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SN/T 2560-2010 English PDF

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SN/T 2560-2010: Determination of carbamate pesticides residues in foodstuffs for import and export. LC-MS/MS method
Status: Valid
Standard IDUSDBUY PDFLead-DaysStandard Title (Description)Status
SN/T 2560-2010889 Add to Cart 6 days Determination of carbamate pesticides residues in foodstuffs for import and export. LC-MS/MS method Valid

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Basic data

Standard ID: SN/T 2560-2010 (SN/T2560-2010)
Description (Translated English): Determination of carbamate pesticides residues in foodstuffs for import and export. LC-MS/MS method
Sector / Industry: Commodity Inspection Standard (Recommended)
Classification of Chinese Standard: X04
Classification of International Standard: 67.050
Word Count Estimation: 36,357
Date of Issue: 2010-05-27
Date of Implementation: 2010-12-01
Quoted Standard: GB/T 6682
Regulation (derived from): National Quality Inspection [2010] No. 290
Issuing agency(ies): General Administration of Customs
Summary: This standard specifies the food aminocarb, aldicarb, aldicarb sulfoxide, aldicarb sulfone, methomyl, long effect Viagra sulfone, sulfoxide long Wia efficiency, carbon Granville, pirimicarb, Kebai Granville, evil insects salty, propoxur, carbaryl, B sulfur benzene salty, elimination Granville, isoprocarb, mixed kill Wei, 20 carbamate pesticide residues in sample preparation and liquid chromatography mass spectrometry/mass spectrometry. This standard applies to rice, spinach, potatoes, citrus, grapes, walnuts, tea, pork, fish, liver and milk aminocarb, aldicarb, fraternal metolcarb sulfone, aldicarb sulfoxide, methomyl, long effect Viagra sulfone, sulfoxide long Wia efficiency, carbon Granville, pirimicarb, Kebai Qi, bendiocarb, propoxur, carbaryl, Ethiofencarb, elimination Granville, isoprocarb, mixed kill Wei, Fenobucarb, methiocarb and promecarb Shao residual amount of quantitative determination and confirmation.

SN/T 2560-2010: Determination of carbamate pesticides residues in foodstuffs for import and export. LC-MS/MS method


---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Determination of carbamate pesticides residues in foodstuffs for import and export.LC-MS/MS method People's Republic of China Entry-Exit Inspection and Quarantine Standards Import and export food carbamate pesticide residues Determination of liquid chromatography - mass spectrometry/mass spectrometry Issued on. 2010-05-27 2010-12-01 implementation People's Republic of China The State Administration of Quality Supervision, Inspection and Quarantine released

Foreword

This standard was drafted in accordance with GB/T 1.1-2009 given rules. This standard is proposed and managed by the National Certification and Accreditation Administration Committee. This standard was drafted. People's Republic of China Hunan Exit Inspection and Quarantine, Central South University of Forestry and Technology. The main drafters. Zhang Ying, Mei-ling, Zhang Fan, Huang Ping, Wang Xiangxian, Dingley, Yan Hongfei, Zhu Shaohua, Huang Zhiqiang. Import and export food carbamate pesticide residues Determination of liquid chromatography - mass spectrometry/mass spectrometry

1 Scope

This standard specifies the terminator foods Granville, aldicarb, aldicarb sulfoxide, aldicarb sulfoxide, methomyl, long effect Granville sulfone, long effect Wia sulfoxide, dioxane Granville, pirimicarb, carbofuran, bendiocarb, propoxur, carbaryl, ethyl benzene, sulfur Granville, elimination Granville, isopropyl Granville, Granville mixed kill 20 kinds of agricultural carbamate Sample preparation and liquid chromatography detection of drug residues in - Mass/mass spectrometry. This standard applies to rice, spinach, potatoes, citrus, grapes, walnuts, tea, pork, fish, liver and milk terminator Granville, aldicarb Granville, aldicarb sulfoxide, aldicarb sulfoxide, methomyl, long effect Granville sulfone, long effect Wia sulfoxide, dioxane Granville, pirimicarb, carbofuran, bendiocarb, propoxur, A Carbaryl, ethyl benzene, sulfur Granville, elimination Granville, Granville isopropyl, mixed kill Wei, bassa, methiocarb and Promecarb residual amounts of quantitative determination and confirmation.

2 Normative references

The following documents for the application of this document is essential. For dated references, only the dated version suitable for use herein Member, undated references, the latest edition (including any amendments) applies to this document. Laboratory use specifications and test methods GB/T 6682 Analysis

3 Method summary

The sample was extracted with acetonitrile carbamate pesticide residues, or extract through C18 carbon graphite composite amino SPE column liquid chromatography Spectrum - MS/MS detection and confirmation, external standard.

4 Reagents and materials

Except where noted, all reagents were of analytical grade water as a water line with GB/T 6682 regulations. 4.1 acetonitrile. HPLC grade. 4.2 Methanol. HPLC grade. 4.3 toluene. 4.4 acetic acid. 4.5 sodium chloride. 4.6 anhydrous sodium sulfate. After burning 650 ℃ 4h, the dryer use. 4.7 0.1% acetic acid solution. Take 1mL acetic acid, diluted with water and dilute to 1000mL. 4.8 Methanol - water (11 volume). Measure 100mL methanol, 100mL water was added, mixing spare. 4.9 Toluene - acetonitrile (13 volume). Measure 100mL of toluene, 300mL of acetonitrile, mix standby. 4.10 terminator Granville, aldicarb, aldicarb sulfoxide, aldicarb sulfoxide, methomyl, long effect Granville sulfone, long effect Wia sulfoxide, dioxane Granville, pirimicarb, carbofuran, Bendiocarb, propoxur, carbaryl, ethyl benzene, sulfur Granville, elimination Granville, Granville isopropyl, mixed kill Wei, bassa, methiocarb and Promecarb Standards. Great purity Than or equal to 98%, see Appendix A. 4.11 standard stock solution. accurately weighed amount of the above standards, with acetonitrile were prepared at a concentration of 1.0mg/mL standard stock solution Liquid, 4 ℃ stored in the dark. 4.12 intermediate mixed standard solution. take the appropriate amount of the above standard stock solution with acetonitrile formulated as 10μg/mL standard mixed solution at 4 ℃ to avoid
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