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GB/T 22661.1-2008 English PDF

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GB/T 22661.1-2008: Chemical analysis methods of potassium fluoborate -- Part 1: preparation and storage of test samples
Status: Valid
Standard IDUSDBUY PDFLead-DaysStandard Title (Description)Status
GB/T 22661.1-2008149 Add to Cart 2 days Chemical analysis methods of potassium fluoborate -- Part 1: preparation and storage of test samples Valid

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Basic data

Standard ID: GB/T 22661.1-2008 (GB/T22661.1-2008)
Description (Translated English): Chemical analysis methods of potassium fluoborate -- Part 1: preparation and storage of test samples
Sector / Industry: National Standard (Recommended)
Classification of Chinese Standard: H61
Classification of International Standard: 77.120.10
Word Count Estimation: 5,553
Date of Issue: 2008-12-29
Date of Implementation: 2009-11-01
Quoted Standard: GB/T 6679
Regulation (derived from): National Standard Approval Announcement 2008 No.23 (Total No.136)
Issuing agency(ies): General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China
Summary: This standard specifies the sample preparation and storage of raw and dry potassium fluoroborate sample. Preparation and storage of the applicable portion of the original sample and dry potassium fluoroborate sample.

GB/T 22661.1-2008: Chemical analysis methods of potassium fluoborate -- Part 1: preparation and storage of test samples


---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Chemical analysis methods of potassium fluoborade Part 1. Preparation and storage of test samples ICS 77.120.10 H61 National Standards of People's Republic of China Chemical analysis methods of potassium fluoroborate Part 1. Preparation and storage of test samples Posted 2008-12-29 2009-11-01 implementation Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China Standardization Administration of China released

Foreword

GB/T 22661 "potassium fluoroborate chemical analysis method" is divided into 10 parts. --- Part 1. Preparation and storage of test samples; --- Part 2. Determination of the weight of water in the wet method; --- Part 3. Determination of potassium fluoride boric acid sodium hydroxide volumetric method; --- Part 4. Determination of magnesium by flame atomic absorption spectrometry; --- Part 5. Determination of calcium content by flame atomic absorption spectrometry; --- Part 6. Determination of silicon content - Molybdenum blue spectrophotometric method; --- Part 7. Determination of sodium content by flame atomic absorption spectrometry --- Part 8. Determination of the free boronic acid sodium volumetric method; --- Part 9. Determination of the chlorine content of mercuric nitrate volumetric method; --- Part 10. Determination of phosphorus pentoxide content - Molybdenum blue spectrophotometric method. This section GB/T 22661 Part 1. This part is proposed by the China Nonferrous Metals Industry Association. The non-ferrous metal part by the National Standardization Technical Committee. This section is drafted. Hunan Nonferrous fluorine chemical limited liability company. Participated in the drafting of this section. Fluoride Chemicals Co., Ltd., Zhengzhou Research Institute, Aluminum Corporation of China, Hengyang City State Friends Chemical Technology Co., Ltd. The main drafters of this section. Li Zhijian, Zhu Liang, Liao Zhihui, Chen Chun, Xu Jin Xue, Lvjin Kui, Feng Jingdong, Liu Zhihong Huang Ju in particular, Liu Min. Chemical analysis methods of potassium fluoroborate Part 1. Preparation and storage of test samples

1 Scope

This section GB/T 22661 specifies the preparation and storage of the original sample and potassium fluoroborate dried sample. Preparation and Storage This section applies to the original sample and potassium fluoroborate dried sample.

2 Normative references

The following documents contain provisions which, through reference GB/T 22661 in this section constitute provisions of this section. For dated reference documents Member, all subsequent amendments (not including errata content) or revisions do not apply to this section, however, encouraged to reach under this section Parties to research agreement to use the latest versions of these documents. For undated reference documents, the latest versions apply to this section. GB/T 6679 General rules for sampling solid chemical products Preparation and storage of specimens 3 3.1 laboratory sample Using GB/T 6679 stipulated in laboratory sample preparation and storage methods. 3.2 original sample For some geometric properties measured for testing certain physical and physico-chemical properties, as well as for determination of hygroscopic moisture. Take about 300g solid Laboratory sample (3.1), which was stored in a sealed container, the container is almost filled sample is appropriate. 3.3 drying specimens Chemical tests for the determination of certain geometrical characteristics and certain physical and chemical physics test. 3.3.1 Sample grinding The sample was milled and sieved until all of 0.125mm sieve pore size of up. The sample mixing sieved at 110 ℃ ± 5 ℃ drying 2h. 3.3.2 Equipment 3.3.2.1 test sieve. its sieve size of 0.125mm. Not tested by introducing an impurity element material, and be based on potassium fluoroborate Properties measured impurity element selected test sieves. 3.3.2.2 mortar. steel made of jade or agate. 3.3.2.3 electric oven. Natural convection ventilation, to control the temperature of 110 ℃ ± 5 ℃. 3.3.3 Procedure 3.3.3.1 About 100g laboratory sample (3.1) through the test sieve (3.3.2.1), the sieve residue particles on the mortar (3.3.2.2 ) Milled and sieved again, sieved material was added to the front of the screen carefully mixing the compound. Repeated grinding, screening, mixing until all samples All through a sieve so far. 3.3.3.2 The sample (3.3.3.1) into a platinum dish, and put into an electric oven (3.3.2.3), and at a temperature of 110 ℃ ± 5 ℃ drying 2h . and After removing the platinum dish from an electric oven, placed in the dryer to cool to room temperature. 3.3.3.3 The sample (3.3.3.2) stored in airtight containers for the storage requirements of the container volume to almost completely filled by the sample Appropriate.
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