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Delivery: <= 3 days. True-PDF full-copy in English will be manually translated and delivered via email. GA/T 1914-2021: Forensic sciences - Examination methods for oleandrin and adynerin in biological samples - LC-MS Status: Valid
Basic dataStandard ID: GA/T 1914-2021 (GA/T1914-2021)Description (Translated English): Forensic sciences - Examination methods for oleandrin and adynerin in biological samples - LC-MS Sector / Industry: Public Security (Police) Industry Standard (Recommended) Classification of Chinese Standard: A92 Word Count Estimation: 11,118 Issuing agency(ies): Ministry of Public Security GA/T 1914-2021: Forensic sciences - Examination methods for oleandrin and adynerin in biological samples - LC-MS---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order. Forensic sciences - Examination methods for oleandrin and adynerin in biological samples - LC-MS ICS 13.310 CCSA92 People's Republic of China Public Safety Industry Standards Oleandrin and oleander in forensic biological samples Detection of Oleandrin B by Liquid Chromatography-Mass Spectrometry Published on 2021-10-14 2022-05-01 Implementation Published by the Ministry of Public Security of the People's Republic of China forewordThis document is in accordance with the provisions of GB/T 1.1-2020 "Guidelines for Standardization Work Part 1.Structure and Drafting Rules of Standardization Documents" Drafting. Please note that some content of this document may be patented. The issuing agency of this document assumes no responsibility for identifying patents. This document is proposed by the National Criminal Technology Standardization Technical Committee Toxic Analysis Sub-Technical Committee (SAC/TC179/SC1). focal point. This document is drafted by. Ministry of Public Security Material Evidence Identification Center, Hangzhou Public Security Judicial Identification Center, People's Public Security University of China. The main drafters of this document. Wang Fanglin, Luan Yujing, Yao Yiren, Ying Jianbo, He Hongyuan. Oleandrin and oleander in forensic biological samples Detection of Oleandrin B by Liquid Chromatography-Mass Spectrometry1 ScopeThis document specifies the liquid chromatography-mass spectrometry of oleandrin and oleandrin B in biological samples (blood, urine) in the field of forensic science (LC-MS) inspection method. This document is suitable for the qualitative analysis and quantitative analysis of oleandrin and oleandrin B in biological samples (blood, urine) in the field of forensic science. analysis. Other test materials can be used for reference.2 Normative referencesThe contents of the following documents constitute essential provisions of this document through normative references in the text. Among them, dated citations documents, only the version corresponding to that date applies to this document; for undated references, the latest edition (including all amendments) applies to this document. GB/T 6682 Analysis Laboratory Water Specifications and Test Methods GA/T 122 Toxic Analysis Terminology3 Terms and DefinitionsTerms and definitions defined in GA/T 122 apply to this document.4 PrinciplesWith blank samples and added samples as controls, the biological samples were extracted, purified and concentrated according to the requirements of parallel operations, and liquid chromatography was used Spectroscopic-tandem mass spectrometry detection was based on retention time, mass spectral characteristic ion pair and ion pair abundance ratio as qualitative judgment basis; peak area was used as the basis for qualitative judgment. The data were quantitatively analyzed by external standard method.5 Reagents and materials5.1 Reagents The experimental water should meet the first-class water specified in GB/T 6682.Unless otherwise stated, the reagents used in the analysis were of chromatographic grade, including Include the following reagents. a) Acetonitrile. b) Methanol. c) Formic acid. d) Ammonium formate. e) Phosphate buffer solution (pH is 6.0). Weigh 8.34 g of sodium dihydrogen phosphate (analytical grade), 0.87 g of disodium hydrogen phosphate (analytical grade), and put them in 1000mL volumetric flask, add water to dissolve, and dilute to the mark. ......Tips & Frequently Asked Questions:Question 1: How long will the true-PDF of GA/T 1914-2021_English be delivered?Answer: Upon your order, we will start to translate GA/T 1914-2021_English as soon as possible, and keep you informed of the progress. The lead time is typically 1 ~ 3 working days. 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