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SN/T 1784-2006 English PDF

Standard IDUSDBUY PDFLead-DaysStandard Title (Description)Status
SN/T 1784-2006319 Add to Cart 3 days Determination of dioxane residues in cosmetics for import and export. Gas chromatography-mass spectrometry method Obsolete

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Basic data

Standard ID: SN/T 1784-2006 (SN/T1784-2006)
Description (Translated English): Determination of dioxane residues in cosmetics for import and export. Gas chromatography-mass spectrometry method
Sector / Industry: Commodity Inspection Standard (Recommended)
Classification of Chinese Standard: Y42
Classification of International Standard: 71.100.70
Word Count Estimation: 8,871
Date of Issue: 2006-04-25
Date of Implementation: 2006-11-15
Quoted Standard: GB/T 6379
Regulation (derived from): Industry Standard Notice 2006 No. 7 (No. 79 overall)
Issuing agency(ies): General Administration of Customs
Summary: This standard specifies the use of gas chromatography mass spectrometry dioxane in cosmetics residues approach. This standard applies to cosmetics dioxane residues. This standard dioxane limit of determination: 2. 5mg/kg.

SN/T 1784-2006: Determination of dioxane residues in cosmetics for import and export. Gas chromatography-mass spectrometry method


---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Determination of dioxane residues in cosmetics for import and export.Gas chromatography-mass spectrometry method People's Republic of China Entry-Exit Inspection and Quarantine Industry Standard Determination of dioxane residues in cosmetics for import and export Gas chromatography tandem mass spectrometry Released on.2006-04-25 Implementation of.2006-11-15 People's Republic The General Administration of Quality Supervision, Inspection and Quarantine issued

Foreword

Appendix A and Appendix B of this standard are informative annexes. This standard is proposed and managed by the National Certification and Accreditation Administration. This standard was drafted by the China Academy of Inspection and Quarantine. The main drafters of this standard. Wang Chao, Ji Meiqin, Wang Xing, Hao Nan, Cai Tianpei. This standard is the first industry standard for entry-exit inspection and quarantine. Determination of dioxane residues in cosmetics for import and export Gas chromatography tandem mass spectrometry

1 Scope

This standard specifies the method for the determination of dioxane residues in cosmetics by gas chromatography-mass spectrometry. This standard applies to the determination of dioxane residues in cosmetics. The lower limit of determination of this standard dioxane. 2.5mg/kg.

2 Normative references

The terms in the following documents become the terms of this standard by reference to this standard. All dated references, followed by all Modifications (not including errata content) or revisions do not apply to this standard, however, parties to agreements based on this standard are encouraged to study Is it possible to use the latest version of these files? For undated references, the latest edition applies to this standard. GB/T 6379 Accuracy of measurement methods and results (correctness and precision) (all parts)

3 Principle

After the sample is heated and extracted in the headspace bottle, it is determined by gas chromatography-mass spectrometry (GC/MSD) method, and the external standard method is used for quantification. The test is made to determine.

4 reagents and materials

Unless otherwise specified, the reagents used were of analytical grade and the water was secondary water. 4.1 Dioxane. purity 98%. 4.2 Dioxane standard stock solution. Accurately weigh the appropriate amount of dioxane standard (accurate to 0.0001g). Water is configured to a concentration of Standard stock solution of 1000 μg/mL. The stock solution is stored in a 4 ° C refrigerator and can be used for 2 months. 4.3 Dioxane standard working solution. The above (4.2) stock solution was separately mixed with methanol to a dioxane concentration of 0.1 μg/mL, 0.5 μg/mL, 1 μg/mL, 10 μg/mL, 20 μg/mL, 50 μg/mL, and 100 μg/mL standard working solution were stored at 4 ° C for 1 week.

5 instruments

5.1 Gas Chromatograph. equipped with a mass selective detector (MSD). 5.2 Headspace Sampler. 5.3 Headspace bottle. 20mL. 5.4 Analytical balance. Sensitivity 0.0001g. 5.5 Ultrasonic cleaning instrument.

6 Determination steps

6.1 Sample Processing Accurately weigh 2.0g of the mixed sample to the nearest 0.001g, place it in the headspace sample bottle, add 1g of sodium chloride solid, add 8mL of steam The distilled water was sealed, gently shaken, placed in a headspace sampler, and equilibrated at 70 ° C for 40 min. Take 1 mL of the upper gas after the gas is equilibrated. Into gas chromatography-mass spectrometry.
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