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Delivery: <= 2 days. True-PDF full-copy in English will be manually translated and delivered via email. GB/T 8152.17-2023: Methods for chemical analysis of lead concentrates - Part 17: Determination of aluminum, magnesium, iron, copper, zinc, cadmium, arsenic, antimony, bismuth and calcium contents - Inductively coupled plasma atomic emission spectrometry Status: Valid
Basic dataStandard ID: GB/T 8152.17-2023 (GB/T8152.17-2023)Description (Translated English): Methods for chemical analysis of lead concentrates - Part 17: Determination of aluminum, magnesium, iron, copper, zinc, cadmium, arsenic, antimony, bismuth and calcium contents - Inductively coupled plasma atomic emission spectrometry Sector / Industry: National Standard (Recommended) Classification of Chinese Standard: H13 Classification of International Standard: 77.120.60 Word Count Estimation: 27,272 Date of Issue: 2023-05-23 Date of Implementation: 2023-12-01 Issuing agency(ies): State Administration for Market Regulation, China National Standardization Administration GB/T 8152.17-2023: Methods for chemical analysis of lead concentrates - Part 17: Determination of aluminum, magnesium, iron, copper, zinc, cadmium, arsenic, antimony, bismuth and calcium contents - Inductively coupled plasma atomic emission spectrometry---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order. ICS 77:120:60 CCSH13 National Standards of People's Republic of China Chemical analysis method of lead concentrate Part 17: Aluminum, magnesium, iron, copper, zinc, cadmium, arsenic, Determination of antimony, bismuth and calcium content Inductively Coupled Plasma-Atomic Emission Spectrometry Released on 2023-05-23 Implemented on 2023-12-01 State Administration for Market Regulation Released by the National Standardization Management Committee forewordThis document is in accordance with the provisions of GB/T 1:1-2020 "Guidelines for Standardization Work Part 1: Structure and Drafting Rules for Standardization Documents" drafting: This document is part 17 of GB/T 8152 "Methods for Chemical Analysis of Lead Concentrates": GB/T 8152 has released the following parts: --- Part 1: Determination of lead content acid dissolution-EDTA titration method; --- Part 2: Determination of lead content - lead sulfate precipitation - EDTA back titration method; --- Part 3: Determination of the amount of aluminum oxide - Chromazurin S spectrophotometric method; --- Part 4: Determination of zinc content EDTA titration method; --- Part 5: Determination of the amount of arsenic atomic fluorescence spectrometry; --- Part 6: Determination of bismuth content by polarography; --- Part 7: Determination of copper content by flame atomic absorption spectrometry; --- Part 8: Determination of bismuth content by dithiodiantipyrine methane spectrophotometry; --- Part 9: Determination of magnesium oxide by flame atomic absorption spectrometry; --- Part 10: Determination of silver and gold content lead precipitation or pyrolysis gold and flame atomic absorption spectrometry; --- Part 11: Determination of mercury content atomic fluorescence spectrometry and direct solid injection method; --- Part 12: Determination of the amount of cadmium flame atomic absorption spectrometry; --- Part 13: Determination of the amount of thallium by inductively coupled plasma mass spectrometry and inductively coupled plasma-atomic emission spectrometry; --- Part 14: Determination of silica content Molybdenum blue spectrophotometry; --- Part 15: Determination of soluble lead content by flame atomic absorption spectrometry; --- Part 16: Determination of calcium oxide content by flame atomic absorption spectrometry; --- Part 17: Determination of aluminum, magnesium, iron, copper, zinc, cadmium, arsenic, antimony, bismuth, calcium content Inductively coupled plasma atomic emission light spectral method: Please note that some contents of this document may refer to patents: The issuing agency of this document assumes no responsibility for identifying patents: This document is proposed by China Nonferrous Metals Industry Association: This document is under the jurisdiction of the National Nonferrous Metals Standardization Technical Committee (SAC/TC243): This document was drafted by: Beikuang Testing Technology Co:, Ltd:, Industrial Analysis and Testing Center of Guangdong Academy of Sciences, Kunming Metallurgical Research Institute Co:, Ltd:, Shenzhen Zhongjin Lingnan Nonferrous Metals Co:, Ltd:, Zijin Mining Group Co:, Ltd:, Jiangxi Copper Lead and Zinc Metal Co:, Ltd: Co:, Ltd:, National Standard (Beijing) Inspection and Certification Co:, Ltd:, Hunan Nonferrous Geological Survey Research Institute, Nantong Customs Comprehensive Technology Center, Daye Nonferrous Metals Design and Research Institute Co:, Ltd:, Shandong Hengbang Smelting Co:, Ltd:, Fumin Xinye Industry and Trade Co:, Ltd:, Tongling Nonferrous Metals Group Holding Co:, Ltd: Ltd: The main drafters of this document: Han Xiao, Ruan Guise, Fang Di, Su Chunfeng, Ma Yanfang, Liu Yingbo, Yuan Lili, Qiu Qingliang, Tang Huaquan, Hu Mengqiao, Sun Yunchao, Dou Huaizhi, Liu Yan, Luan Haiguang, Kong Fanli, Wang Jing, Xiong Xiaoyan, Yang Yunjin, Lin Ye, Liu Yongyu, Dai Bin, Huang Lining, Ding Juxiang, Liu Xiaoyan, Wang Feihu, Feng Junhua, Wu Yong, Zhang Yucheng, Liu Min:IntroductionLead concentrate is the main raw material for the production of metallic lead, lead alloys, lead compounds, etc: Lead is second only to copper, aluminum, and zinc in the consumption of non-ferrous metals in my country: GB/T 8152 "Chemical Analysis Methods of Lead Concentrates" stipulates the chemical analysis methods for the content of each element in lead concentrates, aiming to meet the quality requirements of lead concentrates: Arbitration and inspection needs: GB/T 8152 consists of 17 parts: --- Part 1: Determination of lead content acid dissolution-EDTA titration method; --- Part 2: Determination of lead content - lead sulfate precipitation - EDTA back titration method; --- Part 3: Determination of the amount of aluminum oxide - Chromazurin S spectrophotometric method; --- Part 4: Determination of zinc content EDTA titration method; --- Part 5: Determination of the amount of arsenic atomic fluorescence spectrometry; --- Part 6: Determination of bismuth content by polarography; --- Part 7: Determination of copper content by flame atomic absorption spectrometry; --- Part 8: Determination of bismuth content by dithiodiantipyrine methane spectrophotometry; --- Part 9: Determination of magnesium oxide by flame atomic absorption spectrometry; --- Part 10: Determination of silver and gold content lead precipitation or pyrolysis gold and flame atomic absorption spectrometry; --- Part 11: Determination of mercury content atomic fluorescence spectrometry and direct solid injection method; --- Part 12: Determination of the amount of cadmium flame atomic absorption spectrometry; --- Part 13: Determination of the amount of thallium by inductively coupled plasma mass spectrometry and inductively coupled plasma-atomic emission spectrometry; --- Part 14: Determination of silica content Molybdenum blue spectrophotometry; --- Part 15: Determination of soluble lead content by flame atomic absorption spectrometry; --- Part 16: Determination of calcium oxide content by flame atomic absorption spectrometry; --- Part 17: Determination of aluminum, magnesium, iron, copper, zinc, cadmium, arsenic, antimony, bismuth, calcium content Inductively coupled plasma atomic emission light spectral method: In the original series of national standard methods, zinc is determined by volumetric method, aluminum is determined by spectrophotometry, and calcium, magnesium, cadmium and copper are determined by atomic absorption spectrometry: Determination of arsenic by atomic fluorescence spectrometry, antimony by cerium sulfate titration and so on: The content of impurity elements such as arsenic, copper, bismuth in lead concentrate has exceeded the original The upper limit of the measurement range of the series method standards, and there is no method for the determination of iron, so the establishment of inductively coupled plasma atomic emission spectrometry Timely determination of impurity elements in lead concentrate has very important practical significance and necessity: Chemical analysis method of lead concentrate Part 17: Aluminum, magnesium, iron, copper, zinc, cadmium, arsenic, Determination of antimony, bismuth and calcium content Inductively Coupled Plasma-Atomic Emission Spectrometry Caution --- Personnel using this document should have practical experience in formal laboratory work: This document does not address all possible security issues question: It is the user's responsibility to take appropriate safety and health measures and ensure compliance with the conditions stipulated in the relevant national laws and regulations:1 ScopeThis document describes a method for the determination of aluminum, magnesium, iron, copper, zinc, cadmium, arsenic, antimony, bismuth, and calcium in lead concentrates: This document is applicable to the determination of aluminum, magnesium, iron, copper, zinc, cadmium, arsenic, antimony, bismuth and calcium in lead concentrate: The determination range of each element is shown in Table 1: Table 1 Determination range of each element element Measuring range (mass fraction) element Measuring range (mass fraction) Al 0:050~2:00 Cd 0:030~0:20 Mg 0:10~2:00 As 0:020~2:00 Fe 2:00~10:00 Sb 0:010~10:00 Cu 0:50~8:00 Bi 0:030~5:00 Zn 0:50~10:00 Ca 0:50~3:502 Normative referencesThe contents of the following documents constitute the essential provisions of this document through normative references in the text: Among them, dated references For documents, only the version corresponding to the date is applicable to this document; for undated reference documents, the latest version (including all amendments) is applicable to this document: GB/T 6682 Analytical laboratory water specifications and test methods3 Terms and DefinitionsThis document does not have terms and definitions that need to be defined:4 principlesThe sample is decomposed with nitric acid, hydrochloric acid, hydrofluoric acid, perchloric acid, in the mixed acid medium, with inductively coupled plasma atomic emission spectrometer, in The emission intensity of each element was measured at the selected wavelength, and the mass fraction of each element was calculated according to the standard working curve method: ......Tips & Frequently Asked Questions:Question 1: How long will the true-PDF of GB/T 8152.17-2023_English be delivered?Answer: Upon your order, we will start to translate GB/T 8152.17-2023_English as soon as possible, and keep you informed of the progress. 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