Exit Inspection and Quarantine Standards Determination of fipronil hydrazone residues in food exports in cyanide Liquid chromatography - mass spectrometry/mass spectrometry LC-MS/MSmethod Issued on. 2014-01-13 2014-08-01 implementation People's Republic of China The State Administration of Quality Supervision, Inspection and Quarantine released ForewordThis standard was drafted in accordance with GB/T 1.1-2009 given rules. Please note that some of the content of this document may involve patents. Distribution of this document Institutions do not assume the responsibility to identify these patents. This standard is proposed and managed by the National Certification and Accreditation Administration Committee. This standard was drafted. Jilin People's Republic of China Exit Inspection and Quarantine, People's Republic of China Entry-Exit Inspection and Tonghua Quarantine Bureau. The main drafters of this standard. Li Aijun, Mou Jun, Shi Xiaoli, ZHANG Dai Hui, Wang Mingtai, Kangming Qin, Ting-Ting Hu. Determination of fipronil hydrazone residues in food exports in cyanide Liquid chromatography - mass spectrometry/mass spectrometry1 ScopeThis standard specifies the metaflumizone export of food and its metabolites (3-trifluoromethyl benzoate) residual amount of liquid chromatography - mass spectrometry / MS detection and confirmation methods. This standard applies to residual amount of metaflumizone and its metabolites in foods as corn, rice, grapes, citrus, onions, peanuts, milk and other measurement And confirmation.2 Normative referencesThe following documents for the application of this document is essential. For dated references, only the dated version suitable for use herein Member. For undated reference documents, the latest versions apply to this document. Laboratory use specifications and test methods GB/T 6682 analysis.3 Method summarySample metaflumizone and its metabolites extracted with methanol, dried PSA (N-2-aminoethyl) solid phase extraction (SPE), methanol eluent After concentration, methanol solution (1 by volume ratio) was dissolved constant volume, liquid chromatography - mass spectrometry/mass spectrometer and validation, external standard.4 Reagents and materialsUnless otherwise specified, the reagents were of analytical grade water as a water GB/T 6682 regulations. 4.1 methanol. residual level. 4.2 sodium chloride. 4.3 magnesium sulfate. 4.4 sodium hydroxide. 4.5 Sodium hydroxide solution (0.1mol/L). Weigh 4.0g of sodium hydroxide dissolved in water and dilute to 1000mL. 4.6 metaflumizone (CAS No. 139968-49-3) and its metabolite [3-trifluoromethyl-benzoic acid methyl ester (CAS No. 2967-66-0)] Standard. Purity not less than 98.0%. 4.7 metaflumizone and metabolite standards stock solution. Accurately weigh an appropriate amount of metaflumizone and its metabolites standards, prepared in methanol and concentrated Degree of 100μg/mL of the standard stock solution. The solution at 0 ℃ ~ 4 ℃ refrigerator stored. 4.8 metaflumizone and its metabolites standard solution. as needed metaflumizone and its metabolites standard stock solution was diluted with methanol to Applicable standard working solution concentration. The solution at 0 ℃ ~ 4 ℃ refrigerator stored. 4.9 PSA (N-2-aminoethyl) SPE. PSA, 250mg, 6mL, or equivalent person; before use, with 6mL methanol activation, stream Rate 1mL/min. 4.10 microporous membrane. 0.20μm, organic phase. ......Tips & Frequently Asked Questions:Question 1: How long will the true-PDF of SN/T 3852-2014_English be delivered?Answer: Upon your order, we will start to translate SN/T 3852-2014_English as soon as possible, and keep you informed of the progress. 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