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GA/T 1906-2021 English PDF

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GA/T 1906-2021: (Forensic Science Inspection of 10 drugs including methamphetamine in biological samples Liquid chromatography-mass spectrometry)
Status: Valid
Standard IDUSDBUY PDFLead-DaysStandard Title (Description)Status
GA/T 1906-2021299 Add to Cart 3 days (Forensic Science Inspection of 10 drugs including methamphetamine in biological samples Liquid chromatography-mass spectrometry) Valid

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Basic data

Standard ID: GA/T 1906-2021 (GA/T1906-2021)
Description (Translated English): (Forensic Science Inspection of 10 drugs including methamphetamine in biological samples Liquid chromatography-mass spectrometry)
Sector / Industry: Public Security (Police) Industry Standard (Recommended)
Classification of Chinese Standard: A92
Classification of International Standard: 13.310
Word Count Estimation: 13,146
Date of Issue: 2021-10-14
Date of Implementation: 2022-05-01
Issuing agency(ies): Ministry of Public Security

GA/T 1906-2021: (Forensic Science Inspection of 10 drugs including methamphetamine in biological samples Liquid chromatography-mass spectrometry)


---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
ICS 13.310 CCSA92 People's Republic of China Public Security Industry Standards Methamphetamine and more in forensic science biological samples Liquid Chromatography-Mass Spectrometry for Testing 10 Drugs Released on 10-14-2021 2022-05-01 implementation Released by the Ministry of Public Security of the People's Republic of China

foreword

This document is in accordance with the provisions of GB/T 1.1-2020 "Guidelines for Standardization Work Part 1.Structure and Drafting Rules for Standardization Documents" drafting. Please note that some contents of this document may refer to patents. The issuing agency of this document assumes no responsibility for identifying patents. This document was proposed by the National Criminal Technology Standardization Technical Committee Toxic Analysis Sub-Technical Committee (SAC/TC179/SC1) and submitted Focus on. This document was drafted by. Narcotics Control Bureau of the Public Security Bureau of Yunnan Province, Procuratorial Technology Information Research Center of the Supreme People's Procuratorate, Yuxi City Public Security Bureau Institute of Science and Technology. The main drafters of this document. Li Hong, Wang Chaohong, Zhao Meng, Li Shaopeng, Yang Fazhen, Chen Kang, Li Jiyin, Liu Hongmin, Zhang Wenjing. Methamphetamine and more in forensic science biological samples Liquid Chromatography-Mass Spectrometry for Testing 10 Drugs

1 Scope

This document regulates methamphetamine, amphetamine, MDA (3,4-methylenedioxyphenylpropanoid) in forensic science biological samples (blood, urine) amine), MDMA (3,4-methylenedioxymethamphetamine), MBDB[N-methyl-1-(3,4-methylenedioxyphenyl)-2-butylamine], MDEA (3,4-methylenedioxyethylamphetamine), cathinone, methcathinone, PMMA (paramethoxymethamphetamine), ketamine and other 10 poisons Liquid chromatography-tandem mass spectrometry (LC-MS/MS) qualitative and quantitative testing method for the product. This document applies to methamphetamine, amphetamine, MDA, MDMA, MBDB, Qualitative and quantitative analysis of 10 drugs including MDEA, cathinone, methcathinone, PMMA, and ketamine. Other test materials can refer to use.

2 Normative references

The contents of the following documents constitute the essential provisions of this document through normative references in the text. Among them, dated references For documents, only the version corresponding to the date is applicable to this document; for undated reference documents, the latest version (including all amendments) is applicable to this document. GB/T 6682 Analytical laboratory water specifications and test methods GA/T 122 Toxicological Analysis Terminology

3 Terms and Definitions

The terms and definitions defined in GA/T 122 apply to this document.

4 principles

Using the blank sample and the added sample as a control, according to the requirements of parallel operation, the 10 kinds of drugs in the biological samples (see the appendix for compound information) A) After extraction and purification, use liquid chromatography-tandem mass spectrometry for qualitative and quantitative analysis. The abundance ratio was used as the basis for qualitative judgment; the peak area was used as the basis for quantitative analysis with external standard method.

5 Reagents and materials

5.1 Reagents The experimental water should meet the first-class water specified in GB/T 6682.Unless otherwise stated, all reagents used in the analysis were chromatographically pure. Reagents include. a) Methanol; b) acetonitrile; c) 0.3% formic acid solution. Measure 1.5mL of formic acid, dilute with water and set the volume to 500mL;
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