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SN/T 3792-2014 English PDF

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SN/T 3792-2014: Determination of the azo colorants in electrical and electronic products. High performance liquid chromatography-mass spectrometry method
Status: Valid
Standard IDUSDBUY PDFLead-DaysStandard Title (Description)Status
SN/T 3792-2014259 Add to Cart 3 days Determination of the azo colorants in electrical and electronic products. High performance liquid chromatography-mass spectrometry method Valid

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GB/T 6113.102   GB/T 34986   GB/T 32910.3   SN/T 4240   SN/T 3793   SN/T 3791   

Basic data

Standard ID: SN/T 3792-2014 (SN/T3792-2014)
Description (Translated English): Determination of the azo colorants in electrical and electronic products. High performance liquid chromatography-mass spectrometry method
Sector / Industry: Commodity Inspection Standard (Recommended)
Classification of Chinese Standard: L04
Classification of International Standard: 29.020
Word Count Estimation: 10,140
Quoted Standard: GB/T 6682
Regulation (derived from): AQSIQ notification issued in 2014 on the first batch of 230 industry-standard entry-exit inspection and quarantine
Issuing agency(ies): General Administration of Customs
Summary: This Standard specifies the electrical and electronic products can be cleaved azo dyes aromatic primary amine liquid chromatography - mass spectrometry. This Standard applies to electrical and electronic plastic parts measured azo dyes.

SN/T 3792-2014: Determination of the azo colorants in electrical and electronic products. High performance liquid chromatography-mass spectrometry method


---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Determination of the azo colorants in electrical and electronic products. High performance liquid chromatography-mass spectrometry method People's Republic of China Entry-Exit Inspection and Quarantine Standards Determination of electrical and electronic products of azo dyes Liquid Chromatography - Mass Spectrometry Issued on. 2014-01-13 2014-08-01 implementation People's Republic of China The State Administration of Quality Supervision, Inspection and Quarantine released

Foreword

This standard was drafted in accordance with GB/T 1.1-2009 given rules. This standard is proposed and managed by the National Certification and Accreditation Administration Committee. This standard was drafted. People's Republic of China Shandong Entry Inspection and Quarantine Bureau, People's Republic of China Guangdong Entry-Exit Inspection and Quarantine Bureau. The main drafters of this standard. Cattle Zengyuan, Duheng Qing, Luo Xin, Tony Feng, Cai Xue, Liang, ZHOU Ming-hui. Determination of electrical and electronic products of azo dyes Liquid Chromatography - Mass Spectrometry

1 Scope

This standard specifies the electrical and electronic products can be cleaved azo dyes aromatic primary amine liquid chromatography - mass spectrometry. This standard applies to electrical and electronic components in the determination of azo dyes in plastic.

2 Normative references

The following documents for the application of this document is essential. For dated references, only the dated version suitable for use herein Member. For undated references, the latest edition (including any amendments) applies to this document. Laboratory use specifications and test methods GB/T 6682 Analysis

3 Method summary

After sonication the sample an organic solvent with methanol to precipitate the polymer matrix, after reduction with sodium dithionite, extraction with methyl t-butyl ether, the extract After concentration and purification, liquid chromatography - mass spectrometry (LC-MS) and validation, external standard.

4 Reagents and materials

Unless otherwise indicated, the reagents used were of analytical grade. Water is in line with GB/T 6682 provided a water. 4.1 Sodium dithionite. purity of greater than or equal to 87%. 4.2 sodium hydroxide. 4.3 acetone. chromatography. 4.4 dichloromethane. chromatography. 4.5 tetrahydrofuran. chromatography. 4.6 Methanol. chromatographically pure. 4.7 methyl tert-butyl ether. chromatography. 4.8 hexane. chromatographically pure. 4.9 acetonitrile. chromatography. 4.10 formic acid. 88%. 4.11 hydrochloric acid (ρ1.38g/mL ~ 1.40g/mL). pure class distinctions. 4.12 aromatic primary amine standard. purity of greater than or equal to 98%, see Appendix A. 4.13 dithionite solution.200mg/mL, the time is now equipped with. 4.14 Sodium hydroxide solution. 4mol/L. 4.15 hydrochloric acid solution. 4mol/L. 4.16 methanol - water mixed solution (11 volume). an equal volume of methanol and water miscible. 4.17 formic acid. volume fraction of 0.1%. 4.18 standard stock solution. namely, accurately weighed amount of aromatic primary amine standard, prepared in methanol at a concentration of 1000mg/L standard
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