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SN/T 2690-2010 English PDF

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SN/T 2690-2010: Determination of vinyl chloride in used mechanical and electronic products
Status: Valid
Standard IDUSDBUY PDFLead-DaysStandard Title (Description)Status
SN/T 2690-2010239 Add to Cart 3 days Determination of vinyl chloride in used mechanical and electronic products Valid

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Basic data

Standard ID: SN/T 2690-2010 (SN/T2690-2010)
Description (Translated English): Determination of vinyl chloride in used mechanical and electronic products
Sector / Industry: Commodity Inspection Standard (Recommended)
Classification of Chinese Standard: J04
Classification of International Standard: 25.010
Word Count Estimation: 9,910
Date of Issue: 2010-11-01
Date of Implementation: 2011-05-01
Regulation (derived from): National Quality Inspection (2010) 582
Issuing agency(ies): General Administration of Customs
Summary: This standard specifies the old mechanical and electrical products, residual vinyl chloride headspace gas chromatography mass spectrometry. This standard applies to the old mechanical and electrical products in polymeric materials Determination of residual vinyl chloride.

SN/T 2690-2010: Determination of vinyl chloride in used mechanical and electronic products

---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Determination of vinyl chloride in used mechanical and electronic products People's Republic of China Entry-Exit Inspection and Quarantine Standards Determination of the old mechanical and electrical products in the vinyl chloride Issued on. 2010-11-01 2011-05-01 implementation People's Republic of China The State Administration of Quality Supervision, Inspection and Quarantine released

Foreword

This standard was drafted in accordance with GB/T 1.1-2009 given rules. This standard is proposed and managed by the National Certification and Accreditation Administration Committee. This standard was drafted. Chinese Academy of Inspection and Quarantine. The main drafters. Zhang, Wang Chao, birch, Xiao Haiqing, Dong Yiyang, Ma Qiang, Yan Yan. This is the first issue of inspection and quarantine industry standards. Determination of the old mechanical and electrical products in the vinyl chloride

1 Scope

This standard specifies the old mechanical and electrical products in the residual vinyl chloride headspace gas chromatography mass spectrometry. This standard applies to the determination of the old mechanical and electrical products in the residual vinyl chloride polymer material. Principle 2 The sample vial is placed in a glass transition temperature above content using gas chromatography mass spectrometry chloride.

3 Reagents and materials

Unless otherwise specified, reagents were of analytical grade. 3.1 Methanol. chromatographically pure. 3.2 vinyl chloride standard solution. the commercialization of certified standard solution, 5000mg/L, using methanol as solvent, vinyl chloride purity of greater than 99.5%, refrigerated stored. 3.3 standard solution Ⅰ. accurate Pipette vinyl chloride standard solution 2mL to 100mL brown volumetric flask, constant volume of methanol, concentrated to give Degree of 100mg/L of standard solution, refrigerated stored. 3.4 standard solution Ⅱ. accurate Pipette 1mL to 100mL standard solution Ⅰ brown volumetric flask, constant volume of methanol to give a concentration Save as 1mg/L standard working solution Ⅱ, refrigerated in the dark.

4 instruments and equipment

4.1 Gas chromatograph with mass selective detector (MSD). 4.2 air injector. 4.3 micro syringe. 10μL, 50μL. 4.4 bottles. 20mL. 4.5 Analysis of balance. a sense of the amount of 0.1mg. Step 5 Analysis 5.1 Determination 5.1.1 GC-MS analysis conditions Because the test results depends on the instrument used, it is impossible to give general parameters chromatographic analysis. Using the following operating conditions are It proved to be suitable for testing. a) capillary column. DB-624 capillary column 1). 30m × 0.32mm × 1.80μm or equivalent person; 1) DB-624 is the trade name of the company provided by Agilent, this information is given for the convenience of users of this standard does not mean that the product identified can. If other equivalent product has the same effect, you can use these equivalent products. b) temperature program. Initial temperature 30 ℃ (held 3min), and then heating rate 20 ℃/min was raised to 100 ℃ (held
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