GB/T 30936-2014 English PDFUS$299.00 · In stock
Delivery: <= 3 days. True-PDF full-copy in English will be manually translated and delivered via email. GB/T 30936-2014: Determination of chlorpropamide, tolbutamide and carbutamide 3 banned sulfonylureas in cosmetics Status: Valid
Basic dataStandard ID: GB/T 30936-2014 (GB/T30936-2014)Description (Translated English): Determination of chlorpropamide, tolbutamide and carbutamide 3 banned sulfonylureas in cosmetics Sector / Industry: National Standard (Recommended) Classification of Chinese Standard: Y42 Classification of International Standard: 71.100.70 Word Count Estimation: 13,190 Date of Issue: 7/8/2014 Date of Implementation: 11/1/2014 Quoted Standard: GB/T 6682 Regulation (derived from): 2014 National Standards Bulletin No. 18 Issuing agency(ies): General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China Summary: This standard specifies the cosmetics chlorpropamide, tolbutamide and carbutamide three kinds of substances sulfonylurea disabled liquid chromatography (HPLC) and liquid chromatography - mass spectrometry/mass spectrometry (LC-MS/MS)test methods. This sta GB/T 30936-2014: Determination of chlorpropamide, tolbutamide and carbutamide 3 banned sulfonylureas in cosmetics---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order. Determination of chlorpropamide, tolbutamide and carbutamide 3 banned sulfonylureas in cosmetics ICS 71.100.70 Y42 National Standards of People's Republic of China Cosmetics chlorpropamide, tolbutamide and carbutamide Determination of three kinds of substances sulfonylurea disabled Determinationofchlorpropamide, tolbutamideandcarbutamide Issued on. 2014-07-08 2014-11-01 implementation Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China Standardization Administration of China released ForewordThis standard was drafted in accordance with GB/T 1.1-2009 given rules. The standard proposed by China National Light Industry Council. This standard by the National Standardization Technical Committee of Fragrance Flavor and Cosmetic (SAC/TC257) centralized. This standard was drafted. Shandong Institute of Product Quality Supervision, Inspection and the State Environmental Protection Product Quality Supervision and Inspection Center, Shandong Freda Biological Engineering Co., Ltd., Shanghai Daily Chemical Industry Institute (Fragrance Flavor and Cosmetic National Quality Supervision and Inspection Center). The main drafters of this standard. Wang Jun, Zhou Lili, ACADAMIC LIBRARY Zhang Yan, Zhao Wengang, Hu Mei, Yang Suzhen, Li Hui, Shenzhong Lan, Wang Yanli, Yu Wen Jiang, Yang Ying, Qian Yan.IntroductionThe standard test substance is banned substances of "Hygienic Standard for Cosmetics" provisions, not as a cosmetic raw material, component Added to cosmetics. If technically unavoidable banned substances as impurities into cosmetics, the finished cosmetic products should follow the "Cosmetics Health standards "General requirements for cosmetics, that is, under normal and reasonably foreseeable conditions of use, should not cause harm to human health. China has yet to establish these limit values \u200b\u200bsubstances present standards, the determination of these substances in cosmetics only provide detection methods. Cosmetics chlorpropamide, tolbutamide and carbutamide Determination of three kinds of substances sulfonylurea disabled1 ScopeThis standard specifies performance liquid chromatography cosmetics chlorpropamide, tolbutamide and carbutamide three kinds of substances sulfonylurea disabled (HPLC) and liquid chromatography - mass spectrometry/mass spectrometry (LC-MS/MS) measurement method. This standard applies to creams, lotions, liquid cosmetics etc. chlorpropamide quantitative, tolbutamide and carbutamide measured in; liquid chromatography Spectrum - mass spectrometry/mass spectrometry applied to cosmetics sulfonylureas substances qualitative confirmation. Determination of the standard liquid chromatography chlorpropamide, tolbutamide, carbutamide detection limit of 20mg/kg, the limit of quantification of 60mg/kg; Liquid Mass spectrometry/mass spectrometry chlorpropamide, tolbutamide, carbutamide detection limit of 0.025mg/kg, the limit of quantification of 0.080mg/kg - chromatography.2 Normative referencesThe following documents for the application of this document is essential. For dated references, only the dated version suitable for use herein Member. For undated references, the latest edition (including any amendments) applies to this document. Laboratory use specifications and test methods GB/T 6682 Analysis Method 3 first high performance liquid chromatography (HPLC) 3.1 Principle Acid extracted with methanol, and the extract after centrifugation, were determined by HPLC. External standard. 3.2 Reagents and materials Unless otherwise indicated, the reagents used were of analytical grade water as a water GB/T 6682 regulations. 3.2.1 Methanol. chromatographically pure. 3.2.2 formic acid. 3.2.3 formic acid methanol solution (1%). The exact amount of 1mL 99mL of methanol and formic acid, after mixing spare. 3.2.4 formic acid (0.2%). The exact amount of 0.2mL 99.8mL formic acid and water, mix and reserve. 3.2.5 Standard chlorpropamide, tolbutamide standards, carbutamide standard. not less than 98% purity, chlorpropamide, tolbutamide Urea and ammonia tolbutamide CAS number, molecular formula, molecular mass and structural formula, see Appendix A. 3.2.6 Standard stock solution. Weigh accurately chlorpropamide, tolbutamide and carbutamide standard each 0.1g, accurate to 0.0001g, points Do a 50mL beaker, add appropriate amount of methanol dissolved quantitatively transferred to 100mL solution colorimetric tube, diluted with methanol to the mark, mix, that Have a concentration of 1000mg/L of standard stock solution. -18 ℃ cryopreservation. 3.2.7 mixed standard stock solution. Pipette the appropriate amount each standard stock solution (3.2.6), diluted with methanol. 1 ℃ ~ 4 ℃ cold storage. 3.2.8 microporous membrane. 0.2μm, organic phase. 3.3 instruments and equipment 3.3.1 High performance liquid chromatography (HPLC) instrument. with a UV detector or diode array detector. ......Tips & Frequently Asked Questions:Question 1: How long will the true-PDF of GB/T 30936-2014_English be delivered?Answer: Upon your order, we will start to translate GB/T 30936-2014_English as soon as possible, and keep you informed of the progress. 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